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1.
Easy and hard magnetization curves of Nd_2Co_(14)B compound have been measured withextracting-sample-magnetometer(μ_0H_(max)=6T)at 10~300 K.Magnetic anisotropy constants K_1 and K_2have been determined by fitting the hard magnetization curves,in which only K_1 ,K_2 and misalignment anglehave been taken as fitting parameters.The values of K_1 and K_2 at 4.2 K were derived by extrapolation.Anisotropy coefficients,x_2~° and x_4~°were derived from the anisotropy constants.The anisotropy constant K_2increases rapidly with increasing temperature when TT_(sr).The temperature depen-dence of the magnetic anisotropy coefficient x_2~° was fitted with the formula.The anisotropy coefficients x_2~°can be well described by the tenth-power law from 4.2 K to T_(sr)and by the sixth-power law from T_(sr_ to 300 K. 相似文献
2.
Homogeneous and nano-sized BPNT [(Ba1-xPbx)Nd2Ti5O14] powders were prepared under various hydrothermal conditions. Crystallinity and homogeneity of the synthetic powders were
investigated. The microwave dielectric properties of the filters prepared with hydrothermal powders were compared with those
of the filters prepared with conventional powders. The microwave dielectric properties of the filter prepared with the hydrothermal
powders were also better than those of the filter manufactured with the conventional powders. The dielectric constant, quality
constant and temperature coefficient of resonance frequency of hydrothermally prepared filter under optimum condition and
measured at 3.5 GHz around were about 93, 6067 and 0 ppm/°C, respectively. 相似文献
3.
Fabian SobotkaThomas Kneib 《Computational statistics & data analysis》2012,56(4):755-767
Quantile regression has emerged as one of the standard tools for regression analysis that enables a proper assessment of the complete conditional distribution of responses even in the presence of heteroscedastic errors. Quantile regression estimates are obtained by minimising an asymmetrically weighted sum of absolute deviations from the regression line, a decision theoretic formulation of the estimation problem that avoids a full specification of the error term distribution. Recent advances in mean regression have concentrated on making the regression structure more flexible by including nonlinear effects of continuous covariates, random effects or spatial effects. These extensions often rely on penalised least squares or penalised likelihood estimation with quadratic penalties and may therefore be difficult to combine with the linear programming approaches often considered in quantile regression. As a consequence, geoadditive expectile regression based on minimising an asymmetrically weighted sum of squared residuals is introduced. Different estimation procedures are presented including least asymmetrically weighted squares, boosting and restricted expectile regression. The properties of these procedures are investigated in a simulation study and an analysis on rental fees in Munich is provided where the geoadditive specification allows for an analysis of nonlinear effects of the size of flats or the year of construction and the spatial distribution of rents simultaneously. 相似文献
4.
5.
The compound effect of Nd2Fe14B/Fe3B-Ferrite bonded magnets was studied.The result shows that the value ofβjHC obviously decreases with the ferrite content increasing.In addition, a functional relation between magnetic properties and ferrite content was clearly revealed by the physical relation in the magnetic powders. 相似文献
6.
基于湿法氧化法对核电厂产生的放射性废树脂进行前处理,建立了树脂中3H和14C的测量方法,分析了影响方法回收率的因素,并对国内某核电厂废树脂中的3H和14C进行了测量。结果表明,H2O2浓度对方法回收率影响最大,在最优的氧化条件下,方法回收率达96.8%;3H和14C最小可探测比活度分别为41 Bq/g和1.3 Bq/g;14C测量结果与《生物样品中14C的分析方法 氧弹燃烧法》(GB/T 37865-2019)的测量结果相比,无显著性差异,14C测量精密度为10.2%。对国内某核电厂废树脂进行测量,3H和14C的平均比活度分别为(6 134 ±640) Bq/g和(2 724±147) Bq/g。 相似文献
7.
8.
一种新型钛合金半固态锻造后的断裂行为研究 总被引:1,自引:0,他引:1
以新型钛合金Ti14为对象,对比研究常规和半固态锻造合金经不同时间热暴露后的室温拉伸性能,探讨热暴露后的断裂行为及其断裂机制。结果表明,半固态锻造试样热暴露后的强度均明显高于常规锻造试样,而塑性略低于常规锻造试样。常规锻造试样宏观断口三要素清晰可见,断口由细小的韧窝组成,韧窝密度较大;半固态锻造试样纤维区模糊,剪切唇区较大,断口为韧窝和解理的混合型断口,并伴随少量二次裂纹的出现。析出相的尺寸、形态、分布的差异是导致两种锻造态合金热暴露后断裂机制改变的主要原因。 相似文献
9.
BaO-Nd2O3-TiO2系富钛区含La或Sm的陶瓷,XRD、SEM显微结构分析表明,其主晶相为R(R=La或Sm)取代Nd固溶体BaNd2-yRyTi5O14和BaNd2-yRyTi4O12,均属斜方晶系,并存在少量的次晶相R2Ti2O7、BaTi4O9、Ba2Ti9O20等。富钛区BaNd2Ti4+xO12+2x(x=0~1.400)组分和含La或Sm的BaNd2-yRyTi5O14组分所组成的瓷料,介质损耗显著地降低,介电常数和电容温度系数遵从李赫涅德凯对数混合定律。 相似文献
10.
Maurus Biedermann Konrad Grob Carlo Mariani Joachim P. Schmidt 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1996,202(3):199-204
Adulteration of expensive edible oils, such as olive oil, often involves desterolized oils in order to render the adulteration undetectable. Sunflower oil contains characteristic 7-sterols, which are readily removed upon strong bleaching. It is shown that these 7-sterols do not primarily dehydrate (as do 5-sterols), but isomerize to 8(14)- and 14-sterols. These compounds can be analysed by LC on silica gel or GC on capillary columns with stationary phases of intermediate to high polarity. 相似文献