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1.
A process of physical refining wheat germ oil using the technique of molecular distillation (MD) is presented in this work. Wheat germ oil was obtained from the germ by solvent extraction using hexane and also by cold pressing. The oil extracted with hexane was degummed and bleached before deacidification in order to modify the parameters of phosphorus and color. The goal in carrying out the stage of physical refining by MD was to preserve the maximum amount of original antioxidative potential obtained from extraction of the crude oil. The effect of evaporation temperature of one‐stage MD on the efficiency of free fatty acid elimination was studied. The antioxidant portion was followed by means of analytic determination of tocopherols by high‐performance liquid chromatography. Tocopherol retention up to 98% was achieved in the oil extracted by pressing, and yields of up to 96% were achieved in the oil extracted with hexane. Copyright © 2007 Society of Chemical Industry  相似文献   
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An investigation of the effect of reaction conditions on product distribution in the skeletal isomerisation reaction of linear butenes has been carried out. The main reaction routes over ferrierite have been identified. Beside the main product isobutene, major by-product formation occurs. The unwanted reactions include dimerisation of butene to form octenes, hydrogen transfer yielding small amounts of saturated C3 and C4 hydrocarbons and disproportionation producing propene and pentenes. The most abundant by-products were pentene and propene, though these were not formed in equimolar amounts as could be expected. Oligomerisation experiments of propene over ferrierite produced large amounts of butene and pentene, revealing the presence of adsorbed nonene. The cracking of this surface species to hexene and propene is the most likely reaction route for the excess propene formation. This additional path to propene formation operates mainly at temperatures above 623 K.  相似文献   
4.
Stress in the parenting role has been found to be related to family functioning and parenting behavior. However, most research in this area has been conducted with clinical samples and has not compared parenting stress of mothers and fathers. In this study, 589 married couples with young children (12 to 60 months old) completed the Parenting Stress Index-Short Form (Abidin, 1990) and measures of child-rearing behaviors and attitudes, social support, and child behavior. The validity of Abidin's measure and theoretical model was tested, and results were mixed. Small effects were found for mothers and fathers, and these were moderated by child age and marital happiness. Stress as a normal consequence of parenting is discussed. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   
5.
Microwave-Assisted Reaction Sintering of Bismuth Titanate-Based Ceramics   总被引:1,自引:0,他引:1  
Bismuth titanate-based ceramics, pure and doped with 5 mol% WO3, were prepared by reaction-sintering using a microwave oven. High densities, ≥96% of theoretical density were achieved with very short thermal treatments, with soaking time ranging from 5 to 15 min. Relatively small platelet-like grains were formed, and microstructure seemed not to be strongly affected by doping nor soaking time. Electrical measurements were performed and, as expected, a decrease of electrical conductivity was observed in WO3-doped materials. The results of reaction-sintered samples, both conventional as well as microwave sintered, are compared with those of samples prepared with previously calcined powders and sintered using microwaves as well as a conventional electric furnace.  相似文献   
6.
This article describes the application, at the team and individual level, of findings from the positive psychology research. An overview of this research is presented focusing on several areas generally included in the positive psychology domain: flow, appreciative inquiry, the broaden and build theory, and other strategies for increasing the experience of positive emotions and the identification and deployment of strengths. The authors propose that these applications show promise in consulting psychology engagements and may have merit when utilized by practitioners themselves. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   
7.
The goal of the present studies was to construct and validate a short form of the 50-item Smoking Consequences Questionnaire (SCQ; T. H. Brandon & T. B. Baker, 1991), a measure of smoking outcome expectancies. In Study 1, a 21-item short form (S-SCQ) was derived from a sample of 107 young adults previously treated for substance abuse. In Study 2, the measure was cross-validated on 125 adolescents in treatment for substance abuse. Confirmatory factor analyses revealed good model fit and factorial invariance for the 4 S-SCQ subscales across both samples. Validation analyses on each sample found that subscale scores generally correlated significantly with smoking-related variables. The present studies provide initial evidence for the utility of the S-SCQ when used with young adults and adolescents. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   
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In diethyl ether extracts from celeriac (Apium graveolens L. var.rapaceum) all four stereoisomers of (3a–7a)-cis-3-butylhexahydrophthalide were found to be present. The analyses were carried out by means of GC, enantioselective GC and GC-MS. The assignment of the relative configuration of the diastereomers3 and4 was accomplished by NOE difference spectroscopy.
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9.
Three- and 4-yr-old children were tested for comprehension of knowledge formation. In Exp 1, 34 Ss watched as a surprise was hidden under 1 of 4 obscured cups. The experimenter then pointed to the cup. All children searched under the correct cup, but no 3-yr-olds (in contrast to most 4-yr-olds) could explain how they knew where to look. Ss then discriminated between simultaneous pointing by 2 adults, one who had hidden a surprise and one who had left the room before the surprise was hidden. Most 4-yr-olds (but no 3-yr-olds) showed clear discrimination between the adults. In Exp 2, 16 Ss were tested with procedures designed to make the source of their own knowledge more obvious, but this had no effect on performance. It is concluded that studies using very similar procedures with chimpanzees and rhesus macaques were measuring an ability (or inability) to understand how knowledge states form. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   
10.
The development of verbal and spatial working memory was investigated with an interference paradigm. Memory spans were obtained from 3 groups (8-, 10-, and 19-yr olds) under 6 different conditions: Two primary memory tasks (1 verbal, 1 spatial) were administered in isolation and in conjunction with 2 versions of a secondary task. The primary tasks required recalling a series of visually presented digits and recalling the locations of Xs in a series of visually presented grids. The secondary tasks required reporting the color of the stimuli as they were presented using either a verbal or a spatial response. Analyses revealed that all age groups showed domain-specific interference (i.e., interference by a secondary task from the same domain as the primary task), but only the 8-yr-olds also showed nonspecific interference (i.e., interference by a secondary task from a domain different than the primary memory task), suggesting that at least some executive functions do not reach adult levels of efficiency until approximately age 10. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   
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