工艺参数设置和厚度对电子束熔融加工Ti-6Al-4V合金微观结构的影响

研究了试件尺寸和工艺参数(电子束强度,扫描速度,焦点偏移量和扫描长度)对电子束熔融(EBM)加工Ti-6Al-4V合金微观结构的影响。结果表明,可以观察到EBM加工的Ti-6Al-4V合金的微观结构由原始β相的柱状晶粒组成。在柱状晶粒内部观察到典型的(α+β)结构,即魏氏体α片和在细小的α晶粒的界面上形成的杆状β相。还发现沿原始β柱状晶粒的晶界形成的α层晶界。随着试件厚度、电子束能量密度和扫描长度的增加,先前的β柱状晶粒的直径增大,并且生长的方向与加工方向一致。同时,柱状晶粒直径随着试件高度的增加而减小。随着试件厚度和电子束能量密度的增加,α片会变得更粗大。     

Orientation Dependence of the Micro-Pillar Compression Strength in an Electron Beam Melted Ti–6Al–4V Alloy

An α/β two-phase Ti-6 Al-4 V alloy was fabricated by electron beam melting to obtain a basketweave structure.The orientation dependence of the mechanical properties of Ti-6 Al-4 V alloy was studied by micro-pillar compression and post-mortem transmission electron microscopy analysis.The results indicate that different grains have different mechanical responses,and the possible attributions were discussed.Besides the orientation effect,due to the limited volumes of micropillars,the size of the a phases,dispersion of the β phases,and the presence of the free dislocation path also affect the mechanical properties of the micropillars to a large extent.Although no direct link was discovered between the mechanical properties and the parent βorientations,this work provided a promising method to further study the anisotropic mechanical behavior in Ti-6 Al-4 V alloy.     

中国城市能源环境效率研究

随着中国能源和环境问题日益凸显,如何平衡经济增长和可持续发展成为现在中国发展迫切需要解决的问题。而能源环境效率是其重要的研究指标,本文采用EBM模型对中国60个城市2015年能源环境效率进行了测算。通过研究得出如下结论:经济发展水平越高的城市越有可能有较高的效率;我国城市效率存在明显差异性,存在城市发展不平衡问题;一线城市能源环境效率普遍较高,二线城市效率普遍不高,三线城市效率普遍较低,四线城市及五线城市效率差异较大;大部分资源型城市为四线城市及五线城市,城市不同的能源禀赋、主导产业、科研能力、环境状况以及为保护环境采取的各类措施都会对城市的能源环境效率产生影响。     

用放射性核素体外分析法研究仙灵、地黄液的药理作用

动物实验表明仙灵液可提高肺-β受体含量,提高大鼠血浆及肺组织中cAMP含量;地黄液可降低大鼠血浆、肺组织中cGMP含量及降低大鼠E_2含量。两药均使cAMP/cGMP比值升高,亦可提高大鼠皮质醇含量。     

Mechanical behavior of electrochemically hydrogenated electron beam melting (EBM) and wrought Ti–6Al–4V using small punch test

The influence of electrochemical charging of hydrogen at j = ?5 mA/cm² for 6, 12, 48 and 96 h on the structural and the mechanical behavior of wrought and electron beam melting (EBM) Ti–6Al–4V alloys containing 6 wt% β and similar impurities level was investigated. The length of the α/β interphase boundaries in the EBM alloy was larger by 34% compared to that in the wrought alloy. The small punch test (SPT) technique was used to characterize the mechanical behavior of the non-hydrogenated and hydrogenated specimens. It was found that the maximum load and the displacement at maximum load of the wrought alloy remained nearly stable after 6 h of charging, showing a maximum decrease of ～32% and 11%, respectively. Similarly, hydrogenation of the EBM alloy resulted in a gradual degradation in mechanical properties with charging time, up to ～81% and 86% in pop-in load and displacement at the “pop-in” load, respectively. The mode of fracture of the wrought alloy changed from ductile to semi-brittle with mud-cracking in all hydrogenated specimens. In contrast, the mode of fracture of the EBM alloy changed from a mixed mode ductile-brittle fracture to brittle fracture with star-like morphology. The degraded mechanical properties of the EBM alloy are attributed to its α/β lamellar microstructure which acted as a short-circuit path and enhanced hydrogen diffusion into the bulk as well as δ_a and δ_b hydride formation on the surface. In contrast, a surface layer with higher concentration of δ_a and δ_b hydrides in the wrought alloy served as a barrier to hydrogen uptake into the bulk and increased the alloy resistivity to hydrogen embrittlement (HE). This study shows that EBM Ti–6Al–4V alloy is more susceptible to mechanical degradation due to HE than wrought Ti–6Al–4V alloy.     

