计算机控制的SEESR实验系统的研制

SEESR(Simultaneous Electrochemical ESR)是研究电极过程中的自由基中间体行为的理想和方便的手段。在以前研制的ESR仪数据系统的基础上,我们应用IBM-PC/XT微机与JES-FE1XG型(JEOL产)ESR谱仪及HDV-7型恒电位仪研制了一套由计算机控制的SEESR实验装置。该系统可以完成包括循环伏安法、电流阶跃、电位阶跃及电位反转等多种电化学方法的SEESR实验。系统还具有包括数据平滑、曲线拟合等功能的多种数据处理软件,使用方便。我们应用模型化合物对该系统进行了实际测量,所得结果与文献报道一致。     

ZS1756振动筛动态分析

应用ＳＡＰ５Ｐ软件计算矿用振动筛前４０阶固有模态，从提高寿命观点看，第１阶，第３－４阶和第６阶模态应采取抑制措施；从队噪观点看，前６阶模态应给予注意。     

Top-Down方法在成型模具设计中的应用

介绍模具Top—Down设计的基本思想、设计流程及其主要特点，并基于Pro/Engineer软件平台，以一鞋楦模具为设计对象，例示出模具Top—Down设计方法的主要设计过程。采用先进的Top-Down模具设计方法可以帮助设计者提高设计速度，避免一般设计中容易发生的错误，降低设计制造成本，加快交货期限。     

A code-pattern-driven digital background calibration technique for SAR ADCs

The article presents the buck converter for the application on headlights of vehicle with chip-level design. The LED components are used as for lighting source, which near/far lights are controlled with high-current switching circuit in the chip. The level-shift circuit and its current driver is proposed to control the input of high-voltage power MOS. The bypass method is presented to reduce the transient time as load current changes suddenly. The input voltage widely ranges from 8 to 21 V while keeping a stable output voltage with 6 V. The chip current can output from 20 to 1500 mA with excellent regulation. This chip had been implemented with TSMC0.25 µm HV- process, and the size of the circuit layout is about 8.6 mm², where includes power switch and far/near lighting switches. Measurements show that peak efficiency can achieve 86.3%. The power regulation is excellent, where the load regulation is only 0.3%, and the line regulation is only 0.5%.

     

Feasibility study of the application of voltage contrast to printed circuit board

Voltage contrast (VC) has been a powerful tool for the failure analysis of integrated circuits and multichip module. As the packing density of printed circuit board (PCB) is increasing, conventional failure analysis methods to detect open or short circuit in PCBs are no longer adequate, and voltage contrast method could be a method for this purpose. However, unlike the cases of integrated circuits and multichip module, there are many areas in PCB that will produce serious charging effect when examine under the scanning electron microscope. One of the areas is the presence of solder mask on PCB.This work examines the feasibility of using voltage contrast for PCB failure analysis. Specially designed PCB is used for experimentation, and it is found that positive bias on one track and zero bias on another copper track provide a better image contrast as compared to negative and zero biases on the tracks. Also, the variation of the image contrast with different spacing between inter copper tracks has studied. It is found that the variation depends on the presence of solder mask and its location. The variation can be very different for negative bias case as compared to the positive bias case.Finite element analysis is also performed to explain the experimental observations. All the observations can be well explained by the charging effect of the solder masks. The charging effect of solder mask is indeed very significant in affecting the image contrast, and it could reduce the contrast to almost zero in some cases.     

振动筛振动方向角的调整

建立振动筛力学模型和运动微分方程，推导出振动方向角的表达式，通过分析影响振动方向角的因素，提出振动方向角的调整方法。     

偏苯三酸酐修饰的吸附树脂对苯酚和对硝基苯酚的吸附研究

通过后交联及化学修饰反应制备了偏苯三酸酐修饰的超高交联吸附树脂(TMA),研究了TMA树脂对苯酚和对硝基苯酚的吸附行为。结果表明,TMA树脂具有较高的比表面积和较丰富的微孔,对苯酚和对硝基苯酚均具有较好的吸附性能,且吸附过程为典型的物理吸附,其等量吸附焓变、自由能变和熵变均为负值。Langmuir和Freundlich等温方程均能较好地拟合苯酚和对硝基苯酚在TMA树脂上的吸附等温线。吸附动力学过程符合准一级动力学方程,颗粒内扩散过程是TMA树脂吸附苯酚和对硝基苯酚的主要控制步骤。     

大菱鲆病原鳗弧菌生物学及分子特征研究

从山东沿海养殖发病大菱鲆分离了5株鳗弧菌。5株菌对大菱鲆有较强的致病性,LD50范围为2.32×101～4.03×102cfu/g鱼;5株菌分别属于O1、O2、O3血清型,菌株之间的16SrRNA基因序列相似性范围97.1%～99.9%;与国外报道的鳗弧菌的序列相似性范围为89.7%～99.9%。5株菌的生理生化特征与鳗弧菌标准菌株一致,能产生多种胞外酶和溶血素;都含有金属蛋白酶基因和溶血素基因,其中3株菌各含有一个67kb大质粒。病原菌对青霉素、苯唑青霉素、氨苄青霉素、先锋霉素Ⅳ、先锋霉素Ⅴ、先锋霉素Ⅵ、链霉素、强力霉素、洁霉素、万古霉素、灭滴灵等11种常用抗菌药物有抗性,只对新生霉素、呋喃妥因、利福平、新霉素等4种药物敏感。     

海盐污秽下悬式绝缘子闪络电压特性试验

通过涂污的XP-70型绝缘子在盐雾条件下的人工污秽试验,研究在粉尘污染源较少且靠近海的地区海盐污秽单独对表面洁净绝缘子闪络特性的影响,以及在粉尘污染源较多且靠近海的地区粉尘污秽和海盐污秽共同对绝缘子闪络特性的影响。试验结果表明:盐雾电导率越大,绝缘子的闪络电压越低;绝缘子表面等值附盐密度越大,其闪络电压越低。针对沿海地区环境情况,对海盐污染地区绝缘子选型提出建议:粉尘污源较少地区选用钟罩型玻璃绝缘子;粉尘污源较多地区选用复合绝缘子,但应综合考虑其老化特性。     

浙江省火力发电机组非计划停运统计及预防

通过对2015—2018年纳入浙江省技术监督管理系统的火力发电机组非计划停运事件的统计与分析,找出影响机组运行可靠性的主要故障原因和薄弱环节,为发电厂增强设备故障预防,加强运行、维护与管理等方面指明方向,提供建议及参考依据。