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1.
Optical pregroove dimensions: design considerations 总被引:1,自引:0,他引:1
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Watabe H Hatazawa J Ishiwata K Ido T Itoh M Iwata R Takahashi T Hatano K Nakamura T 《IEEE transactions on medical imaging》1995,14(4):688-696
We proposed a new method (;linearized method') to analyze neuroleptic ligand-receptor specific binding in a human brain using positron emission tomography (PET). We derived the linear equation to solve four rate constants, k(3), k(4), k(5), k(6) from PET data. This method does not demand a radioactivity curve in plasma as an input function to the brain, and can perform fast calculations in order to determine rate constants. We also tested the nonlinearized method including nonlinear equations which is a conventional analysis using plasma radioactivity corrected for ligand metabolites as an input function. We applied these methods to evaluate dopamine D(2) receptor specific binding of [(11)C] YM-09151-2. The value of B(max)/K(d)=k(3)/k (4) obtained by the linearized method was 5.72+/-3.1 which was consistent with the value of 5.78+/-3.4 obtained by the nonlinearized method. 相似文献
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A specimen heating holder equipped with a gas injector and an evaporator has been developed for use with conventional transmission electron microscopes (TEMs). The developed specimen holder allows both synthesis of metal oxide support and deposition of catalyst nano-particles in situ. Since the holder is designed to be used in small gapped high-resolution objective lens pole-piece, all the procedure from the synthesis of support material to the deposition of catalyst as well as the behavior of the catalyst nano-particles on the support can be observed at near atomic resolution. The developed specimen holder was applied to the study of AuPd catalyst. First, air was injected onto heated aluminum particles via a gas injector to synthesize Al(2)O(3) support. Then, nano-particles of AuPd were deposited on the Al(2)O(3) support. After the deposition, the synthesized Al(2)O(3) support was heated and air was injected again to observe behaviors of the deposited AuPd nano-particles at elevated temperatures in the aerial environment. Behaviors of the AuPd nano-particles such as coalescence, segmentation and diffusion to the Al(2)O(3) support were dynamically observed at atomic level high resolution. 相似文献
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Yaguchi T Suzuki M Watabe A Nagakubo Y Ueda K Kamino T 《Journal of electron microscopy》2011,60(3):217-225
An environmental cell for high-temperature, high-resolution transmission electron microscopy of nanomaterials in near atmospheric pressures is developed. The developed environmental cell is a side-entry type with built-in specimen-heating element and micropressure gauge. The relationship between the cell condition and the quality of the transmission electron microscopic (TEM) image and the diffraction pattern was examined experimentally and theoretically. By using the cell consisting of two electron-transparent silicon nitride thin films as the window material, the gas pressure inside the environmental cell is continuously controlled from 10(-5)?Pa to the atmospheric pressure in a high-vacuum TEM specimen chamber. TEM image resolutions of 0.23 and 0.31?nm were obtained using 15-nm-thick silicon nitride film windows with the pressure inside the cell being around 5?×?10(-5) and 1?×?10(4)?Pa, respectively. 相似文献
5.
Amano T. Nakamura S. Yamada T. Watabe S. Kamitani A. 《Applied Superconductivity, IEEE Transactions on》1992,2(4):205-213
The multiple stability observed exclusively in forced-flow cooled superconductors is numerically calculated, and the result is quantitatively compared with the value measured by J.W. Lue et al. (1980). The calculated and measured values agreed well in certain cases, and did not in others. Based on this comparison, the effects of the transient heat transfer coefficient and ohmic heat generation on the quantitative prediction of stability are discussed. From this comparison, it is learned that a precise understanding of the transient heat transfer coefficient is essential for reliable predictions, and also that the ordinary evaluation method of ohmic heat generation, which considers the flux-flow resistance, tends to overevaluate the situation 相似文献
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Ken Hosoya Mitsuko Bendo Nobuo Tanaka Yoshiyuki Watabe Tohru Ikegami Hiroyoshi Minakuchi Kazuki Nakanishi 《大分子材料与工程》2005,290(8):753-758
Summary: Uniformly sized polymer particles were prepared by an emulsification and polymerization technique utilizing a silica monolithic membrane, namely the “silica monolithic membrane emulsification technique”. In this paper, we utilized silica monolithic membrane as a device for the preparation of uniformly sized polymer particles. A mixture of monomers, diluents and oil‐soluble initiator was emulsified into a continuous medium through the silica monolithic membrane and polymerized. The particles obtained had a higher size uniformity than that of particles prepared by previously reported membrane emulsification techniques, such as the Shirasu Porous Glass (SPG) emulsification technique. Through the silica monolithic membrane emulsification technique, we could prepare particles having availability as a possible packing material for solid‐phase extraction (SPE) and high performance liquid chromatography (HPLC).
7.
High‐resolution synchrotron powder X‐ray diffraction (XRD) experiments were conducted to clarify the transformation of sillimanite to mullite (mullitization) and determine the mullitization temperature (Tc). We were able to distinguish sillimanite and mullite in the XRD patterns, despite their very similar crystallographic parameters, and to detect the appearance of small mullite peaks among sillimanite peaks. Analysis of the Johnson‐Mehl‐Avrami (JMA) equation for mullitization ratio (ζ) revealed that at temperatures T≥1240°C the mullitization had the same kinetics. The activation energy E at T≥1240°C obtained from the Arrhenius plot was 679.8 kJ mol?1. In analysis using a time‐temperature‐transformation diagram for mullitization, a mullitization curve of ζ=1% can be described as where t is time, n is a reaction‐mechanism‐dependent parameter determined as 0.324 by JMA‐analysis, k0 is the frequency factor, EA is the activation energy for atomic diffusion, and represents the activation energy for nucleation. The results of fitting the data to this equation were Tc=1199°C, A=3.9×106 kJ mol?1 K?2, EA=605 kJ mol?1, and k0=3.65×1015. We conclude that the boundary between sillimanite and mullite+SiO2 in the phase diagram is ~1200°C. 相似文献
8.
Tomoki Nakayama Yutaka Matsumi Keiko Kawahito Yoshifumi Watabe 《Aerosol science and technology》2018,52(1):2-12
A new palm-sized optical PM2.5 sensor has been developed and its performance evaluated. The PM2.5 mass concentration was calculated from the distribution of light scattering intensity by considering the relationship between scattering intensity and particle size. The results of laboratory tests suggested that the sensor can detect particles with diameters as small as ~0.3 µm and can measure PM2.5mass concentrations as high as ~600 µg/m3. Year-round ambient observations were conducted at four urban and suburban sites in Fukuoka, Kadoma, Kasugai, and Tokyo, Japan. Daily averaged PM2.5 mass concentration data from our sensors were in good agreement with corresponding data from the collocated standard instrument at the Kadoma site, with slopes of 1.07–1.16 and correlation coefficients (R) of 0.90–0.91, and with those of the nearest observatories of the Ministry of the Environment of Japan, at 1.7–4.1 km away from our observation sites, with slopes of 0.97–1.23 and R of 0.89–0.95. Slightly greater slopes were observed in winter than in summer, except at Tokyo, which was possibly due to the photochemical formation of relatively small secondary particles. Under high relative humidity conditions (>70%), the sensor has a tendency to overestimate the PM2.5 mass concentrations compared to those measured by the standard instruments, except at Fukuoka, which is probably due to the hygroscopic growth of particles. This study demonstrates that the sensor can provide reasonable PM2.5 mass concentration data in urban and suburban environments and is applicable to studies on the environmental and health effects of PM2.5.
Copyright © 2018 American Association for Aerosol Research 相似文献
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