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1.
氧化锌压敏陶瓷烧结致密化过程的研究 总被引:6,自引:0,他引:6
本文研究了氧化锌压敏陶瓷的致密化过程,结果发现只有当烧结温度升高到一定值时,试样中的ZnO粉粒产生聚集,致密化过程才开始.致密化是瓷体获得稳定电性能的基础.低熔点添加剂B2O3可以降低致密化的起始温度,而致密化过程中的等温烧结对ZnO压敏陶瓷的最大密度几乎没有影响. 相似文献
2.
Recent developments of high-performance NEOMAX magnets 总被引:6,自引:0,他引:6
For further improvement in achieving extremely high magnetic properties of Nd- Fe- B sintered magnets, extensive investigation
has been done to densify the magnet up to the theoretical value, to increase the volume fraction of the Nd
2Fe14B matrix phase, and to achieve a high degree of alignment. By controlling chemical composition and the amount of constituent
phases,improving particle size distribution, and adopting the isostatic pressing method to get better alignment of fine particles,
we have succeeded in obtaining a high-performance magnet having residual flux density (Br) of 1.495 T (14.95 kG), maximum energy product [(BH)max] of 431 kj/m3 (54.2 MGOe), and intrinsic coercivity (iHc) of 845 kA/m (10.62 kOe). 相似文献
3.
Fon-Chieh Chang R. R. Fessler B. D. Merkle J. M. Borton W. M. Goldberger 《Particulate Science and Technology》2004,22(1):35-50
Electroconsolidation® is a process for densifying complex-shaped parts by using electrically conductive particulate solids as a pressure-transmitting medium. The part is immersed in a bed of the particulate medium contained in a die chamber. Sintering temperature is achieved by resistive heating of the medium while applying compaction pressure. The process is capable of ultrahigh temperatures and short cycle times and offers the potential for low processing costs.
Control of the process and selection of process conditions require knowledge of the temperatures within the die. Temperature gradients exist because of the high heating rate and because of variations of density and electrical resistivity of the medium due to the presence of the part. Direct measurement of temperature with thermocouples or other conventional means is impractical because of the high temperatures, high currents, and high pressures that are involved. Therefore, a computer model was developed to predict temperature as a function of time and applied voltage for any location in the die. The computer model is composed of three parts: a geometrical model to approximate the density and resistivity variations in the medium, a finite-element model to calculate the rate of resistive heating within each element, and a finite-difference model to calculate the temperature distribution based on solution of the heat-transfer equations. Predicted temperatures have been shown to be in excellent agreement with measurements, and numerical simulation provided encouraging consistency and reasonably accurate predictions of temperature profiles within the die. The model demonstrated the feasibility of a new process to achieve simultaneous application of pressure and heat to powder densification in Electroconsolidation. 相似文献
Control of the process and selection of process conditions require knowledge of the temperatures within the die. Temperature gradients exist because of the high heating rate and because of variations of density and electrical resistivity of the medium due to the presence of the part. Direct measurement of temperature with thermocouples or other conventional means is impractical because of the high temperatures, high currents, and high pressures that are involved. Therefore, a computer model was developed to predict temperature as a function of time and applied voltage for any location in the die. The computer model is composed of three parts: a geometrical model to approximate the density and resistivity variations in the medium, a finite-element model to calculate the rate of resistive heating within each element, and a finite-difference model to calculate the temperature distribution based on solution of the heat-transfer equations. Predicted temperatures have been shown to be in excellent agreement with measurements, and numerical simulation provided encouraging consistency and reasonably accurate predictions of temperature profiles within the die. The model demonstrated the feasibility of a new process to achieve simultaneous application of pressure and heat to powder densification in Electroconsolidation. 相似文献
4.
