Surface morphology of styrene-butadiene rubber vulcanizate filled with novel electron beam modified dual phase filler by atomic force microscopy

Topographic and phase imaging in tapping mode atomic force microscopy (TMAFM) has been performed to investigate the effect of unmodified and modified dual phase fillers on the morphology of and the microdispersion of the filler particles in the rubber matrix. The above fillers were modified using acrylate monomer (trimethylol propane triacrylate, TMPTA) or a silane coupling agent (triethoxysilylpropyltetrasulphide, Si-69) followed by electron beam modification at room temperature. Both unmodified and surface treated fillers were incorporated in a styrene-butadiene rubber. The phase images of the above composites show three levels of contrasts that correspond to matrix, filler aggregates, and bound rubber around the filler aggregates. Also, the images further elucidate the aggregated nature of the filler due to modification, which is more pronounced in the case of electron beam modified acrylated filler loaded rubber. The corresponding topographic images have been characterized by various statistical quantities like roughness parameters and one- and two-dimensional power spectral densities (1D-PSD and 2D-PSD). As compared to the control, significant increase in surface roughness is observed in the case of the modified dual phase filler loaded composites. The higher fractal value of these vulcanizates confirms the above fact. AFM study also suggests that the electron beam modification of the above fillers significantly increases the filler-filler and filler-polymer interactions.     

Long-term stabilization of the optical fiber phase control using dual PID

We propose an approach of long-term stabilization of optical fiber phase by controlling a piezo-based phase modulator and a Peltier component attached to the fiber via a phase-locked loop( PLL) circuit w ith dual proportional-integral- derivative( PID) adjustment. With this approach,we can suppress the fast disturbance and slow drifting of optical fiber to satisfy the requirements of optical phase long-term locking. In theory,a mathematical model of an optical fiber phase control system is established. The disturbance term induced by environment influence is considered into the PLL model. The monotonous and continuous changing environment disturbance w ill cause a steady-state error in this theory model. The experimental results accords w ell w ith the theory. The steady-state performance,adjusting time,and overshoot can be improved by using the dual PID control. As a result,the long-term,highly stable and low noise fiber phase locking is realized experimentally.     

高压水除鳞泵站变频节电运行方式研究技术报告

高压除鳞系统是高速、高压设备,非生产状态下能耗高;在满足轧线连续自动除鳞的工艺要求的前提下,结合公司实施的节能减排项目,对泵站进行变频节电改造,以实现节能降耗的目的。     

Mechanical and fatigue behaviour of laser and resistance spot welds in advanced high strength steels

Abstract

A study was carried out on laser and resistance spot welds in overlapped sheets of dual phase advanced high strength steel (DP780) and deep drawing steel (DC04) of 2˙0 mm in thickness. The aim of the study was to investigate the fatigue performance of these joints under tensile shear loading as well as the monotonic performance for applications in the automotive industry. The mechanical properties, failure behaviour and fatigue life analyses of spot welds in similar and dissimilar joints were investigated by experimental and numerical methods. The structural stress concept was used to describe the fatigue lives of spot welded specimens. The results revealed different failure types with different fatigue behaviours for laser and resistance spot welds under the application of cyclic loads at 'high load' and 'low load' levels.     

Transformation texture of allotriomorphic ferrite in steel

Abstract

Many aspects of the crystallographic texture which develops when austenite transforms into martensite or bainite are well established because the process by which the parent lattice is transformed into that of the product is mathematically defined. This is not the case when the ferrite forms by a reconstructive mechanism. The allotriomorphic ferrite nucleates heterogeneously at austenite grain boundaries, and although a reproducible, low energy orientation relationship is expected to exist between the ferrite and one of the austenite grains with which it is in contact, there are reports that the ferrite can simultaneously adopt this orientation with more than one austenite grain. The authors examine this possibility using crystallographic theory in order to assess the probability of such events as a function of the strength of the texture within the austenite before its transformation.     

Mechanisms of inclusion formation in low alloy steels deoxidised with titanium

Abstract

In the present investigation, the conditions for inclusion formation in two Ti deoxidised steels and one Al–Ca deoxidised steel have been examined by means of optical and electron microscopy, in combination with a thermo dynamic analysis of the phase relations involved. It is concluded that the Ti containing inclusions form as a result of a series of reactions occurring in the ladle, during solidification and in the solid state. The important solid state reaction products are MnS, TiN, and MnOTiO₂ . The presence of Mn rich compounds at the surface of the inclusions is consistent with the observation of a Mn depleted zone in the surrounding steel matrix. In contrast, the primary inclusions in the Al–Ca deoxidised steel are complex oxysulphides, which are thermodynamically more stable and can therefore form in the liquid state.     

Mechanical properties of directly air cooled copper added microalloyed steels

Abstract

An attempt has been made to develop dual phase like microstructures in directly air cooled 1·5 wt-%Cu added Ti–B microalloyed steels. The chosen compositions have allowed to avoid pearlite formation during air cooling and yielded continuous work hardening behaviour with attractive combination of strength and ductility. Aging treatment has effectively improved the ductility without deterioration of strength. Differential Jaoult–Crussard analysis of the tensile results has explained contributions of the constituent phases in work hardening behaviour of the investigated steels.     

Failure mode transition and mechanical properties of similar and dissimilar resistance spot welds of DP600 and low carbon steels

Abstract

The present work addresses the microstructure and mechanical properties of similar and dissimilar resistance spot welds of low carbon steel (LCS) and dual phase steel (DP600). Correlations between the critical fusion zone size required to ensure pullout failure mode, the weld microstructure and the weld hardness characteristics were developed. Dissimilar DP600/LCS spot welds exhibit the lowest tendency to fail in interfacial failure mode. Effects of weld physical attributes and weld microstructure on the peak load and energy absorption of similar and dissimilar DP600/LCS resistance spot welds are analysed.     

Static and fatigue performance of weld bonded dual phase steel sheets

Abstract

Lap joints of dual phase steel sheets of 1·0 mm were prepared by adhesive bonding, spot welding and weld bonding processes using a one component epoxy base structural adhesive. Mechanical properties of the joints were evaluated by tensile shear and fatigue tests. The size of the weld nugget for both spot weld and weld bond was measured for different welding parameters (current, time) and compared. For identical welding parameters, weld bonded nuggets exhibit higher nugget diameter. Tensile shear strength of weld bonded joints is 40 and 58% higher than spot welded joints and 15 and 39% higher than adhesive bonded joints and for DP590 and DP780 steels respectively. Considering 10⁶ cycles, the endurance limit of weld bonded joint is much higher than spot welded joint but smaller than adhesive bonded joints. Overall the performance of weld bonded joints is superior to those of resistance spot welding.     

Comparison of formability of friction stir welded and laser welded dual phase 590 steel sheets

Abstract

The formability of welded dual phase 590 (DP 590) steel sheets was investigated, using both friction stir welding and laser welding. Similar and dissimilar gauge sheets were joined using both processes. The laser welded sheets were produced under process conditions typical of industrial production of tailor welded blanks. The friction stir welded specimens were produced in a lab, where different tool rotational speeds and translation speeds were investigated in order to obtain good weld properties. The formability of the welded sheets was evaluated using a series of mechanical tests, including transverse tension and plane strain formability testing. Friction stir welded specimens performed about the same as laser welded specimens in transverse tension testing; however, hardness profiles showed that the laser welds had greater peak hardness than the friction stir welds. Therefore plane strain formability tests were performed with the welds oriented along the major strain direction. When this type of weld stretching was performed the friction stir welded sheets were shown to be ～20% more formable than the laser welded sheets.