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Nanostructured polyaniline films with controlled thickness have been successfully grown on fluorine-doped tin oxide (FTO) glass substrates using the cyclic voltammetry (CV) method at room temperature. The formation mechanism of the polyaniline film is monitored by CV techniques, alternating current (AC) impedance spectroscopy, scanning electron microscopy (SEM) and atomic force microscopy (AFM). It is found that the accumulation of nanostructured polyaniline (>70 nm) on both the scattered and compact layers simultaneously increased the reactive interface, which supports charge transfer at the interface and resistance that hinders electronic transport in the film. By optimising the preparation conditions, the short-circuit photocurrent density of a dye-sensitised solar cell (DSSC) with a PANI counter electrode (CE) increased by 11.6% in comparison to a DSSC with an electrodeposited platinum CE. 相似文献
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Jun Zhang Xiaoxue Li Wei Guo Tubshin Hreid Jinfeng Hou Haiquan Su Zhuobin Yuan 《Electrochimica acta》2011,(9):170
Composite films of poly(3,4-ethylenedioxythiophene) and functionalized, multi-walled, carbon nanotubes (PEDOT–MWCNT) were fabricated by a simple oxidative electropolymerization method. These films were formed on fluorine-doped, tin oxide, glass substrates as counter electrodes (CEs) of platinum-free, dye-sensitized solar cells (DSSCs). The surface morphology, formation mechanism and electrochemical nature of PEDOT–MWCNT films were investigated using scanning electron microscopy (SEM), atomic force microscopy (AFM), cyclic voltammetry (CV) and alternating current (AC) impedance spectroscopy. The SEM and AFM images showed that PEDOT–MWCNT films were more porous than PEDOT films. CV and AC impedance spectroscopy revealed that the PEDOT–MWCNT electrode had higher electrocatalytic activity for the I3−/I− redox reaction and a smaller charge transfer resistance than the PEDOT electrodes. The energy conversion efficiency of the DSSC with a PEDOT–MWCNT CE was 13.0% higher than with a PEDOT CE using the same conditions with a ruthenium sensitizer. 相似文献
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