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排序方式: 共有100条查询结果,搜索用时 15 毫秒
1.
文章采用氢氧化钠碱熔试样,经硫酸中和后,在1+1盐酸介质中蒸馏分离锗,使大部分干扰元素经蒸馏分离,并在1+1盐酸介质中用碘酸钾容量法滴定锗。该法滴定终点明显,准确率高。标准回收率为95.52%~105.78%,变异系数为3.18%~4.42%。适用于锗渣中高含量的锗的测定分析。 相似文献
2.
水溶液晶体的空间生长及其地基模拟实验 总被引:1,自引:0,他引:1
空间水溶液晶体生长是通过搭载人造卫星、宇宙飞船和空间站等飞行器,在微重力条件下从水溶液中进行晶体生长实验.许多透明单晶体,诸如:KDP(磷酸二氢钾,potassium dihydrogen phosphate)、ADP(磷酸二氢铵,ammonium dihydrogen phosphate)、TGS(硫酸三甘氨酸,triglycine sulfae)、沸石和α-碘酸锂(α-LiIO3)等无机非线性光学晶体,尿素等有机非线性光学晶体以及蛋白质等生物晶体,均可采用水溶液法生长.美国、前苏联、西欧和日本等国在从事空间材料科学研究的高科技发展计划中,均把水溶液晶体生长作为一项重要项目.由于水溶液晶体生长方法的研究在地面上已有丰富的基础,而且具有温度低,能耗小,可实现原位实时观察等优点,所以,它是探索空间晶体生长原理和方法、研究晶体生长微重力效应的重要材料制备技术.由于空间晶体生长受搭载条件限制,空间实验的次数与地面相比是十分稀少的,为了获得空间实验的高成功率,在地面上必须建立相应的实验基地,开展深入的地基研究工作.本文将分别从空间实验和地基研究两个方面作系列介绍,包括蛋白质晶体,沸石晶体,α-LiIO3晶体的空间生长以及TGS,NaClO3(sodium chlorate,氯酸钠),Sr(NO3)2(strontium nitrate,硝酸鍶)和Ba(NO3)2(barium nitrate,硝酸钡)等晶体生长过程的原位实时观察,并展望了空间晶体生长的发展前景. 相似文献
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文章研究了锡阳极泥中锡含量的测定方法,样品通过焙烧,过氧化钠分解后,以热水浸取,过滤,使锡与铜、砷等干扰元素分离。滤液经酸化处理,于盐酸溶液中,用铝片还原,以碘酸钾滴定法完成测定。 相似文献
6.
文章建立了借助I-3对光的吸收测定碘盐中IO-3的新方法。该方法最大吸收波长为350nm,摩尔吸光系数为8.24×104L/mol·cm,碘在2μg~60μg范围内符合朗伯—比耳定律,相对标准偏差2.63%,回收率为96.69%~102.3%,方法操作简便,快速。 相似文献
7.
Grazia M. Borrelli Donatella B. M. Ficco Natale Di Fonzo & Clara Fares 《International Journal of Food Science & Technology》2006,41(6):639-645
To study the involvement of lipoxygenase (LOX) and oxidising agent potassium iodate (KIO3) in rheological behaviour of dough, mixograph and alveograph tests were performed using durum cultivars differing for quality and endogenous levels of LOX. Both tests were done in standard condition and with the adding of KIO3 and of LOX and/or its substrate, utilised singly or in different combinations. The effects of these treatments were related to change of ‐SH and S–S content in relative mixograph dough. The mixograph and alveograph responses showed that the KIO3 had an improving effect on dough tenacity and that the adding of LOX system enhanced this trend; on the contrary, the LOX system alone seemed not affect mixing stability. No relation was found between rheological responses and ‐SH and S–S content in the mixograph doughs. The results obtained could suggest that in durum wheat the main effect of LOX could be ascribable to bleaching action because of the co‐oxidation of carotenoid pigments. 相似文献
8.
本文通过对我公司碘酸钾生产现状的分析,结合清洁生产工艺的要求及现阶段碘酸钾生产工艺研究的进展,提出了合理的碘酸钾清洁生产工艺方案. 相似文献
9.
Jasmin Balmer Rahel Zulliger Stefano Roberti Volker Enzmann 《International journal of molecular sciences》2015,16(7):15086-15103
Herein, we have investigated retinal cell-death pathways in response to the retina toxin sodium iodate (NaIO3) both in vivo and in vitro. C57/BL6 mice were treated with a single intravenous injection of NaIO3 (35 mg/kg). Morphological changes in the retina post NaIO3 injection in comparison to untreated controls were assessed using electron microscopy. Cell death was determined by TdT-mediated dUTP-biotin nick end labeling (TUNEL) staining. The activation of caspases and calpain was measured using immunohistochemistry. Additionally, cytotoxicity and apoptosis in retinal pigment epithelial (RPE) cells, primary retinal cells, and the cone photoreceptor (PRC) cell line 661W were assessed in vitro after NaIO3 treatment using the ApoToxGlo™ assay. The 7-AAD/Annexin-V staining was performed and necrostatin (Nec-1) was administered to the NaIO3-treated cells to confirm the results. In vivo, degenerating RPE cells displayed a rounded shape and retracted microvilli, whereas PRCs featured apoptotic nuclei. Caspase and calpain activity was significantly upregulated in retinal sections and protein samples from NaIO3-treated animals. In vitro, NaIO3 induced necrosis in RPE cells and apoptosis in PRCs. Furthermore, Nec-1 significantly decreased NaIO3-induced RPE cell death, but had no rescue effect on treated PRCs. In summary, several different cell-death pathways are activated in retinal cells as a result of NaIO3. 相似文献
10.
Comparison of absorption efficiency of three hydrogen sulfide absorbents and optimization of absorption conditions of potassium iodate system 下载免费PDF全文
Hydrogen sulfide is corrosive and toxic, and the use of absorbents to absorb hydrogen sulfide gas is an important desulfurization treatment. The absorption efficiency of different absorbent is different. The absorption efficiency of three different hydrogen sulfide absorbent, namely ferric chloride system, potassium iodate system and alkaline potassium ferricyanide system, was firstly compared. Based on this, the absorption parameters of potassium iodate system were optimized, and the effects of concentration, temperature, pH, gas flow rate and time on the hydrogen sulfide gas absorption efficiency were discussed. The optimum absorption conditions were obtained by orthogonal test: temperature 55℃, pH 6.01, H2S flow rate 0.3 L·min-1, absorption time 1 min, the third-order absorption efficiency of 8%(mass) potassium iodate is 51.56%. The results of this study provide a theoretical reference for the absorption of hydrogen sulfide and support for the study of indirect electrolysis process. 相似文献