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1.
FTIR spectroscopy was applied to study the initial steps of ethylene polymerization on reduced chromia-silica (0.5 wt% Cr/SiO2). To decrease the speed of the reaction small doses of gas were introduced to the catalyst in each run and C2D4 was used to confirm band assignments. At the initial steps of the reaction only ethylene molecules coordinated to probably Cr
A
2+
cations were observed. The concentration of such complexes was estimated to be about 50% of the total amount of Cr atoms in the sample. The FTIR spectrum of the polymer formed at the initial doses of C2H4 (when [C2H4] 74460264254120/xxlarge8776.gif" alt="ap" align="MIDDLE" BORDER="0"> [Cr]) was found to be slightly different from that formed after excess ethylene was introduced onto the catalyst ([C2H4] > [Cr]). 相似文献
2.
3.
Influence of expandable graphite on fire resistance and water resistance of flame-retardant coatings 总被引:1,自引:0,他引:1
Expandable graphite (EG) coating and ammonium polyphosphate-pentaerythritol-melamine (APP-PER-MEL) coating were prepared. Thermal degradation and char formation of the coatings were investigated by differential thermal analysis (DTA), thermogravimetry (TG), X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The results have shown that the anti-oxidation and fire-resistant properties of expandable graphite coating containing EG with size of 74 μm are better than those of APP-PER-MEL coating. The static immersion test was applied to study water resistance of the coatings, and the fire protection test and mechanical test were used to analyse heat insulation and mechanical properties of coatings before and after water immersion. The fire-resistant and mechanical properties of APP-PER-MEL coating were severely damaged by water immersion, whereas EG coating containing 8.5% EG with size of 74 μm could retain the good fire resistance even after 500 h water immersion. 相似文献
4.
NC74-1型氨合成催化剂的升温还原及应用 总被引:1,自引:0,他引:1
介绍了NC74-1氨合成催化剂在山东华鲁恒升化工股份有限公司大氮肥氨合成的装填、升温还原及使用情况。 相似文献
5.
针对目前广泛应用的DALLAS公司的数字温度传感器DS18B20,分析了多点测温电路的缺陷,介绍了一个实现多点测温模块的实现方法。使用DS18B20,配合总线驱动双向三态门74LS245的电路成功实现了多点测温,并给出了编写模块驱动程序的流程,最后说明了多点测温模块适用的场合。 相似文献
6.
摘要:为了适应嵌入式设备外设的多样性,本文以特殊矩阵键盘为例,设计了一套完整的驱动控制模块。硬件电路设计采用外扩3片SN74HCl64芯片的方式,节省了GPIO引脚的使用,大大提高了利用效率。同时,在此基础上引出了Linux内核中input子系统的特性和工作机制,呈现了较为完整的输入事件由内核空间传递到用户空间进程的过程。实验结果表明,设计的驱动模块具有良好的实时性和准确性。 相似文献
7.
Takeshi Emura 《Computational statistics & data analysis》2010,54(12):3033-3043
A goodness-of-fit testing procedure for Archimedean copula (AC) models is developed based on right-censored data. The proposed approach extends an existing method, which is suitable for the Clayton model, to general AC models. Asymptotic properties of the proposed test statistics under the true model assumption are derived. Simulation analysis shows that the proposed test has reasonable performance. Finally, two real data examples are analyzed for illustrative purposes. 相似文献
8.
Jens MaßbergJan Schneider 《Theoretical computer science》2011,412(50):6948-6958
We formulate a generalization of the NP-complete rectangle packing problem by parameterizing it in terms of packing density, the ratio of rectangle areas, and the aspect ratio of individual rectangles. Then we show that almost all restrictions of this problem remain NP-complete and identify some cases where the answer to the decision problem can be found in constant time. 相似文献
9.
Guochang Wang 《Computational statistics & data analysis》2012,56(3):587-601
Functional linear regression has been widely used to model the relationship between a scalar response and functional predictors. If the original data do not satisfy the linear assumption, an intuitive solution is to perform some transformation such that transformed data will be linearly related. The problem of finding such transformations has been rather neglected in the development of functional data analysis tools. In this paper, we consider transformation on the response variable in functional linear regression and propose a nonparametric transformation model in which we use spline functions to construct the transformation function. The functional regression coefficients are then estimated by an innovative procedure called mixed data canonical correlation analysis (MDCCA). MDCCA is analogous to the canonical correlation analysis between two multivariate samples, but is between a multivariate sample and a set of functional data. Here, we apply the MDCCA to the projection of the transformation function on the B-spline space and the functional predictors. We then show that our estimates agree with the regularized functional least squares estimate for the transformation model subject to a scale multiplication. The dimension of the space of spline transformations can be determined by a model selection principle. Typically, a very small number of B-spline knots is needed. Real and simulation data examples are further presented to demonstrate the value of this approach. 相似文献
10.
多位LED串行显示电路设计与应用 总被引:2,自引:0,他引:2
74HC595A芯片具有串行输入、并行输出功能,利用该集成电路可设计多位LED(发光二极管)串行显示电路。文中介绍了利用该芯片设计的12位LED串行显示电路,详细说明了该电路的工作原理及编程思路,并给出了参考程序。该电路只占用单片机3根口线,较并行显示方式极大地节省了系统资源,已在实际系统中得到应用。 相似文献