Comparative studies on thermal and toughness properties of polybenzoxazine composites with two functionalized graphene oxides

Abstract

Graphene oxide (GO) was functionalized by polyether amine (PEA) via two methods which were one-pot modification in acetone (GON) and two steps with the intermediate product of GOCO-Cl generated (GONS). There were more PEA successfully grafted onto GO for GONS than GON. The onset polymerization temperatures of the benzoxazine (Bz) composites decreased by the inclusion of 1?wt% of GO, GON or GONS. Thermal stability of the polybenzoxazine (PBz) composites was significantly improved indicated from the increase of weight loss temperature. T₁₀, T₂₀ and T₅₀ values of the composites with GONS were higher than that of the others. Toughness of PBzs may be enhanced by the incorporation of nanofillers, and GONS had stronger interfacial interaction with PBz matrix than GON.     

基于Lab VIEW的小型汽油机磁电机点火提前角的测量

本文介绍了磁电机点火系统的点火提前角测量原理。对点火系统的点火信号和触发信号进行采集、调理，再用单片机进行处理，最后用LabVIEW进行点火提前角数据存储和显示。     

臭氧氧化-光催化降解水中的五氯酚

利用臭氧氧化-光催化技术降解水中的有机污染物五氯酚(PCP)。对比了紫外光照射、臭氧氧化、光催化、臭氧氧化-光催化4种方法降解PCP的情况。考察了臭氧氧化-光催化体系中臭氧流量、臭氧产量、PCP初始质量浓度、pH和CO23-等因素对PCP降解率的影响。实验结果表明,臭氧氧化-光催化法比单独使用紫外光照射、臭氧氧化、光催化法更能有效的去除PCP;增加臭氧流量和臭氧产量有利于提高PCP的降解率;降低PCP的初始浓度,PCP的降解率显著提高;pH对PCP的降解效果影响不明显;CO23-的存在显著降低了PCP的降解率。在臭氧氧化-光催化体系中,除臭氧直接氧化降解PCP外,臭氧与TiO2协同作用产生的.OH对PCP的降解也起到了重要作用。     

GPS接收机多径误差及窄相关性能分析

减少GPS接收机多径干扰的办法是采用特殊天线和在接收机中采取一定的措施。文中针对窄相关技术展开分析。重点分析影响接收机多径误差的因素及窄相关的性能，并给出仿真及分析结果。     

双能X射线骨密度仪测定技术研究

以Ｌｕｎａｒ公司ＤＰＸ－Ｌ型双能Ｘ射线骨密度仪为例，研究引起测量误差的主要因素并提出质控措施。用自检模块、腰椎体膜评定仪器的体外测量精度好于１％。对１０位志愿者重复２次测量，体内精度对腰椎，ＭＰＤ（平均百分差）为０．４６，ＣＶ（变异系数）为０．７５；对股骨颈，ＭＰＤ为１．２６、ＣＶ为０．４７；Ｗａｒｄ’ｓ三角区ＭＰＤ为２．０１、ＣＶ为１．１４；大转子ＭＰＤ为１．６６、ＣＶ为０．７２。扫描图像由２位     

An improved generative adversarial network for translating clothes from the human body to tiled image

Neural Computing and Applications - Nowadays, purchasing the products similar to the styles of stars’ products has become a new trend in e-commerce platforms. Clothing transaction constitutes...     

嵌入式三轴运动控制系统的以太网通信实现

研究了嵌入式三轴运动控制系统的以太网通信问题;采用LM3S9B92微控制器设计主控制器和各轴电动机控制器,通过移植实时操作系统μC/OS-Ⅱ和TCP/IP协议栈LwIP,实现主控制器与各轴电机控制器之间的信息交互;按电动机控制数据传输紧急程度要求不同,在以太网MAC层之上建立调度表,优先传输紧急数据,提高三轴运动控制系统实时性;实验结果表明嵌入式三轴运动控制系统实现了以太网数据的无差错传输,并且在重载情况下时间延迟大约为系统改进前的72%,改进了系统的实时性。     

Synthesis and xylene isomers adsorption of silicalite-1 crystals with intracrystalline mesopores aided by 3-glycidoxypropyl-trimethoxysilane and polyethene glycol

Journal of Porous Materials - Well-defined silicalite-1 crystals with intracrystalline mesopores were successfully synthesized in the presence of 3-glycidoxypropyl-trimethoxysilane (GPTMS) and...     

基于碳化硅器件的无线充电系统电源设计

碳化硅(SiC)器件耐高频高温、散热性能好、导通电阻小,应用于无线充电系统可有效提高无线充电系统的效率。文中首先对比了SiC材料与Si材料的特性,在此基础上研制了一套基于SiC器件的无线充电系统电源装置。该装置由整流模块和逆变模块构成,输入端接市电,且装置的整流模块具有功率因数校正功能。文中详细给出了整流模块的整流桥选型策略、滤波电路参数设计方法、Boost电路功率器件和无源元件设计原则及开关管控制电路设计方法,还给出了逆变模块的开关管选型策略、开关管驱动电路和开关管保护电路的设计方法。最后,实验结果验证了方案的有效性和可行性,输入侧实现了高功率因数,逆变电路开关管电压振荡得到抑制,实验样机的效率峰值可达98.2%。     

Correction to: Bismuth Yttrium Oxide (Bi3YO6), A New Electrode Material For Asymmetric Aqueous Supercapacitors

Journal of Inorganic and Organometallic Polymers and Materials - The original version of this article unfortunately contained mistakes. In line 9 of the abstract, 5% should read as 2%. The...