过共晶铝硅合金细化初晶硅的研究

研究了ZL8604过共晶铝硅合金初晶硅细化剂和加入方式与加入量以及影响细化效果的冶铸工艺因素,实验结果达到了技术指标要求。     

高速钢坯料制备工艺的问题与对策

现行的高速钢坯料制备工艺主要是电渣重熔和粉末冶金两大类。其中电渣重熔锭比普通冶炼模铸钢锭的组织致密,明显改善了初始共晶碳化物的分布,但是电耗过高,生产中产生的氟化物对环境的污染严重;粉末冶金虽然从根本上解决了碳化物偏析和粗大的问题,但其工艺复杂,成本过高,应用受到限制。而半固态连铸工艺既解决了初始碳化物偏析和粗大问题,又克服了电渣重熔中电耗高、环境污染以及粉末冶金成本高的缺点,是值得重视的一个新工艺。     

超声冲击细化22SiMn2TiB超高强钢焊接接头晶粒研究

晶粒细化有助于提高焊接接头性能。应用超声冲击装置对母材为22SiMn2TiB、焊接材料为Cr20Ni10Mn6的异种钢焊接接头进行冲击强化试验,研究了冲击区域金属的塑性变形情况。用扫描电镜观测冲击层断面区,可看到冲击塑性变形层达到150μm,其中晶粒细化区超过50μm;用X-Ray衍射仪测试冲击层细晶衍射线宽化现象,并计算冲击层细化晶粒尺寸,计算结果表明母材冲击层平均晶粒尺寸为63nm,焊缝金属冲击层平均晶粒尺寸为82nm。研究表明,超声冲击时冲击针的高频大能量输入,引起冲击层金属晶格畸变,位错增殖、运动、重排,是晶粒细化的主要原因。     

大蒜多糖提取液的澄清条件研究

为了获得澄清透明的大蒜多糖提取液用以生产大蒜多糖,采用不同的pH、不同的澄清剂及其用量等条件处理大蒜多糖提取液。结果表明:在pH为4的条件下,澄清时单宁和明胶用量为0.04%和0.02%,或膨润土、明胶和明矾用量比为0.1%0∶.01%0∶.015%2种方法,均获得了澄清透明的大蒜多糖溶液。该结果可用于大蒜多糖的工业化生产。     

微钙钢中第二相粒子细化晶粒效果的研究

通过热处理试验、热模拟试验以及埋弧焊试验,研究了微钙钢中的第二相粒子对奥氏体晶粒的细化效果。结果表明:在热处理条件下微钙钢的奥氏体晶粒尺寸随保温时间的延长而增大,但增大幅度较小;热模拟条件下微钙钢当t8/5=80 s时,模拟CGHAZ的奥氏体晶粒尺寸为80μm,t8/5=200 s时约为110μm,细化效果明显;焊接条件下,未加钙钢CGHAZ的晶粒平均尺寸约为400μm,微钙钢CGHAZ平均晶粒尺寸约为120μm,细化效果显著。微钙钢中的第二相粒子能够有效地细化奥氏体晶粒。     

2~4p阶群的类型(Ⅰ)——p为奇素数,且Sylow子群正规

本文用群论的理论和方法研究2~4p阶群的分类。给出了Sylow子群正规时所有2~4p群的定义关系。     

Parvalbumin in fish skin-derived gelatin: is there a risk for fish allergic consumers?

The major allergen parvalbumin was purified from cod muscle tissues, and polyclonal antibodies were raised towards it. The antibodies were tested for specificity and an enzyme-linked immunosorbent assay (ELISA) was developed using these antibodies. The ELISA was applied to measure parvalbumin in cod skin, the starting material for fish gelatin made from deep sea, wild fish. The ELISA was sufficiently sensitive (LLOQ?=?0.8?ng?ml^?1 in extracts, corresponding to 0.02?µg of parvalbumin per g of tissue), and did not cross-react with common food constituents. Fish gelatin, wine and beer, matrices for the potential use of this ELISA, did not cause disturbance of the assay performance. The data show that the parvalbumin content in cod muscle tissue is 6.25?mg?g^?1, while the skins contained considerably less, 0.4?mg?g^?1. Washing of the skins, a common industrial procedure during the manufacturing of fish gelatin, reduced the level of parvalbumin about 1000-fold to 0.5?µg?g^?1, or 0.5?ppm. From 95 commercial lots of fish gelatin it is shown that 73 are below 0.02?µg?g^?1 parvalbumin. From the other 22 lots, the one with the highest concentration contained 0.15?µg?g^?1 of parvalbumin. These levels are generally assumed to be safe for fish-allergic individuals.     

Effects of Fining Agents on Antioxidant Capacity of Red Wines

The antioxidant capacity of wine depends not only on the grape variety but also on the wine processing steps. The aim of this study was to determine the effects of different fining agents, used at different concentrations, on the antioxidant status of fined wines. The results demonstrated that the use of a combination of gelatin and Kieselsol led to the highest total phenol value (3,491 mg/L GAE) and antioxidant activities (29%) among the tested fining agents. Wines were mostly negatively affected by the use of egg white as an agent and led to the lowest value of total phenol (3,038 mg/L GAE) and the lowest rate of antioxidant activity (26%). Significant differences (p<0.05) were determined between gelatin, egg white, and the control groups. The results of the grouping of analyzed parameters in n‐dimensional space, with different fining agents at different concentrations, demonstrated the importance of a low concentration of fining agents for high antioxidant activity and total phenols.     

球磨过程中的涂层形成与粉末细化

研究了Cr粉、Al粉、Cu粉、Cr20Al80粉末球磨过程中粉末粒度尺寸的变化以及磨球表面涂层的形成规律,结果发现,磨球表面涂层的形成与粉末细化之间有一定的关系.球磨初期,磨球涂层厚度迅速增加,随后逐渐趋于稳定.Cu粉末在球磨过程中未在磨球表面形成涂层.金属粉末球磨至24h后,随球磨时间增加,磨球涂层厚度几乎不再变化;除Al粉末外,其余金属粉末的细化速率降低.磨球塑性好易形成厚涂层,粉末脆性大容易细化.     

黄河中游干流泥沙组成规律

本文利用系统、 颗粒级配资料，详细分析了黄河中游主要控制站长时期泥沙组成和泥沙粒径的变化，认为近期黄河中游有来沙细化的现象，但这是由于来沙量的减少造成的，泥沙组成规律并未发生明显的趋势性变化。