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排序方式: 共有191条查询结果,搜索用时 15 毫秒
1.
Marcela Stoia Cornelia Păcurariu Ciprian Mihali Iosif Mălăescu Cătălin Nicolae Marin Aylin Căpraru 《Ceramics International》2019,45(2):2725-2735
Magnetic MnFe2O4 nanopowders were synthesized by an original solvothermal method in the absence and in the presence of tetra-n-butylammonium bromide (TBAB) and Tween 80 (TW) as surfactants. Manganese ferrite/polyaniline (PANI) hybrid materials were synthesized by in situ polymerization of aniline on the surface of MnFe2O4 using ammonium persulfate as oxidant. The purpose of the study was to investigate the influence of the two surfactants on the properties of the MnFe2O4 powders and of their composites with PANI. The specific surface area, the cumulative surface area of pores and the cumulative volume of pores are influenced by the nature of surfactant in case of MnFe2O4 powders and are higher by comparison to those of the MnFe2O4/PANI hybrid materials. The values of saturation magnetization in case of MnFe2O4 powders are higher than those of the hybrid materials and are not influenced by the surfactant nature. These features revealed that MnFe2O4 powders can be efficiently used as adsorbents for the purification of wastewaters. The values of the electrical conductivity of the composites exhibit a significant increase in comparison to the MnFe2O4 powders and depend on the surfactant nature. The highest value of electrical conductivity was achieved by the composite obtained using Tween 80 as surfactant (σDC = 54.5·10?5S?m?1) which was close to that of PANI (σDC = 61.2·10?5 S?m?1). The fact that the magnetic and electric properties of the synthesized MnFe2O4/PANI composites can be changed by design, demonstrate the high potential of these materials to be used in magneto-electric applications. 相似文献
2.
Analytical model of displacement amplification and stiffness optimization for a class of flexure-based compliant mechanisms 总被引:1,自引:0,他引:1
The paper formulates an analytical method for displacement and stiffness calculations of planar compliant mechanisms with single-axis flexure hinges. The procedure is based on the strain energy and Castigliano’s displacement theorem and produces closed-form equations that incorporate the compliances characterizing any analytically-defined hinge, together with the other geometric and material properties of the compliant mechanism. Displacement amplification, input stiffness and output stiffness calculations can simply be performed for any serial compliant mechanism. The class of amplifying compliant mechanisms that contain symmetric corner-filleted or circular flexure hinges is specifically addressed here. A parametric study of the mechanism performance is performed, based on the mathematical model, and an optimization procedure is proposed, based on Lagrange’s multipliers and Kuhn-Tucker conditions, which identifies the design vector that maximizes the performance of these flexure-based compliant mechanisms. Independent finite element simulation confirms the analytical model predictions. 相似文献
3.
A rapid and easy analysis method for polymers is presented. The method involves sample preparation by SFE, separation of the extracted compounds by SFC and simultaneous quantitative detection by FID, as well as identification of unknowns by MS. The applications illustrate how structural research work and routine polymer analysis can be done with this time saving method. 相似文献
4.
This paper explores different means of representation for algebraic transductions, i.e., word relations realized by pushdown transducers. The relevance of this work lies more in its point of view rather than any particular result. We are aiming at giving specific techniques for obtaining, or perhaps explaining, decompositions of algebraic (and incidentally, rational) relations, relying solely on their “machine” definition rather than some complex algebraic apparatus. From this point of view, we are hoping to have demystified the heavy formalism employed in the present literature. Some of the novelties of our work are: the use of “stack languages” and “embeddings,” which eliminate the need of arbitrary context-free languages in our characterizations, the study of uniformizations for algebraic transductions and the use of the so-called stack transductions for exposing the anatomy of pushdown transducers.This work was supported by the Natural Science and Engineering Research Council of Canada grants R220259 and OGP0041630. 相似文献
5.
Narad Rampersad Nicolae Santean Jeffrey Shallit Bala Ravikumar 《Theoretical computer science》2009,410(24-25):2431-2441
For each basic language operation we define its “unique” counterpart as being the operation that results in a language whose words can be obtained uniquely through the given operation. These unique operations can arguably be viewed as combined basic operations, placing this work in the popular area of state complexity of combined operations on regular languages. We study the state complexity of unique rational operations and we provide upper bounds and empirical results meant to cast light into this matter. Equally important, we hope to have provided a generic methodology for estimating their state complexity. 相似文献
6.
