PM 2 Tec 2003: PM industry turning the corner

Abstract

MPIF's 2003 International Conference on Powder Metallurgy and Particulate Materials in Las Vegas attracted 1100 delegates from more than 30 countries. JOSEPH M. CAPUS reviews the event, while JOHN DUNKLEY assesses developments pointing the way to higher density, higher performance PM components.     

Serrated yielding in Cu-1 wt-%Cd alloy

Abstract

The influence of grain size and temperature on the serration patterns of the Portevin-Le Chatelier (PLC) effect and on the yield and flow stresses in a Cu-1 wt-%Cd alloy was investigated in the temperature range 150 to 360 ° C. Two kinds of serration patterns were observed in this alloy. Type I occurred at lower temperatures and its yield points are moderately spaced. Type II consists of regular jerky flow observed athigher temperatures. The Hall-Petch equation is obeyed over the temperature range in which jerky flow occurs. The Hall-Petch parameter k (?) is observed to show a local maximum in the temperature range where serrated flow is first observed. The PLC effect is associated with the solute- dislocation interactions, implying that k (?) contains a component associated with grain size dependent dislocation storage.     

Effect of vapour phase hydrogen peroxide,as a decontaminant for civil aviation applications,on microstructure,tensile properties and corrosion resistance of 2024 and 7075 age hardenable aluminium alloys and 304 austenitic stainless steel

Abstract

A response to the chemical or biological contamination of aircraft requires the use of a suitable decontaminant. Among possible chemical decontaminants, vapour phase hydrogen peroxide appears to be a likely candidate in terms of a combination of efficacy, low environmental impact and potential for materials compatibility. The present paper examines the effect of hydrogen peroxide, both in the vapour phase and as a liquid concentrate on two common structural materials used in aviation, namely 2024 and 7075 age hardenable aluminium alloys and on 304 austenitic stainless steel, the latter as employed in galley and lavatory surfaces. The present paper characterises both the effects of hydrogen peroxide on the microstructure of the materials and the impact that decontamination has on the tensile properties and corrosion resistance of these materials. Microstructural effects are both relatively small in magnitude and confined to a region immediately beside the exposed surface. No systematic effect is found on either the tensile properties or the post-exposure corrosion resistance of the three alloys examined. These observations are encouraging in terms of the use of vapour phase hydrogen peroxide for decontamination applications.     

Transport of large nuclear power plant components: experiences in mechanical design assessment

Abstract

In the course of decommissioning of power plants in Germany large nuclear components (steam generator, reactor pressure vessel) must be transported over public traffic routes to interim storage facilities, where they are dismantled or stored temporarily. Since it concerns surface contaminated objects or low specific activity materials, a safety evaluation considering the IAEA transport regulations mainly for industrial packages (type IP-2) is necessary. For these types of industrial packages the requirements from normal transport conditions are to be covered for the mechanical proof. For example, a free drop of the package from a defined height, in dependence of its mass, onto an unyielding target, and a stacking test are required. Since physical drop tests are impossible generally due to the singularity of such 'packages', a calculation has to be performed, preferably by a complex numerical analysis. The assessment of the loads takes place on the basis of local stress distributions, also with consideration of radiation induced brittleness of the material and with consideration of recent scientific investigation results. Large nuclear components have typically been transported in an unpackaged manner, so that the external shell of the component provides the packaging wall. The investigation must consider the entire component including all penetration areas such as manholes or nozzles. According to the present IAEA regulations the drop position is to be examined, which causes the maximum damage to the package. In the case of a transport under special arrangement a drop only in an attitude representing the usual handling position (administratively controlled) is necessary. If dose rate values of the package are higher than maximum allowable values for a public transport, then it is necessary that additional shielding construction units are attached to the large component.     

Tensile and fatigue properties of cold and warm compacted Alumix 431 alloy

Abstract

In this experimental study, tensile and fatigue properties of the Alumix 431 alloy (Al, Zn, Mg and Cu alloys) produced using the conventional press and sinter processes in different pressures and temperatures are investigated. The results clearly showed that the warm compacted specimens can reach the mechanical properties of the cold compacted ones under less pressure. In the fatigue tests it was observed that fracture started from large pores as shown in all scanning electron microscope (SEM) examinations and ductile fracture occurred. 85% of the 180 MPa/80°C and 77% of the 230 MPa/RT specimens fractured at the machined surface. Tensile and fatigue properties of warm compacted (180 MPa/80°C) and cold (230 MPa/RT) compacted specimens are almost equal at these same densities. This result indicates the economic benefit of warm compaction by the much lower applied compaction pressure.     

