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New technology, especially in the field of microelectronics and mechatronics, created the need for making, positioning and inspection techniques of long microbore-holes and gaps (defined by length/width to diameter ratio l/d > 10 for d < 200 μm). The technological aspect is, in principle, subdued but the metrological one is still unsolved.In Zosel et al. [Zosel J, Guth U, Thies A, Reents B. Flow measurements in micro holes with electrochemical and optical methods. Electrochim Acta 2003;48:3299–305] the properties (power loss and phase distortion) of focused laser microbeam penetrating extremely long through microbores is described; it was proved that the measurement information is distorted depending on the microbore geometry. The samples were prepared of glass–resin laminate with microbore diameter ranging from 35 to 200 μm.In present research an adjustable 100 μm microbore is used as a master. It is formed of mutually accurately adjusted 20 metal plates 100 μm thick set of coaxially in pile. Precise positioning of each plate enables creating free-shaped microbore.The photon batching device emitting 2.5 million photons per second is used as a generator of incident photon beam. The measured transmission efficiency is understood as a relation between outgoing and incoming light energy. The outgoing energy, for particular microbore, was determined by scanning linearly and angularly the bore with photon beam and integrating the results. Experiments were performed in dark room with background 2/5 photons per second (including dark current of photomultiplier).These changes describe the relationship between the shape of the microbore and the transmission energy and can be considered as a measure of microbore cylindricity deviation. 相似文献
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Adrienne R. Boden Gerald E. Ladwig Eric J. Reiner 《Polycyclic Aromatic Compounds》2013,33(3-4):301-310
The gas chromatographic analysis of polycyclic aromatic compounds can be completed faster and with increased chromatographic resolution using microbore columns (Fast GC). Microbore columns contain two to three times the number of theoretical plates per meter when compared to 0.25 mm internal diameter (i.d.) capillary columns. The increased chromatographic resolving power of microbore columns enables separations to be carried out with much shorter columns giving rise to faster analysis times. Analysis times of priority polycyclic aromatic hydrocarbons on 20 m (5% phenyl, 0.1 mm i.d., 0.1 w m film thickness) and 10 m (5% phenyl, 0.1 mm i.d., 0.1 w m film thickness) columns are reduced by about 45% and 60% respectively in comparison with 30 m columns, and data quality (precision and accuracy) is not affected. All areas/parameters of the chromatographic system must be adjusted and optimized to ensure proper chromatographic performance. Smaller injection volumes (0.2-0.5 w L) and injection liners (1-2 mm i.d.) are required to obtain optimum (and reproducible) chromatography on 0.1 mm i.d. columns. 相似文献
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对橡胶与聚乙烯共混微孔材料进行了静态力学和动态力学性能表征,并通过电镜观察其材料拉伸受力前后的微孔结构变化,了解材料的各种力学行为及材料组份和加工工艺对材料力学性能的影响,同时检验材料的透水性能。 相似文献
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