Terry Anderson John Loftus Narad Rampersad Nicolae Santean Jeffrey Shallit 《Information and Computation》2009,207(11):1096-1118
Given a language L and a non-deterministic finite automaton M, we consider whether we can determine efficiently (in the size of M) if M accepts at least one word in L, or infinitely many words. Given that M accepts at least one word in L, we consider how long a shortest word can be. The languages L that we examine include the palindromes, the non-palindromes, the k-powers, the non-k-powers, the powers, the non-powers (also called primitive words), the words matching a general pattern, the bordered words, and the unbordered words. 相似文献
7.
Lobontiu N 《The Review of scientific instruments》2012,83(1):016107
The bending compliances of generalized notch flexure hinges with transverse or transverse-and-axial symmetry are studied in two particular reference frames. For an end-point reference frame, the cross compliance and the rotary compliance are proportional. When the reference frame is placed at the flexure's midpoint, the cross compliance is zero. The translatory and rotary compliances of only half the flexure hinge are sufficient to calculate the overall compliances of a transverse-symmetry flexure configuration. Similarly, the overall bending compliances of a flexure hinge with transverse-and-axial symmetry require prior calculation of the translatory and rotary compliances of a quarter flexure solely. 相似文献
8.
Radu Nicolae Revnic Gabriela Fabiola tiufiuc Valentin Toma Anca Onaciu Alin Moldovan Adrian Bogdan
igu Eva Fischer-Fodor Romulus Tetean Emil Burzo Rare Ionu tiufiuc 《International journal of molecular sciences》2022,23(15)
We report a very simple, rapid and reproducible method for the fabrication of anisotropic silver nanostars (AgNS) that can be successfully used as highly efficient SERS substrates for different bioanalytes, even in the case of a near-infra-red (NIR) excitation laser. The nanostars have been synthesized using the chemical reduction of Ag+ ions by trisodium citrate. This is the first research reporting the synthesis of AgNS using only trisodium citrate as a reducing and stabilizing agent. The key elements of this original synthesis procedure are rapid hydrothermal synthesis of silver nanostars followed by a cooling down procedure by immersion in a water bath. The synthesis was performed in a sealed bottom flask homogenously heated and brought to a boil in a microwave oven. After 60 s, the colloidal solution was cooled down to room temperature by immersion in a water bath at 35 °C. The as-synthesized AgNS were washed by centrifugation and used for SERS analysis of test molecules (methylene blue) as well as biological analytes: pharmaceutical compounds with various Raman cross sections (doxorubicin, atenolol & metoprolol), cell lysates and amino acids (methionine & cysteine). UV-Vis absorption spectroscopy, (Scanning) Transmission Electron Microscopy ((S)TEM) and Atomic Force Microscopy (AFM) have been employed for investigating nanostars’ physical properties. 相似文献
9.
Muhammad Hamid Raza Kaveh Movlaee Salvatore Gianluca Leonardi Nicolae Barsan Giovanni Neri Nicola Pinna 《Advanced functional materials》2020,30(6)
Hierarchical core–shell (C–S) heterostructures composed of a NiO shell deposited onto stacked‐cup carbon nanotubes (SCCNTs) are synthesized by atomic layer deposition (ALD). A film of NiO particles (0.80–21.8 nm in thickness) is uniformly deposited onto the inner and outer walls of the SCCNTs. The electrical resistance of the samples is found to increase of many orders of magnitude with the increasing of the NiO thickness. The response of NiO–SCCNT sensors toward low concentrations of acetone and ethanol at 200 °C is studied. The sensing mechanism is based on the modulation of the hole‐accumulation region in the NiO shell layer upon chemisorption of the reducing gas molecules. The electrical conduction mechanism is further studied by the incorporation of an Al2O3 dielectric layer at NiO and SCCNT interfaces. The investigations on NiO–Al2O3–SCCNT, Al2O3–SCCNT, and NiO–SCCNT coaxial heterostructures reveal that the sensing mechanism is strictly related to the NiO shell layer. The remarkable performance of the NiO–SCCNT sensors toward acetone and ethanol benefits from the conformal coating by ALD, large surface area of the SCCNTs, and the optimized p‐NiO shell layer thickness followed by the radial modulation of the space‐charge region. 相似文献
10.
Nicolae Dumitru Alexandru Alexandra Ligia Onofrei 《Wireless Personal Communications》2010,53(1):141-151
This paper is focused on the problem of reducing the intercarrier-interference (ICI) power in the transmission over Orthogonal
Frequency Division Multiplexing Systems (OFDM) using pulse shaping methods. A new pulse was proposed here and it was investigated
in terms of ICI interference. It appears to be suitable for transmission in OFDM systems with carrier frequency offset. The
results obtained by calculations show that the performance improvements are significant for reducing average intercarrier-interference
(ICI) power and increasing the ratio of average signal power to average ICI power (SIR). 相似文献