The Synthesis of Sulfated Titanium Oxide Nanotubes

TiO₂ nanotubes can be prepared in gram quantities by treating anatase TiO₂ powder with concentrated NaOH solution. These TiO₂ nanotubes acquired strong acidity after being impregnated with sulfuric acid solution and calcined at 300 °C. The anatase TiO₂ powder used to prepare the nanotube did not catalyze the esterification between cyclohexanol and acetic acid, while sulfated TiO₂ nanotubes were very reactive toward the esterification reaction.     

Effect of Thickness of the p-AlGaN Electron Blocking Layer on the Improvement of ESD Characteristics in GaN-Based LEDs

The following letter presents a study regarding GaN-based light-emitting diodes (LEDs) with p-type AlGaN electron blocking layers (EBLs) of different thicknesses. The study revealed that the LEDs could endure higher electrostatic discharge (ESD) levels as the thickness of the AlGaN EBL increased. The observed improvement in the ESD endurance ability could be attributed to the fact that the thickened p-AlGaN EBL may partly fill the dislocation-related pits that occur on the surface of the InGaN-GaN multiple-quantum well (MQW) and that are due to the strain and the low-temperature-growth process. If these dislocation-related pits are not partly suppressed, they will eventually result in numerous surface pits associated with threading dislocations that intersect the InGaN-GaN (MQW), thereby reducing the ESD endurance ability. The results of the experiment show that the ESD endurance voltages could increase from 1500 to 6000 V when the thickness of the p-AlGaN EBL in the GaN LEDs is increased from 32.5 to 130 nm, while the forward voltages and light output powers remained almost the same.     

Directly Compressible Acetaminophen Compositions Prepared by Fluidized-Bed Granulation

Polyvinylpyrrolidone (PVP) in aqueous solution was used as a binding agent in a fluidized-bed system to agglomerate acetaminophen powder into directly compressible granules. It was found that a minimal amount of 5% w/w PVP in a concentration of 7.5% w/v or less was needed to produce granules with an acceptable flow and the corresponding tablets having enough hardness without capping. There was a strong correlation between the time for 80% dissolved (T₈₀) and the logarithm of granule volume-surface mean diameter. A directly compressible acetaminophen composition to manufacture tablets having a T₈₀ value less than 30 min can be prepared simply by adding an appropriate amount of disintegrant (crospovidone, sodium starch glycolate, or pregelatinized starch) to the agglomerated granules.     

On the hollowness ratio effect on the dynamics of a spinning Rayleigh beam

The analytical solutions of a spinning Rayleigh beam with rotatory moment inertia and gyroscopic effect are presented in this paper. The critical speeds can be written analytically in a function of the length-to-radius ratio (l) defined by the beam's length over its outer radius and the hollowness ratio (α) defined by the hollow area over the total area of the cross section. The sensitivity analyses show that the critical speed is decreasing with l, but increasing with α. Moreover, α is more sensitive to the critical speeds. The design of a spinning beam should therefore be emphasized more on the hollowness factor. Contrary to common belief, only finite critical speeds exist and the number is independent of the boundary conditions. It increases monotonically with l, but decreases with α. The steady state unbalanced response can therefore be expressed analytically by the finite precessional modes and the corresponding generalized coordinates.     

Testing multi-characteristic product capability indices

Recently, studies associated with testing the quality and performance of each process for a product with multi-characteristics are proposed more often. However, most studies are limited to discussing one single type of quality characteristic. Practically, a multi-characteristic product is potentially composed of three types: smaller-the-better, larger-the-better, and nominal-the-best. In this paper, we propose an integrated product capability index which considers these three different types of quality characteristics. According to the theory of testing hypothesis, we develop a testing procedure for the product capability index to judge whether the process capabilities of total quality characteristics meet the customers’ demands. In addition, the relationship between the product capability index and the yield of the entire product will be introduced. Finally, an example is provided as a practical application.     

Modified Hopfield neural networks for retrieving the optimalsolution

Due to the rugged energy function of the original Hopfield networks, the output is usually one local minimum in the energy function. An analysis on the locations of local minima in Hopfield networks is presented, and a modified network architecture to eliminate such local minima is described. In particular, another amplifier is introduced at the processor nodes to give correction terms. This modified Hopfield network has been successfully applied to the construction of analog-to-digital converters with optimal solutions. Experimental results on the voltage transfer characteristics of data converters are presented.     

Partitioning and mapping nested loops on multiprocessor systems

A method for executing nested loops with constant loop-carried dependencies in parallel on message-passing multiprocessor systems to reduce communication overhead is presented. In the partitioning phase, the nested loop is divided into blocks that reduce the interblock communication, without regard to the machine topology. The execution ordering of the iterations is defined by a given time function based on L. Lamport's (1974) hyperplane method. The iterations are then partitioned into blocks so that the execution ordering is not disturbed, and the amount of interblock communication is minimized. In the mapping phase, the partitioned blocks are mapped onto a fixed-size multiprocessor system in such a manner that the blocks that have to exchange data frequently are allocated to the same processor or neighboring processors. A heuristic mapping algorithm for hypercube machines is proposed     

Determination of glycyrrhizin and glycyrrhetinic acid in traditional Chinese medicinal preparations by capillary electrophoresis

A simple, rapid, accurate and reproducible capillary electrophoretic method was developed for the assay of glycyrrhizin and glycyrrhetinic acid in traditional Chinese medicinal preparations. The buffer solution used in this method was acetonitrile and 0.02 M sodium dihydrogen-phosphate solution adjusted to pH 7.5 with 0.05 M sodium hydroxide. The linear calibration range was 0.04-2.00 mg/ml (r = 0.9988) for glycyrrhizin and 0.007-0.35 mg/ml (r = 0.9985) for glycyrrhetinic acid and recoveries were 98.1-101.3% for glycyrrhizin and 98.5-101.4% for glycyrrhetinic acid. The relative standard deviations were 1.02% (n = 6) for glycyrrhizin and 0.91% (n = 6) for glycyrrhetinic acid. The content of these two acids in Glycyrrhizae Radix and Glycyrrhizae Radix-containing Chinese medicinal preparations was successfully determined within 10 min.     

A programmable analog VLSI neural network processor forcommunication receivers

An analog VLSI neural network processor was designed and fabricated for communication receiver applications. It does not require prior estimation of the channel characteristics. A powerful channel equalizer was implemented with this processor chip configured as a four-layered perceptron network. The compact synapse cell is realized with an enhanced wide-range Gilbert multiplier circuit. The output neuron consists of a linear current-to-voltage converter and a sigmoid function generator with a controllable voltage gain. Network training is performed by the modified Kalman neuro-filtering algorithm to speed up the convergence process for intersymbol interference and white Gaussian noise communication channels. The learning process is done in the companion DSP board which also keeps the synapse weight for later use of the chip. The VLSI neural network processor chip occupies a silicon area of 4.6 mmx6.8 mm and was fabricated in a 2-mum double-polysilicon CMOS technology. System analysis and experimental results are presented.