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1.
《Ceramics International》2020,46(15):24213-24224
We report an experimental approach, designed based on the recent findings that domain switching in ferroelectric ceramics can be separated into three regimes during antiparallel electric field loading, to investigate the influence of domain switching process on the electrical fatigue behavior of ferroelectrics. Uniaxial compressive stress (−2 MPã -100 MPa) and thermal loading (20 °C–150 °C) were used to tune the domain switching process. Under the same loading condition, the bipolar electrical fatigue behavior of soft lead zirconate titanate ceramics was systematically characterized. The amplitude and frequency of the applied electric field are 2 kV/mm and 10 Hz, respectively. By analyzing the evolution of the domain switching process, combined with the measured polarization and strain response, as well as the cracks observed on the surface of the specimen, it is found that the fatigue of ferroelectric ceramics was mainly related to the domain switching process near the coercive electric field: the regime 2 defined in this paper. The underlying mechanism was further discussed by considering the interplay between the domain switching process with the main factors affecting the electrical fatigue of ferroelectrics, namely defect redistribution, charge carrier injection, and crack initiation.  相似文献   
2.
改性双马来酰亚胺的研究   总被引:2,自引:0,他引:2  
本文研究了双马来酰亚胺与烯丙基化合物形成的改性树脂体系的固化和热性能,讨论了单体配比、增韧剂、催化剂对性能的影响。  相似文献   
3.
Recent developments in rubber-toughened structural acrylic adhesives now offer sheet steel fabricators the opportunity to replace conventional metal fastening techniques such as spot welding with lower cost, durable, more versatile structural adhesive bonding. These developments, in particular much improved ability to bond oily/waxy surfaces common to the motor car industry and improved retention of fracture toughness after exposure to paint stoving temperatures, are discussed in this paper.  相似文献   
4.
Carboxyl‐terminated butadiene‐acrylonitrile rubber (CTBN) has often been used to improve the toughness of cyanate ester (CE) resin while sacrificing modulus and thermostability. In this paper, the addition of the appropriate amount of epoxy resin (EP) to the CE/CTBN system is shown to not only increase the modulus and thermostability of the blend, but also improve the toughness. The values of impact strength showed a maximum for the CE/CTBN/EP 100/5/5 blend. The temperature of 10 % weight loss (T10) improves from 376 °C for CE/CTBN 100/5 to 407 °C for the CE/CTBN/EP 100/5/2.5 blend. It is proposed that addition of the appropriate amount of EP can decrease the mobility and increase the stability of CTBN via the reaction between the terminal carboxyl group of CTBN and the hydroxyl group of EP. But a very high EP concentration will decrease the crosslinking density of CE, consequently reducing the mechanical properties and thermostability of the blends. Copyright © 2004 Society of Chemical Industry  相似文献   
5.
Some approximate solutions for predicting the stress intensity factor of a short crack penetrating an inclusion of arbitrary shape have been developed under mode I and mode II loading conditions. The derivation of the fundamental formula is based on the transformation toughening theory. The transformation strains in the inclusion are induced by the crack-tip field and remotely applied stresses, and approximately evaluated by the Eshelby equivalent inclusion theory. As validated by detailed finite element (FE) analyses, the developed solutions have good accuracy for different inclusion shape and for a wide range of modulus ratio between inclusion and matrix material.  相似文献   
6.
研究了稳定ZrO_2和部份稳定ZrO_2对β″-Al_2O_3陶瓷的强化和韧化作用,观察了不同种类、不同含量的ZrO_2对β″-Al_2O_3陶瓷的显微结构、力学性能和电导率的影响,探讨了β″-Al_2O_3的韧化机理。  相似文献   
7.
层状Ti3SiC2陶瓷的组织结构及力学性能   总被引:19,自引:0,他引:19       下载免费PDF全文
利用热压烧结TiH2,Si和C粉获得了致密度大于98%的层状Ti3SiC2陶瓷。利用压痕法,在不同的载荷下测定了材料的维氏硬度, 发现其硬度值随载荷的增加而降低,在最大载荷30kg时,硬度值为4GPa。压痕对角线没有发现径向裂纹的出现。 这归因于多重能量吸收机制——颗粒的层裂、裂纹的扩展、颗粒的变形等。利用三点弯曲法和单边切口梁法测定了材料的强度和韧性分别为270MPa和6.8MPa·m1/2。Ti3SiC2材料的断口表现出明显的层状性质,大颗粒易于发生层裂和穿晶断裂,小颗粒易被拔出。当裂纹沿平行于Ti3SiC2基面的方向扩展造成颗粒的层裂,当裂纹沿垂直于基面的方向扩展时,裂纹穿过颗粒的同时,在颗粒内部发生偏转,使裂纹的扩展路径增加。裂纹的扩展路径类似人们根据仿生结构设计的层状复合材料。裂纹在颗粒内的多次偏转、裂纹钉扎以及颗粒的层裂和拔出等是材料韧性提高的主要原因。此外,在室温下得到的荷载-位移曲线,说明Ti3SiC2材料不象其它陶瓷材料的脆性断裂,而是具有金属一样的塑性。  相似文献   
8.
乙烯-1-辛烯共聚物增韧应用研究   总被引:3,自引:0,他引:3  
介绍了聚烯烃系弹性体(POE)的特点及其在PP增韧改性中的应用,同时还报道了马来酸酐接枝的POE在极性聚合物复合体系中的应用研究。  相似文献   
9.
Si3N4陶瓷材料由于具有很好的高温性能及高的力学性能,而被广泛地用于结构陶瓷,如切削刀具等。然而,因为其对缺陷很敏感,故易受灾难性的失效。人们发展了多种Si3N4增韧陶瓷,其中自增韧由于一些优异的性能越来越受到人们的重视。在此文中,着重介绍了影响Si3N4陶瓷长颗粒(柱状晶)晶粒生成的因素,并介绍了国内外对长颗粒Si3N4晶的控制研究。  相似文献   
10.
The equivalent inclusion method (EIM) assuming linear elasticity is used to calculate the mechanical interactions between spherical rubber particles in an amorphous matrix, as in a rubber toughened polymer. The influences of the various calculation parameters are examined and it is shown that the method can provide reliable results with regard to the level of hydrostatic stress in the particles. Damage of the material is simulated by replacing the most stressed particles by voids. Numerical simulations for several hundreds of interacting particles give information on the kinetics and spatial organisation of the damage. It appears that, as the volume fraction of particles increases from 10 to 20%, the spatial configuration of the damage evolves from a localised to a diffuse mode. These results are discussed in relation to the efficiency of rubber toughening.  相似文献   
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