中空激光光内送粉熔池温度控制研究

在激光增材制造过程中,熔池温度的稳定性是表征加工过程稳定性的一个重要指标.设计一套控制熔池温度的闭环反馈系统,以达到控制熔池温度,提高成形件质量.基于C#编程软件实现了温度信号的传递,采用PID控制算法设计了温度控制器.实验结果表明,此系统能实时、准确地实现熔池温度的闭环控制,能够有效消除直壁墙熔覆过程中因热累积而造成的“蘑菇云”现象,且成形件几何精度有显著提高,各处显微组织差异较小,组织致密均匀.     

Catalytic Hydrocracking of a Bitumen‐Derived Asphaltene over NiMo/γ‐Al2O3 at Various Temperatures

Hydrocracking of a bitumen‐derived asphaltene over NiMo/γ‐Al₂O₃ was investigated in a microbatch reactor at varying temperatures. The molar kinetics of asphaltene cracking reaction was examined by fitting the experimental data. Below a defined temperature, the molar reaction showed the first‐order kinetic feature while at higher temperatures secondary reactions such as coke formation became significant, causing deviation of the reaction behavior from the proposed first‐order kinetic model. Selectivity analysis proved that dominant products varied from gases to liquids to gases with increasing temperature, shifting the dominant reaction from C–S bonds cleavage to C–C bonds cleavage.     

油库油料计量操作中存在的问题及其解决办法

介绍了油库油料计量中，在油品高度、油品温度和油品密度测量中存在的问题及应遵循的操作规范和注意事项。     

居住建筑设计的点滴体会

根据石河子的地理位置、自然环境和居住建筑发展的历史,为当地设计了功能较全,布局合理,实用性强的住宅楼。通过设计实践对住宅设计提出了一些看法。     

工业层析洗梯液回收套用的一种方法

以生产甲胺基阿维菌素苯甲酸盐精品的工艺——工业层析产生的洗梯液回收套用的过程为例，说明利用二元恒沸物的组成随压力的变化而变化的规律，对生产洗梯液进行有效、简洁、合理分离及套用的方法。     

基于量化规则格的关联规则渐进更新*

提出一种基于量化规则格的规则更新算法,重点讨论了在新增格节点的过程中规则更新的思想,实现在格的渐增生成过程中,相应的关联规则也得到渐进更新.最后给出简单实例说明规则更新算法的正确性.     

结晶性高聚物作为相变材料的应用

本文研究了结晶性高聚物聚乙烯及其共混物作为相变材料对模拟发热体铜片热量的吸收作用，由于相变的吸热，铜片的温度在一定时间范围内保持在一个定值。选择不同的相变材料，可使这种温度平台出现在不同的温度范围，不共晶的共混物可有两个以上的温度平台，提高了降温效果。     

溶液缩聚物分子量分布及其控制的研究

本文根据溶液缩聚基本原理及反应过程的基本事实，用随机过程方法，得到缩聚产物分子量分布函数，并对分子量及其分布的控制作了讨论。     

Fabricating Water-Insoluble Polyelectrolyte into Multilayers with Layer-by-layer Self-assembly

Summary A water insoluble azo-containing polyelectrolyte (PEAPB6P-AC) was successfully fabricated into multilayer films based on the layer-by-layer adsorption technique by using N, N-dimethylformamide (DMF) as the assembling media. The multilayer growth and structure were studied with UV-vis spectroscopy, and the multilayer surface were imaged with Atomic Force Microscopy and compared with that fabricated in water. The results show that assembling PEAPB6P-AC in DMF can effectively eliminate the hydrophobic aggregation of the azo units and consequently results in a much smoother multilayer surface than that fabricated in water. This improvement to the layer-by-layer adsorption technique, which can avoid some major difficulties faced when assembling hydrophobic polyelectrolytes in aqueous solutions, seems to be a versatile way to fabricate high quality multilayer films when using the hydrophobic even water-insoluble polyelectrolytes as assembling units.     

碳黑水分离技术的研究

脱油沥青作为谢尔气化工艺的气化原料生产化肥在国内尚属首次,由于沥青原料中的灰分和重金属比渣油原料大得多,若仍采用石脑油萃取碳黑技术,灰分和重金属随碳黑返回气化装置,将造成设备的堵塞、磨损,无法保证设备安稳长期运行.通过对碳黑水分离技术进行多方面的研究,寻找到适宜的工艺路线与解决方案.