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1.
The gravity flow characteristics of pharmaceutically important granules were studied in a cylindrical hopper with attachable orifice disk at the bottom. Results indicate that materials property and orifice diameter play key role in determining mass flow rate while keeping environmental condition (temperature) at fixed range. A new dimensionally analyzed equation was developed to predict gravity flow of pharmaceutically important granules. The developed correlation agreed well with the experimental data. Calcium gluconate and lactose were used for preparing granules. Generally, glidant/lubricant materials are added to pharmaceutical granules during tablet manufacturing process, in order to improve physical property of granular material. Hence, the effect of glidant/lubricant on mass flow of granules through hopper was also studied. Magnesium stearate (1.5%) was added as glidant before granulation. 相似文献
2.
Hironori Minoshima 《Chemical engineering science》2006,61(6):2101-2102
Previously developed model for spray drying of slurry droplets with high solid content (Liang, 2001) was revised to describe correctly a boundary condition on the outer surface of droplet on basis of the rate of liquid evaporation. 相似文献
3.
C. A. Biggs C. Sanders A. C. Scott A. W. Willemse A. C. Hoffman T. Instone A. D. Salman M. J. Hounslow 《Powder Technology》2003,130(1-3):162-168
It is possible to link granulation rates to granule properties. The linkage is by multiple dimension population balance equations that, by means of simplifying assumptions, can be reduced to multiple one-dimensional (1-D) population balance equations (PBEs). Using simple physically based models, this paper demonstrates how multiple one-dimensional population balance equations can describe the results of high-shear granulation experiments of two different materials, calcium carbonate and lactose. Good agreement between experimental and simulated results was achieved enabling the granulation rates to be defined by two model parameters: the critical binder volume fraction and the aggregation rate constant. The modelling framework presented in this paper also provides a basis for the kinetic analysis of granulation experiments so that with further work, it is possible to determine the effect of process conditions and material properties on the model parameters. 相似文献
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在分级系统中,分级轮对于物料的分散、分级起着非常重要的作用。通过分析气体在分级轮中所受的作用力,推导出分级粒径公式,并得出分级轮的风量、转速与分级粒度及分级精度的关系。 相似文献
7.
介绍了物料在料仓中的流动状态和掺混机理。通过测量物料的掺混数据,结合影像资料,分析出大颗粒物料掺混中离析的另一原因是质量小的物体在碰撞后的速度大于质量大的物体;掺混时间(循环次数)要根据物料情况而定,时间太长有可能发生物料离析;料仓进料口距料面的距离要尽量小,以降低碰撞的初速度。 相似文献
8.
There have been significant advances in the understanding of wet granulation processes. Foam granulation is the latest development and an emerging area of interest for pharmaceutical manufacturing.Single foam penetration experiments were carried out on static powder beds, followed by short-nucleation experiments (where nuclei are formed by a nucleation-only mechanism) and full foam granulation experiments (where nucleation, growth and breakage are occurring simultaneously). All experiments were performed with lactose monohydrate powder using a 5 L high shear mixer–granulator. The foam penetration/dispersion behaviour was examined and the granule size distributions were investigated as a function of foam quality (83–97% FQ), impeller speed (105–515 rpm) and wet massing period (0–4 min).Nucleation in foam granulation is postulated to undergo either “foam drainage” or “mechanical dispersion” controlled mechanisms. For “foam drainage” mechanism, the foam penetrates the powder bed to form coarse and broad granule size distributions. For “mechanical dispersion” mechanism, the wetting and nucleation conditions are governed by the powder mixing conditions and similar granule size distributions are produced. Regardless of the mechanism, the initial wetting and nucleation behaviour controls the initial nuclei size distribution, and this initial distribution is retained in the final granule size distribution. This work demonstrated the critical importance of the nucleation and binder distribution in determining the granule size distributions for foam granulation process. 相似文献
9.
Role of mass transfer in overall substrate removal rate in a sequential aerobic sludge blanket reactor treating a non-inhibitory substrate 总被引:1,自引:0,他引:1
A laboratory study was undertaken to explore the role of mass transfer in overall substrate removal rate and the subsequent kinetic behavior in a glucose-fed sequential aerobic sludge blanket (SASB) reactor. At the organic loading rates (OLRs) of 2-8 kg chemical oxygen demand (COD)/m3-d, the SASB reactor removed over 98% of COD from wastewater. With an increase in OLR, the average granule diameter (dp = 1.1-1.9 mm) and the specific oxygen utilization rate increased; whereas biomass density of granules and solids retention time decreased (13-32 d). The intrinsic and apparent kinetic parameters were evaluated using break-up and intact granules, respectively. The calculated COD removal efficiencies using the kinetic model (incorporating intrinsic kinetics) and empirical model (incorporating apparent kinetics) agreed well with the experimental results, implying that both models can properly describe the overall substrate removal rate in the SASB reactor. By applying the validated kinetic model, the calculated mass transfer parameter values and the simulated substrate concentration profiles in the granule showed that the overall substrate removal rate is intra-granular diffusion controlled. By varying different dp within a range of 0.1-3.5 mm, the simulated COD removal efficiencies disclosed that the optimal granular size could be no greater than 2.5 mm. 相似文献
10.
Growth and breakdown mechanisms in granulation processes may involve collisions between soft plastically deforming agglomerates. It has been established previously that the flow stress in such collisions increases with the strain rate, which is dependent on the impact velocity and the size of the agglomerates. In the current paper, a scaling model is described that is based on a continuum constitutive relationship and formulated in terms of accessible experimental parameters. It is an extension of an existing contact mechanics model for elastoplastic nonadhesive collisions and therefore limited to deformations in which the contact radius is less than about 40% of the agglomerate radius. In addition, it is assumed that the elastic strains are small compared to the maximum value. Finite element simulations were carried out for a range of impact velocities and material parameters associated with an elastoviscoplastic constitutive relationship of the type used in the scaling model. The results were employed to validate the scaling model. Within the specified limits of applicability, it was found that the coefficient of restitution, contact area, loading and unloading curves and also the time evolution of the compressive displacement could be calculated with relatively high accuracy. Moreover, it was found that for a viscoplastic material the rate of decrease of the coefficient of restitution with increasing impact velocity is greater than for plastic deformation. The model should prove useful in understanding collision processes in granulation systems, particularly those occurring at relatively high impact velocities when the main energy dissipation process arises from viscoplastic deformation. Under this circumstance, the influence of adhesion is negligible and coalescence may be taken to occur when the coefficient of restitution is small. 相似文献