Achieving Rich and Active Alkaline Hydrogen Evolution Heterostructures via Interface Engineering on 2D 1T‐MoS2 Quantum Sheets

Large‐scale production of hydrogen from water‐alkali electrolyzers is impeded by the sluggish kinetics of hydrogen evolution reaction (HER) electrocatalysts. The hybridization of an acid‐active HER catalyst with a cocatalyst at the nanoscale helps boost HER kinetics in alkaline media. Here, it is demonstrated that 1T–MoS₂ nanosheet edges (instead of basal planes) decorated by metal hydroxides form highly active ${\text{edge}}_{{\text{1T‐MoS}}_{\text{2}}}$/ ${\text{edge}}_{\text{Ni}{(\text{OH})}_{\text{2}}}$ heterostructures, which significantly enhance HER performance in alkaline media. Featured with rich ${\text{edge}}_{{\text{1T‐MoS}}_{\text{2}}}$/ ${\text{edge}}_{\text{Ni}{(\text{OH})}_{\text{2}}}$ sites, the fabricated 1T–MoS₂ QS/Ni(OH)₂ hybrid (quantum sized 1T–MoS₂ sheets decorated with Ni(OH)₂ via interface engineering) only requires overpotentials of 57 and 112 mV to drive HER current densities of 10 and 100 mA cm^?2, respectively, and has a low Tafel slope of 30 mV dec^?1 in 1 m KOH. So far, this is the best performance for MoS₂‐based electrocatalysts and the 1T–MoS₂ QS/Ni(OH)₂ hybrid is among the best‐performing non‐Pt alkaline HER electrocatalysts known. The HER process is durable for 100 h at current densities up to 500 mA cm^?2. This work not only provides an active, cost‐effective, and robust alkaline HER electrocatalyst, but also demonstrates a design strategy for preparing high‐performance catalysts based on edge‐rich 2D quantum sheets for other catalytic reactions.     

0Cr20Mn21Ni2N奥氏体不锈钢锻件组织性能研究

研究了无磁钻铤用0Cr20Mn21Ni2N奥氏体不锈钢圆棒锻件横截面的室温强度、硬度和韧性等力学性能,并从微观角度进行了分析。在圆棒表层区域观察到了锻造变形态晶粒组织,而直径四分之一区域为再结晶组织,平均晶粒尺寸为80μm,芯部再结晶晶粒尺寸粗化为150μm,这些差异是由不同的变形温度和降温速度造成的。这种组织差异导致的室温拉伸性能和冲击韧性也有相应的变化趋势。研究结果表明,在900、1000℃以0.5 s-1的应变速率压缩的0Cr20Mn21Ni2N试验钢样品,其应力应变曲线具有一定的加工硬化特征,其芯部硬度比应变速率为0.1 s-1的样品分别提升了28、15 HB。在700、800℃以20%以上的变形量进行压缩时,峰值抗力显著提高,而在900、1000℃以10%~50%的变形量进行压缩时,峰值抗力均无明显提高,可保证顺利的变形过程。     

测试(试井)成果影响因素浅析

随着测试技术的发展、测试质量及资料解释水平的提高，测试（试井）成果的可靠程度越来越受到重视。影响解释成果的环节和因素很多，从客观和主观两方面分析其主要因素，找出症结所在，从而完善现场环节，完善资料解释过程，提高测试技术及解释水平。     

DFIT测试在长庆气田开发中的应用

与常规的小型测试压裂不同，流体注入诊断测试（DFIT）是通过关井阶段出现的拟线性流或拟径向流阶段求取储层压力，采用改进的梅耶霍夫方法（M-method）解释储层渗透率。以长庆榆林气田一口开发井为例，依据DFIT的技术原理和测试步骤，对该井测试压降数据进行解释分析，结果可信度较高，证明了该项工艺在长庆低压低渗油气田的可行性。     

合成氨制气中的以水代汽新工艺

提出了应用油水融合技术在合成氨部分氧化法制气中以水代汽的工艺途径，并分析了其效果和意义。     

激光熔覆前合金粉末的火焰喷涂

火焰喷涂是激光熔覆前合金粉末的预置方法之一。本文在实验的基础上,探讨了工艺过程,并讨论了影响质量的因素。     

提高辽河原油重交通道路沥青的质量

辽河油田石化总厂为提高从辽河原油生产重交通道路沥青的质量，对所用的辽河原油中的低凝点环烷基原油经过分储、分输、分炼，对减压蒸馏塔进行改造，控制减压拔出率，对直馏沥青进行轻度氧化，使９０号重交通道路沥青中沥青质的含量大于１０％，蜡含量小于２％，质量达到了国际先进水平。     

Electrophysiological properties and cholinergic responses of rat ventral oral pontine reticular neurons in vitro

This study analyses the relationship between the use of rotating instruments, the production of a smear layer and the presence of alterations to enamel microstructures. The rotating instruments used were carbide (8-12 blade) and diamond tipped (30-15 m) cutters. Cavities were made in extracted teeth. Subsequently, half the sample was analysed using the rugosimeter before and after the application of ortophosphoric acid at 35% for 15 and the other half suing a Scansion Electronic microscope (SEM). The results obtained showed on the one hand that carbide cutters leave a smoother surfacer than diamond tipped cutters, and on the other that the smear layer is eliminated better by carbide cutters compared to diamond tipped cutters. Moreover, there are no major traumatic-type alterations at the level of the enamel affecting the microstructure after the use of carbide cutters.     

钻速模式动态辨识方法研究

目的：钻进过程是一个复杂的工艺过程，影响钻速的因素错综复杂。为钻井参数优化和实时控制，提出钻速动态模型。方法：对影响钻速的因素进行分析，用系统辨识方法建立钻速模式。结果：利用该方法建立了华北油田岔河集地区的钻速模型，取得满意结果。结论：此动态钻速模式能更准确、科学地描述钻进过程，并在钻井参数最优化、钻井过程的闭环控制等方面具有广阔的应用前景。