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1.
Monomers and their polymers containing 3-arylcarbazolyl electrophores have been synthesized by the multi-step synthetic route. The materials were characterized by thermo-gravimetric analysis, differential scanning calorimetry and electron photoemission technique. The polymers represent materials of high thermal stability having initial thermal degradation temperatures in the range of 331–411 °C. The glass transition temperatures of the amorphous polymeric materials were in the rage of 148–175 °C. The electron photoemission spectra of thin layers of monomers showed ionization potentials in the range of 5.6–5.65 eV. Hole-transporting properties of the polymers were tested in the structures of organic light emitting diodes with Alq3 as the green emitter. The device containing hole-transporting layers of polyether with 3-naphthylcarbazolyl groups exhibited the best overall performance with a maximum current efficiency of 3.3 cd/A and maximum brightness of about 1000 cd/m2. 相似文献
2.
The Er3+ doped oxyfluorogermanate glasses, with a composition containing Na element, were synthesized by the conventional melting–quenching technique. When Na element was introduced into the composition of oxyfluorogermanate glass, the crystals behavior was investigated in details. Depending on the annealing procedure supplied, thermal annealing of precursor glasses in the system GeO2/BaF2/AlF3/Na2O/NaF/ZnO/GdF3/ErF3 led to the precipitation of different crystal phase nanocrystals. It was confirmed the nanocrystals in GC600 is orthorhombic NaBaAlF6 which led to enhance obviously in the UC luminescence of Er3+. However, the nanocrystals in G585 led to decrease in the UC luminescence, which indicated few Er ions enter into the lattice of this nanocrystal phase. The reason of the decrease in UC emission intensity of GC585 was analyzed. 相似文献
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4.
Si3N4 ceramic was jointed to itself using a filler alloy of Cu76.5Pd8.5Ti15, and the mechanical properties of the jointwere measured and analyzed. By using a filler alloy of Cu76.5Pd8.5Ti15, the SisN4/SisN4 joints were obtained bybrazing at 1373~1473 K f 相似文献
5.
在概括了自蔓延高温合成陶瓷内衬钢管的制备原理基础上,从降低陶瓷层孔隙率,减少陶瓷层裂纹和提高陶瓷层结合强度等方面,论述了提高自蔓延高温合成陶瓷内衬钢管性能的措施,对自蔓延高温合成陶瓷内衬钢管的应用现状及展望进行了评述。 相似文献
6.
化学镀非晶态Ni—B合金的研究 总被引:1,自引:0,他引:1
本文通过化学镀方法在铜和钢上沉积非晶态Ni-B合金。着重讨论了还原剂浓度、络合剂浓度对化学镀沉积速率的影响;分析了它的耐蚀原因和其显微硬度随退火温度的变化情况并就其应用和发展略作说明。 相似文献
7.
A systematic investigation of the magnetic and transport properties of Ti doped La0.67Ca0.33MnO3 was reported. The Ti substitution for Mn ions results in a reduction in ferromagnetism and conductivity. The metal-insulator transition temperature is close to Curie temperature which decreases from 274 to 82 K as x increases from 0 to 0.17. The most important effect of Ti doping is to introduce spin clusters in the samples due to the distortion of local lattice and the inhomogeneous magnetic structure induced primarily by the random distribution of Mn ions. A maximum magnetoresistance ratio as large as 90% in 1 T at 122 K was obtained for the sample with x =0. 055, which is four times larger than that obtained for LCMO sample at 272 K. There is a remarkable field-history dependent MR in the cooling process for the doped samples while such phenomenon disappears in the warming run. The resistivity follows well the variable range hopping behavior in paramagnetic state. Both the size effect and spin dependent hopping of carriers between the spin clusters should be considered in this system. 相似文献
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9.
现代民间青花与现代陶艺 总被引:1,自引:0,他引:1
现代民间青花与现代陶艺都是火与土的艺术,都具有粗犷,质朴、自然、大方的共同艺术特点。前者在传统民间青花的基础上,汲取了现代陶瓷科技成就和现代文化艺术成果,而发展成为富有现代艺术意蕴和现代审判内涵的新型民间青花艺术;而后者则是从传统陶艺延伸、扩展、蜕变为纯粹艺术表达和具有独特审判内涵的一门现代艺术。 相似文献
10.
采用X射线衍射分析技术,研究了脉冲化学镀非晶态Ni-P合金的原子分布和函数,得出其短程有序原子集团的尺度为0.754nm,约为熔体激冷法获得的非晶态Ni-P合金短程有序畴的1/2。并利用脉冲化学沉积非晶态合金的微机制择这一结果进行了解释。 相似文献