Modelling of anisotropic elastic properties in alloy 718 built by electron beam melting

ABSTRACT

Owing to the inherent nature of the process, typically material produced via electron beam melting (EBM) has a columnar microstructure. As a result of that, the material will have anisotropic mechanical properties. In this work, anisotropic elastic properties of EBM built Alloy 718 samples at room temperature were investigated by using experiments and modelling work. Electron backscatter diffraction data from the sample microstructure was used to predict the Young’s modulus. The results showed that the model developed in the finite element software OOF2 was able to capture the anisotropy in the Young’s modulus. The samples showed transversely isotropic elastic properties having lowest Young’s modulus along build direction. In addition to that, complete transversely isotropic stiffness tensor of the sample was also calculated.

This paper is part of a thematic issue on Nuclear Materials.     

面向EBM技术的悬挂部件钛合金快速制造

EBM技术是1990年代中期发展起来的现代先进制造技术,文中介绍了EBM技术的基本原理、特点、应用前景以及悬挂部件钛合金的快速制造工艺过程。     

Effects of cutting angle,edge preparation,and nano-structured coating on milling performance of a gamma titanium aluminide

Gamma titanium aluminides are intermetallic alloys. Recently, they have been evaluated as important contenders for structural applications in the automotive and aerospace sectors. This is due to their excellent high-temperature performances and their significantly lower density compared to nickel-based superalloys. In this paper, an analysis of machinability of a gamma TiAl obtained via an electron beam melting (EBM) process is presented. The effects of tool geometry modifications, in terms of cutting tool angles and cutting edge preparation, were investigated. The reduction of radial rake angle and the drag finishing process for cutting edge preparation resulted in an increase of the tool life of the carbide end mills. Nanogradient tool coatings were also observed to affect tool wear during milling tests, and the results highlight that AlSiTiN coating performs better compared to CrAlSiN coating. A post-coating polishing treatment was also taken into account, and it allowed a further reduction of tool wear. The overall results indicate that the machinability of this difficult-to-cut material can be significantly improved by an adjustment of the cutting edge geometry, and by using an AlSiTiN coating system.     

Study,Mechanical Characterization and Mathematical Modeling of Compatible SEBS Blends for Industrial Applications in Orthopedics and Childcare

In this work, a system of compatible blends based on two commercial grades of a thermoplastic elastomer, styrene-ethylene/butylene-styrene (SEBS), with extreme Shore A hardness values (5 and 90), was studied in order to obtain a range of different performance blends for orthopedic and childcare applications, where usually liquid silicone rubber is used. Mechanical properties of different blends were obtained, and Equivalent Box Model (EBM) was used for the prediction of the mechanical behavior. The results show good agreement between the theoretical model and experimental data of new blends of SEBS.     

三元乙丙橡胶与乙烯-丁烯弹性体在电线电缆绝缘中的并用

通过三元乙丙橡胶与乙烯-丁烯弹性体的并用,以过氧化物DCP为硫化剂,TAIC为共硫化剂。研制出具有良好的介电绝缘性能、物理机械性能及加工工艺性能的胶料。生产的成品电缆性能完全能满足符合GB/T5013—2008及JB/T 8735—2011标准要求。