不同硫化体系对钢丝编织液压胶管外胶性能的影响

研究了T1681与硫黄并用硫化体系和FSH与KSH并用硫化体系对钢丝编织液压胶管外胶(氯化聚乙烯,简称CM)的物理机械性能、耐磨性和热空气老化性能的影响。结果表明:T1681与硫黄并用硫化体系硫化胶的扯断伸长率、硬度、撕裂强度均高于FSH与KSH并用硫化体系硫化胶;T1681与硫黄并用硫化体系硫化胶的DIN磨耗量小于FSH与KSH并用硫化体系硫化胶的DIN磨耗量;T1681与硫黄并用硫化体系硫化胶热稳定性较FSH与KSH并用硫化体系硫化胶热稳定性稍好。     

氯蜡70的生产工艺及发展

本文介绍了氯蜡－７０的反应机理和生产工艺，并介绍了国外氯蜡－７０先进的生产工艺技术。     

直接氯化法合成对硝基氯化苄

介绍了以对硝基甲苯和氯气为原料 ,在催化剂存在下合成对硝基氯化苄的方法 ,考察了催化剂种类、反应温度、溶剂配比等因素对反应的影响 ,优化的反应条件为 :对硝基甲苯用量 1 3 7g,对硝基甲苯 /邻二氯苯 (摩尔比 ) =1∶ 0 .6,w (偶氮二异丁腈 ) =0 .6% ,反应时间 3 h,反应温度 1 60℃ ,产物单程收率大于 65 % ;将反应混合物中未反应的原料分离后 ,以无水乙醇为溶剂结晶纯化 ,物料 /溶剂 (摩尔比 ) =1∶ 1 .5时晶体含量在 99.0 %以上 ,结晶收率达 67     

氯化聚氯乙烯生产与应用

介绍氯化聚氯乙烯生产方法、应用与市场，并对氯化聚氯乙烯的发展前景进行评述与展望。     

Corrosion Inhibition Mechanism with Spilt Cell Technique of Rare Earth Metal on LC4 Al Alloy

A new method of studying the corrosion inhibition mechanism of rare earth metal(REM) on LC4 Al alloy with the spilt cell technique was studied. The principle and experimental method of the spilt cell technique were analyzed. By measuring the change of net-electric current between the two electrodes caused by the change of the amount of oxygen in the solution and the addition of CeCl₃, the influence of corrosive performance of CeCl₃ on LC4 super-power aluminum alloy in the 0.1 mol·L⁻¹ NaCl solution was investigated. Meanwhile, the conditional changes of pH values, CeCl₃ solution, additire and time of performance were also studied. Finally, the features of electrode surface were revealed by using SEM and X-ray energy-dispersive spectrometry (EDS). By combining these with other electric chemical techniques, such as potential-time curve, polarization curve et al.     

Effect of Rare Earth Element Cerium on Mechanical Properties and Morphology of TiN Coating Prepared by Arc Ion Plating

TiN coatings were deposited on polished substrates of W18Cr4V high speed steel by means of vacuum arc ion plating. The effect of cerium on adhesion between TiN coating and substrate was studied. The microstructures and composition of TiN coatings were also investigated by means of scanning electron microscope (SEM), Auger electron spectroscopy (AES), and X-ray diffraction (XRD) technique. It was found that cerium is an effective modifying agent and the addition of suitable amount of cerium to TiN coatings can produce relatively excellent properties such as micro-hardness, wear resistance, oxidation resistance and porosity. The experimental results show that the added cerium in TiN coatings makesa contribution to form the preferred direction along with a (111 ) or (222) close packed face, which may be one of the reasons that improves some properties mentioned above.     

高料层操作时烧结矿FeO含量的降低

最近正在Ｋｕｒｅ１号烧结机上进行厚料层作业。在厚料层作业开始之前，我们进行了不同料层高度下的烧结杯试验，来研究料层高度对烧结的影响。     

2,4-二氯氟苯的合成

论述了2，4－二氯氟苯合成的新方法。以对氯硝基苯为起站原料，经氟化反应、硝化反应及氯化反应制得2，4-二氯氟苯，总收率达59．0％。本合成路线工艺简单、操作安全、原料易得、成本低廉，适合于工业化生产。