Preparation and electrochemical characterization of Ti-based amorphous metallic glass with high strength

Ti-based amorphous metallic glasses have excellent mechanical, physical, and chemical properties, which is an important development direction and research hotspot of metal composite reinforcement. As a stable, simple, efficient, and large-scale preparation technology of metallic powders, the gas atomization process provides an effective way of preparing amorphous metallic glasses. In this study, the controllable fabrication of a Ti-based amorphous powder, with high efficiency, has been realized by using gas atomization. The scanning electron microscope, energy-dispersive spectrometer, and X-ray diffraction are used to analyze surface morphology, element distribution, and phase structure, respectively. A microhardness tester is used to measure the mechanical property. An electrochemical workstation is used to characterize corrosion behavior. The results show that as-prepared microparticles are more uniform and exhibit good amorphous characteristics. The mechanical test shows that the hardness of amorphous powder is significantly increased as compared with that before preparation, which has the prospect of being an important part of engineering reinforced materials. Further electrochemical measurement shows that the corrosion resistance of the as-prepared sample is also significantly improved. This study has laid a solid foundation for expanding applications of Ti-based metallic glasses, especially in heavy-duty and corrosive domains.     

滚筒位置参数及摇臂厚度对装煤性能的影响研究

采煤机作为综采工作面的关键设备,其性能直接决定工作面的生产能力,为进一步提升工作面生产能力,在研究滚筒采煤机装煤理论的基础上,基于现有工作面采煤机的参数分别对滚筒位置参数和摇臂厚度对采煤机装煤性能的影响机理进行研究,为后续改进采煤机的结构参数和生产过程中位置参数奠定扎实的理论基础.     

锑酸消除含氚废空气中的氚

用锑酸作消气材料 ,压制成消氚电极 ,在适当外加条件下 ,考察了锑酸作消氚材料直接将含氚废空气中的氚除去的可能性。对消氚过程中料气中氚的浓度及水分对消氚结果的影响进行了考察 ,给出了消气片中氚的物料平衡。结果表明 :在 3 2L含氚空气中 ,用锑酸制成的消氚材料 ,在 2 0 0min左右可将原料气氛中 80 %以上的氚去除     

In-Situ observation on microfracture behavior ahead of the crack tip in 63Sn37Pb solder alloy

in-situ transmission electron microscopy (TEM) tensile tests on as-cast and aged 63Sn37Pb solder alloys were conducted, and the fracture behavior in nanometer scale ahead of the crack tip was inspected and discussed. Results show that the fracture was completed by connecting the discontinuous cracks or voids. Dislocation behavior was concentrated along the grain boundaries for as-cast samples, and displayed mainly as dislocation climb. The crack was intergranular dominated under the lower strain rate. While remarkable mutual dislocation emission was detected in the aged solder. Transgranular cracks were dominant in the fractured area, and they propagated by linking up with the nanometer scale cracks ahead of the crack tips under the effective promotion of the inverse dislocation emission. At the same time, the partial interphase or intergranular cracks in the thinned area were also found. Under this condition, a new critical stress intensity factor K _c ^′ to define the mutual dislocation emission was proposed.     

易逝品联合采购订货决策分析

采购联盟成员间的信息不完全,彼此均以对方的期望需求作为对方实际需求的估计.针对易逝品的特点,提出了调剂价格的特殊约束条件并建立了联盟期望利润模型,最后进行了数值仿真.研究表明:联合采购使联盟总体利润得到改善,但不能使联盟成员的利润都得到改善.     

激光光束质量因子M~2的物理概念与测试方法

激光光束传输质量因子Ｍ２是一种全新的描述激光光束质量的参数，它能定量表征单模、多模光束传播特性。本文介绍Ｍ２的物理概念、特点、测试方法及近年来国外的研究概况。     

废塑料裂化生产汽柴油工业化装置研究

报道了废塑料炼油工艺中连续法、间歇法、半连续法等各种方法的特点 ;重点对各工业化流程中存在的问题和解决的方法进行了讨论 ,并提出了一些合理化的建议。     

艺术建筑设计的探索

通过徐州一中艺术楼的设计实践，寻求优美而独特的艺术形象，并用纯几何形体的组合来达到功能与形式的完美统一。     

低效气藏成因层次剖析

由于我国低效气藏的储量所占比例很大，故而有必要对其进行深入研究，形成适合于不同层面的研究方法和思路，以期达到指导勘探开发生产的目的。为此，将低效气藏剖析为四个层面（气藏开发特征层面、现有地质特征层面、历史地质成因层面、预测及改造层面），并用层次分析法对其进行了研究：第一层次是直接由生产来认识，第二层次通过分析、化验、监测来了解，第三层次通过地质过程和地质历史回溯来表述，第四层次依据现有地质理论，通过地质过程叠合，最终达到预测、改造、有效动用低效气藏的目的。研究结果认为，可以依据不同层次特征对低效气藏进行分类评价：第一层次从经济效益出发，依据投入产出比进行分类；第二层次着眼气藏现今地质特征，表征其地质特征，而储层分布、渗透性则为分类的主要依据；第三层次从气藏形成地质过程着手，分析低效气藏形成过程，沉积和成岩作用作为分类的关键因素；第四层次基于气藏地质特征，预测开发动态，改造气藏特征，促使气藏有效动用。     

城市洪涝试验研究进展

城市洪涝物理试验与原型试验是开展数值模型验证及提高预报预警精度的重要手段。从城市产流过程、地表洪水演进以及地表径流与管网水流交互三方面,综述了近年来国内外城市洪涝试验的研究进展。针对目前城市洪涝试验研究中存在的不足,指出今后应完善现有城市产汇流过程相关机理方面的试验研究,深入研究地表与管网垂向交互过程,加强与城市洪涝期间的流动行为密切相关过程的定量试验研究。