α,β,γ,δ-四(5-磺基噻吩)卟啉柱前衍生反相液相色谱法分离测定铜、镉和钴

以α ,β ,γ ,δ 四 (5 磺基噻吩 )卟啉为柱前衍生试剂 ,用含 1.5mmol/LH3BO3-NaOH缓冲溶液 (pH9.0 )和 5. 0× 10 - 3mol/L溴代三丁基胺 (TBA Br)的乙氰 -水 (3 0 :70 ,V/V)溶液作流动相 ,检测波长 43 0nm ,在KromasilC1 8柱上 ,同时分离测定了铜、镉和钴三种金属络合物 ,检出限 (S/N =3 )分别为 0 .2 0 ,0.16,和 0.13ng/mL。方法用于水样分析 ,结果与光度法相符。     

基于信息流动分析的动态社区发现方法

随着社交网络和微博等互联网应用的逐渐流行,其用户规模在迅速膨胀.在这些大规模网络中,社区发现可以为个性化服务推荐和产品推广提供重要依据.不同于传统的网络,这些新型网络的节点之间除了拓扑结构外,还进行频繁的信息交互.信息流动使得这些网络具有方向性和动态性等特征.传统的社区发现方法由于没有考虑到这些新的特征,并不适用于这些新型网络.在传染病动力学理论的基础上,从节点间信息流动的角度,提出一种动态社区发现方法.该方法通过对信息流动的分析来发现联系紧密、兴趣相近的节点集合,以实现动态的社区发现.在真实数据集上的实验结果表明：相对于传统的社区发现方法,所提出的方法能够更准确地发现社区,并且更能体现网络中社区的动态变化.     

Numerical simulation of cutting process of the slice components cutting machine

By the use of ANSYS/LS-DYNA FEA software,numerical simulation on the cutting process of cutting plates with a reamer was carried out in the paper. The logical improvement was brought forward and the phenomenon of stress concentration was deceased by weighted analysis. The effects of different cut velocities and cutting thickness on life-spans of reamers were investigated, and the cutting parameters were optimized to satisfy the cutting precision and cutting efficiency. The study will provide a guide for the practical production.     

基于改进小波阈值函数的船用雷达回波去噪

为了对船用雷达（9GHz脉冲雷达）回波降噪,提出了基于小波阈值函数的改进方法,分析了中间阈值以及对应的阈值函数对船用雷达回波信号降噪的影响.在模拟雷达回波信号的降噪实验中,对新的阈值方法与软阈值、硬阈值、Firm阈值、Yasser阈值方法进行了比较.通过对阈值函数参数的调整,使得新的小波阈值函数得到更高的信噪比、更小的均方根误差和更大的能量比,证明了新方法的有效性;在实测雷达回波信号的降噪实验中,得到了一致的结论,证明了新方法的实用性.     

高性能MCU的FPGA原型验证系统研究与平台实现

本文研究并实现了一种基于Cortex-A7核的高性能MCU在FPGA原型阶段的验证平台。该设计研究可以针对高性能MCU芯片或其FPGA原型验证阶段的软硬件验证环境快速搭建,通过交互式、软硬件协同的方式对MCU芯片各个模块功能进行实时、可靠的功能验证。高效的FPGA原型验证可以提高MCU研发速度、缩短验证时间、提高验证效率、及时发现芯片设计的缺陷、缩短芯片研发周期。     

基于前向纠错的自适应网络传输机制

针对无线网络中的传输控制协议（TCP）因为丢包触发丢包重传机制而导致传输性能大幅下降的问题,提出了一种基于前向纠错的自适应传输机制（AdaptiveFEC）。该机制通过前向纠错来减少数据段的丢失,以避免触发TCP的丢包重传机制,从而达到提升TCP传输性能的目的。首先,根据当前的网络状况以及当前连接的数据传输特征确定当前时间段中的最优冗余段比例;然后,利用TCP数据段中的数据段序号信息实时进行网络状况的估计,从而根据网络波动来动态更新冗余段比例。大量实验结果说明,在20 ms的往返时延以及5%丢包率的传输环境中,相较于静态的前向纠错机制,AdaptiveFEC能够使得TCP连接的传输速率平均提升42%,当运用在文件下载的应用中时,所提机制能够使得下载速度提升至原来的两倍。     

面向动用计划的车辆装备备件预测研究

针对动用计划下的车辆装备备件的消耗特点,研究了车辆装备维修备件消耗量和库存控制两个预测优化问题。考虑动用计划期内车辆装备的预防性维修和修复性维修,实现定时定程维修和自然随机故障维修下装备维修备件的消耗量的预测。在此基础上,根据备件库存检查方式的特点,建立基于定期检查策略的联合补货库存控制模型,根据模型的结构特点确定决策变量界限,并利用多类种群位置更新方式改进了果蝇优化算法。仿真结果表明,改进的果蝇优化算法具有良好的求解效率,本文所提出的优化方法可为车辆维修保障资源优化提供决策依据。     

采用自适应字典学习的InSAR降噪方法

We consider the phase noise filtering problem for interferometric synthetic aperture radar (InSAR) based on the dictionary learning technique. Due to the non-convexity of the optimization problem is difficult to solve. By using the splitting technique and employing the augmented Lagrangian framework, we obtain a relaxed nonlinear constraint optimization problem with l₁-norm regularization which can be solved efficiently by the alternating direction method of multipliers (ADMM). Specifically, we firstly train dictionaries from the InSAR complex phase data, and then reconstruct the desired complex phase image from the sparse representation. Simulation results based on simulated and measured data show that this new InSAR phase noise reduction method has a much better performance than several classical phase filtering methods in terms of residual count, mean square error (MSE) and preservation of the fringe completeness.     

Investigation on experimental method of low-impedance materials using modified Hopkinson pressure bar

To increase the detectability of split Hopkinson pressure bar (SHPB) of low-impedance materials, modifications were conducted on traditional SHPB apparatus with a PMMA tube to output transmitted signal, and weak signals were further amplified by semiconductor strain gauges. Experiments on soft rubbers and cushioning foam materials were carried out. In order to analyze the accuracy of the experimental results, the stress equilibrium issues involved in the assumptions of SHPB were investigated. First, by way of re-constructing loading process of incident wave, the stress-strain curve was obtained, along with the stress equilibrium ratio of specimen. Secondly, the influences on the accuracy of stress-strain curves were investigated through the elastic modulus comparisons. And the results illustrate that the bilinear incident wave from experiments can ensure the stress equilibrium deformation of specimen after 2 normalized times, much sooner than ramp incident waves. Moreover, it even facilitates specimen deformation with a constant strain rate. The results confirm that the detectability of the modified SHPB can be down to tens kPa with enough accuracy level.     

北斗信号捕获相位相干算法的设计与实现

针对北斗二号卫星导航系统信号捕获运算量大的问题,提出一种利用相位相干算法搜索起始码相位的方法,并给出基于现场可编程门阵列(FPGA)的相位相干算法的具体实现方案,算法中关于旋转因子运算的问题主要借助坐标旋转数字计算方法和查找表方法得以解决。编译综合及仿真结果皆表明,与传统快速傅里叶变化(FFT)算法相比,新方法只需用到复数加法,运算量小,且能正确捕获信号。