Tensile creep behaviour of NiAl-Cr(Zr) multiphase intermetallic alloy

Abstract

The microstructure of a multiphase NiAl-33.5Cr-0.5Zr intermetallic alloy was examined by SEM with energy dispersive spectroscopy and TEM. The tensile creep behaviour of the hot isostatically pressed NiAl-33.5Cr-0.5Zr alloy was studied. The results of the creep test indicated that all of the creep curves under the present test have similar characteristics: a short primary creep stage, a dominant tertiary creep stage, and nearly identical creep strains (~45%). The apparent stress exponent and the apparent activation energy were analysed and discussed. The mechanism of the creep deformation was also analysed by the observation of TEM.     

Effects of heat treatment processes on microstructure and properties of 2·25Cr–1Mo–0·25V HSLA steels

Abstract

In the present paper, the effects of the heat treatment processes with two conditioning treatments and four quenching–tempering processes on the mechanical properties of 2·25Cr–1Mo–0·25V high strength low alloyed (HSLA) steel are investigated. The results show that the conditioning treatments have obvious effects on the low temperature impact energy but little effect on the tensile strength. The elevation of the final austenitising temperature increases the strength, whereas it results in the decrease in the low temperature impact energy due to the coarse microstructure. The results of the fracture surfaces analysis further make sure that the fracture surfaces of tensile specimens all exhibit ductile characters with a lot of dimples. However, the fracture surfaces of impact specimens exhibit two typical fracture characters, i.e. the ductile and brittle fracture surface corresponding to the fine and coarse microstructures respectively. In addition, the elongation and reduction in area seem to be insensitive to the heat treatments. Meanwhile, the impact fracture mode is more sensitive to the grain size and not to the low temperature impact energy.     

Process and compressive properties of porous nickel materials

Abstract

Compressive properties are investigated for the porous Ni materials processing by innovated powder metallurgical (PM) method. The porous Ni materials first show a short elastic region, then a long and oblique stress yield region within the strain range of about 10–50%, and finally, a densification region where the stress increases rapidly.     

New viscoplastic model to simulate hot isostatic pressing

Abstract

Most of the numerical simulation software on the hot isostatic pressing (hipping) process is based on viscoplastic modelling of densification, such as the well known Abouaf's model. These constitutive equations are generally obtained from a viscoplastic potential depending on Green's equivalent stress. An implicit coupling between isotropic and deviator parts is therefore only defined by an equivalent stress. A new viscoplastic formulation proposed by Stutz introduces an explicit coupling between isotropic and deviator parts of the stress state, allowing then more flexibility to take into account the experimental results achieved from isotropic, die compaction, and creep tests. This paper deals with the presentation of this new formulation which has been implemented in the finite elements software PreCAD, and the subsequent changes observed in numerical simulations. These simulations achieved with PreCAD software, are compared with an experiment on a complex part manufactured by CEA Grenoble.     

Design and Realization of a Non-Circular Cable Spool to Synthesize a Nonlinear Rotational Spring

In this paper we present a cable mechanism that realizes a nonlinear rotational spring from a linear translational spring. The spring is pulled by a cable wound around a non-circular spool, which is rigidly attached to the joint. The non-circular shape of the spool induces a nonlinear relationship between its angular position and the torque created by the tension of the cable. Depending on the shape of the spool, various torque–angle relationships can be realized. We show that for a given nonlinear torque–angle relationship, there is an explicit expression (closed-form solution) of the shape of the spool that synthesizes this function. First, we present the geometry of the problem. Then, we derive the methodology to calculate the shape of the spool to synthesize a prescribed torque–angle relationship. Finally, we verify the design methodology by experiments with three different spools realizing a constant force spring, an exponential softening spring and a cubic polynomial spring. We discuss the possible sources of errors between the theoretical and experimental results.