Precipitating spinel into precursor glass and its assistance in crystallization

The crystallization phenomena of spinel in CaO-MgO-Al₂O₃-SiO₂-Fe₂O₃ glass have received much attention due to the particular role in preparation of glass-ceramic materials, which represent an effective option to manage hazardous waste. In this study, both preliminary spinel and secondary spinel were precipitated in the precursor glass. The formation of these spinel was meticulously assessed by a combination of X-ray diffractometry and scanning electron microscopy. The structure of the microenvironment in the precursor glass was characterized by Raman spectrums. These advanced techniques highlight the potential for one-step crystallization of the glass. The investigation, which focused on one-step crystallization, demonstrated the growth of pyroxene on spinel accompanying a migration of chromium. The results also show the microstructure of the obtained glass-ceramic was very dependent on the heat-treat temperature. This study not only unambiguously reveals the precipitation mechanisms of spinel but also provides more documentation for one-step crystallization in the glass-ceramics field.     

乘法器复用技术在滑窗FIR滤波处理中的运用

随着超大规模集成电路的飞速发展,FPGA集成的硬件乘法器越来越多,内核时钟越来越快,使得FPGA在实时信号处理中得到广泛应用。介绍了FIR滤波运算的原理与硬件处理结构,通过乘法器的复用技术,解决了实现滑窗FIR滤波处理时,FPGA内部乘法器的高速运算与外部慢速数据率之间的矛盾。     

产学模式在《数据库原理》课程教学改革中的应用

针对目前《数据库原理》课程采用传统教学模式存在的诸多问题,就如何提高应用型本科计算机专业学生对《数据库原理》课程的学习兴趣和解决实际问题的能力,提出了产学相结合的数据库原理课程教学模式,首先让学生在工程化环境中进行相关理论学习,同时提供课程网站等辅助手段进行扩展学习,在此基础上根据企业的实际需求模拟环境让学生进行实践,并对其实践展开了进一步讨论。     

铌铁酸铅PFN的结构无序及介电相变特性

运用高分辨透射电镜显微技术观察到ＰＦＮ中Ｂ位离子呈无序排列，不易形成有序结构，在性能上，ＰＦＮ的介电常数ε和介电损耗ｔｇδ均很大，相变扩散度小；相应时的介电行为，热容和热膨胀的变化比较特殊。     

深圳河湾污水系统研究

深圳河湾污水截排工程投资超过人民币5亿元。工程方案坚持以科学的发展观为指导，将节水与防污相结合，将发展循环经济作为方案研究的出发点与落脚点，对深圳河湾流域的污水处理尾水排海、污水资源化、水体生态修复等作出了长远规划。     

由西点军校成为企业家摇篮所引发的思考

提起西点，人们会自然而然地联想到这座举世闻名的军校所培养造就的无数杰出军事人才。在世人眼中，这里是军事家的摇篮，是荣誊和胜利的象征。然而，许多人并不清楚，西点除了为美国培养出众多的军事人才外，也造就了无数的企业家和商业精英。结合西点的成功，从职业伦理道德、心理素质训练、领导能力训练三方面入手，简要分析了高等教育中重“做事”教育轻“做人”教育的危害以及“做事”教育与“做人”教育紧密结合的重要性。     

试析书院德育课程体系的构建

古代书院在培养人才、化育人生等方面取得了重大成就，而这与书院的课程体系是分不开的。书院以“明人伦”和“传道济民”为依据，设置了以经学为主体，以史学为补充的基本德育课程体系。     

Enhanced piezoelectric properties and temperature stability of Bi4Ti3O12-based Aurivillius ceramics via W/Nb substitution

Bi₄Ti₃O₁₂ (BIT), a typical Aurivillius ceramics with high Curie temperature (T_c ? 675 °C), has great potential for high temperature applications. This work provides an effective method of inducing structure distortion, relieving the tetragonal strain of the TiO₆ octahedron and decreasing the concentration of oxygen vacancies to improve the piezoelectricity and temperature stability of BIT ceramics. Bi₄Ti_2.98W_0.01Nb_0.01O₁₂ possesses an optimum piezoelectric coefficient (d₃₃) of 32 pC/N, a high T_c of 655 °C and a large resistivity of 3 × 10⁶ Ω·cm at 500 °C. The maximum d₃₃ reported here is approximately quadruple than that of pure BIT (?7 pC/N). Moreover, the d₃₃ of W/Nb co-doped BIT and the in-situ temperature stability of the compression-mode sensor present a highly stable characteristic in the range of 25–600 °C. These results imply that W/Nb-modified BIT ceramics is a promising candidate for application at high temperatures of up to 600 °C.     

Elimination mechanism of micropores on bonding interface during solid-state crystal growth method

A pure yttrium aluminum garnet (YAG) ceramic/YAG single crystal composite material is prepared using the optimized solid-state crystal growth (SSCG) method. The micropores on the bonding interface of the composite sample are eliminated for the first time during the SSCG process and the transmittance is very close to the theoretical value, which reached 83.14% at 1064 nm. Meanwhile, the mechanism of elimination and migration of the pores under high temperature is studied. Additionally, the single crystal growth rate has significantly improved and the time of composite sample preparation has also significantly reduced proving that the SSCG method is an effective method for producing high quality composite material.     

Influence of LiBO2 addition on the microstructure and lithium-ion conductivity of Li1+xAlxTi2−x(PO4)3(x = 0.3) ceramic electrolyte

Concerning the safety problems of conventional Li-ion batteries with liquid electrolytes, it is crucial to develop reliable solid-state electrolytes with high ionic conductivity. Li_1+xAl_xTi_2?x(PO₄)₃ (LATP, x = 0.3) is regarded as one of the most promising solid electrolytes due to its high ionic conductivity and excellent chemical stability to humidity.Herein, a new strategy is proposed for improving the sintering behavior and enhancing the ionic conductivity of LATP by using LiBO₂ as the sintering aid via liquid phase sintering. The as-prepared sample LATP with homogeneous microstructure and high relative density of 97.1% was successfully synthesized, yielding high total ionic conductivity of 3.5 × 10^?4 S cm^?1 and low activation energy of 0.39 eV at room temperature. It was found that the addition of LiBO₂ could effectively enhance the densification and increase the ionic conductivity of LATP electrolyte, proving an effective way to synthesis LATP ceramics by a simple and reliable route.