Eric W. Neuman Benjamin J. Lai Jeremy L. Watts Gregory E. Hilmas William G. Fahrenholtz Laura Silvestroni 《International Journal of Applied Ceramic Technology》2021,18(6):2224-2236
Densification behavior, microstructure, and mechanical properties of zirconium diboride (ZrB2) ceramics modified with a complex Zr/Si/O-based additive were studied. ZrB2 ceramics with 5–20 vol.% additions of Zr/Si/O-based additive were densified to >95% relative density at temperatures as low as 1400°C by hot-pressing. Improved densification behavior of ZrB2 was observed with increasing additive content. The most effective additive amount for densification was 20 vol.%, hot-pressed at 1400°C (∼98% relative density). Microstructural analysis revealed up to 7 vol.% of residual second phases in the final ceramics. Improved densification behavior was attributed to ductility of the silicide phase, liquid phase formation at the hot-pressing temperatures, silicon wetting of ZrB2 particles, and reactions of surface oxides. Room temperature strength ranged from 390 to 750 MPa and elastic modulus ranged from 440 to 490 GPa. Vickers hardness ranged from 15 to 16 GPa, and indentation fracture toughness was between 4.0 and 4.3 MPa·m1/2. The most effective additive amount was 7.5 vol.%, which resulted in high relative density after hot-pressing at 1600°C and the best combination of mechanical properties. 相似文献
5.
Jae Ryong Kim Do-Hyeong Kim Chong Hee Kim 《Journal of the American Ceramic Society》1990,73(8):2567-2569
The effects of ZrO2 and Y2 O3 on the densification of hotpressed Si3 N4 -Zr(Y)O2 composites have been studied. High density could not be obtained by the addition of pure or 3-mol%-Y2 O3 -doped ZrO2 in this composite; however, nearly full density (>97%) could be obtained in Si3 N4 using 6- and 8-mol%-Y2 O3 -doped ZrO2 . It is concluded that Y2 O3 diffusing out from the added Zr(Y)O2 promoted the densification and that ZrO2 also had some role in the formation of an oxynitride glass. 相似文献
6.
S. R. Dargar L. J. Groven J. J. Swiatkiewicz J. A. Puszynski 《International Journal of Self-Propagating High-Temperature Synthesis》2007,16(3):125-132
The primary objective of this investigation was focused on in-situ densification of SHS composites synthesized from nanoreactants.
Simultaneous combustion synthesis and densification technique was utilized and it was found to be an effective method to form
dense intermetallic-ceramic composites. In this research study, two nanoreactant energetic systems, Al-TiO2 and Ni-Al-Al2O3, were explored. In-situ combustion synthesis and densification experiments were conducted in a uniaxial press with densification
pressures up to 200 MPa and preheating capability of 1500K. The experiments were conducted in both vacuum and Ar atmosphere.
Samples of titanium aluminides-alumina composites with density in the range of 95–98% have been obtained at a preheating temperature
of 860°C and pressure of 100 MPa. Reactants and SHS-produced materials were characterized by SEM, XRD, BET, and DSC/TGA. In
addition, more fundamental studies of the reaction kinetics as a function of average particle size of aluminum nanopowders
were conducted using DSC.
相似文献
7.
In the ceramic technology the first step to produce sintered bodies is the manufacturing of powders which then are densified. The adhesion mechanisms between the single particles and the agglomerates produced from them determine the densification process. Starting from theoretical considerations adhesion mechanisms, such as solid bridge formation, adhesive bonding and glide-promoting effects, are discussed in principle. Subsequently, the effects of surface-active substances on the densification behaviour of clay-ceramics and oxide-ceramic bodies are discussed. Further, the evaluation of the action of additives to the powder mixtures on the microstructure of the compacts, such as porsity and texture, leads to a compaction equation which describes the transition from the powder pile to a densified green body. 相似文献
8.
9.
以碳毡为预制体,N2为稀释气体,甲烷为碳源前驱体,其分压为10 kPa,滞留时间为0.15 s的工艺条件下,研究了不同沉积温度对微波热解化学气相渗透(chemical vapor infiltration,CVI)工艺制备碳/碳复合材料的致密化速率、样品的体积密度及其密度均匀性的影响,并对其组织结构进行了观察.分析了沉积温度对微波热解CVI工艺制备碳/碳复合材料的密度与组织结构的变化规律.结果表明:在微波热解CVI工艺中,随着沉积温度的降低,碳毡预制体的致密化速率及最终体积密度呈现先升后降,1100 ℃沉积制备复合材料的密度均匀性最好,并呈现从内到外逐步沉积的规律.热解碳的织构主要为中等织构. 相似文献
10.