Densities and Viscosities of Oleic Acid at Atmospheric Pressure

The densities of oleic acid were measured over the temperature range from (293 to 459) K at atmospheric pressure using a densimeter based on the modified hydrostatic weighing method. The dynamic viscosities of the same oleic acid sample were measured using a capillary viscometer (VPZ-2 m) in the range from (293 to 363) K at atmospheric pressure. The combined expanded uncertainty of the density, atmospheric pressure, viscosity, and temperature measurements at the 95% confidence level with a coverage factor of k = 2 is estimated to be 0.15%, 1.0%, 3.5%, and 15 mK, respectively. The values of uncertainty for density and viscosity include the effects of purity and calibration (total expanded uncertainty). These experimental data were used to develop wide-range correlations for the density and viscosity based on theoretically confirmed Arrhenius–Andrade and Vogel-Tamman-Fulcher (VTF) models. The value of the glass temperature ( T _g= 179.78 K.) for the oleic acid was estimated using the VTF parameters derived from the present viscosity measurements. To additionally validate the reliability of the measured density data, the same oleic acid samples were measured using the pycnometric method. The present study showed that the densities measured using the modified hydrostatic weighing densimeter (HWD) agree with the values obtained using the pycnometric method within 0.09% for Sample 1 and 0.25% for Sample 2.     

电子衡器特殊故障的分析及处理

因为电子衡器在安装与调试过程中出现的较为特殊的故障，难以找出正确的起因与处理方法，所以介绍了如何保证电子衡器的正常使用和计量准确性的工作体会。     

矩形垂直筛板的流体力学性能研究

在600mm的有机玻璃冷模塔中,用水-空气体系测定矩形垂直筛板的塔板压降、漏液和雾沫夹带等流体力学性能,确定了合理的塔板结构,使其具有较高的气液通量和较宽的操作范围,空塔动能因子最大可达3.0kg1/2(m1/2.s)-1,液流强度可达21.6m3/(m.h)。并对不同气液流量下塔板的流体力学实验数据进行关联和分析,得出了矩形垂直筛板的干板压降计算关联式以及漏液率随液流强度和空塔动能因子的变化关系,为矩形垂直筛板的设计提供了依据。与新垂直筛板相比,矩形垂直筛板具有更低的塔板压降。     

Development of a Magnetic Suspension Densimeter and Measurement of the Density of Toluene

The development of a magnetic suspension densimeter that has been built for measurement of the density of compressed liquid at pressures up to 30 MPa in the temperature range 20 to 150°C is described. The densimeter was first built by the author and his coworkers at NIST. We describe here further improvements made on a second system built at NMIJ based on the same principle. The densimeter uses a small coil suspended from an electronic balance. Within the coil is placed a sample cell in which the pressurized sample and a buoy, which is a permanent magnet, are enclosed. For measurement of density, balance readings are recorded (1) with the buoy at rest and (2) with the buoy in magnetic suspension. The measurement procedure is basically a hydrostatic weighing, which is simpler than those of conventional magnetic densimetry. As an example, measurements of toluene density performed as part of an inter-laboratory comparison are presented. The data agreed with reliable literature values to within a few hundredths of a per cent.     

润滑油型常减压蒸馏装置扩能改造

通过对中国石油大连石化分公司Ⅱ套蒸馏装置扩能改造的设计实践，总结归纳了在老工艺装置上采用立体传质塔盘等新技术、新设备的应用成果。改造后的标定数据表明，改造后装置处理能力可达5．1Mt／a，常、减压系统主要产品质量满足设计要求，装置能耗在386.94—406.60MJ／t，低于设计值。     

含铼钼精矿焙烧尾气收尘与铼回收一体化装置的研制与应用

研制了一种含铼钼精矿焙烧尾气收尘和铼回收装置,该装置将自激式除尘器技术与球面筛板塔技术相结合:采用自激式除尘器进行收尘和铼回收;采用球面筛板淋洗塔进行进一步收尘和铼回收,并将其应用到工程实际中。这是国内首次成功地将此类装置应用于钼精矿焙烧尾气收尘和铼回收生产实践中。经过生产实践,证明该装置切实可行,淋洗效率高,并具有结构简单、操作方便、成本低和能耗小等特点。此外,此除尘系统还可应用于冶金矿山、化工和建材等领域中的湿法除尘。     

计量秤在变角度状态的实践

介绍了物料计量秤在变角度下如何计算重量，以及变角度显示仪的工作原理和在实际中的运用。     

3D圆阀塔板性能研究

介绍了3D圆阀塔板的结构特点和实验研究情况。以空气和水为工质进行了冷模实验,研究了3D圆阀塔板的塔板压降、雾沫夹带量和泄漏量等流体力学性能。利用氧解吸法测定其塔板效率,并在相同条件下与F1浮阀塔板进行了对比实验。结果表明,在相同条件下,3D圆阀塔板比传统F1浮阀塔板的塔板效率提高5%~15%,塔板压降约低100 Pa,泄漏量和雾沫夹带量与F1浮阀塔板基本相当,是一种综合性能优良的新型浮阀塔板。     

Metrological Support and Standards in the Design,Production, and Use of High-Load Weighing Machines in Russia

An analysis is presented on development, production, and use of high-capacity weighing machines in Russia in the last ten years. Aspects arising in type approval testing are considered for high-capacity weighing machines working over wide temperature ranges.     

高炉焦炭中子测水与干焦重量补偿模型

文章叙述了高炉焦炭的中子测水原理，并给出了一种干焦重量的补偿方法，最后用一个例子说明实际的效果。