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1.
Damir Sagdeev Il'giz Gabitov Chingiz Isyanov Vener Khairutdinov Mansur Farakhov Zufar Zaripov Ilmutdin Abdulagatov 《Journal of the American Oil Chemists' Society》2019,96(6):647-662
The densities of oleic acid were measured over the temperature range from (293 to 459) K at atmospheric pressure using a densimeter based on the modified hydrostatic weighing method. The dynamic viscosities of the same oleic acid sample were measured using a capillary viscometer (VPZ-2 m) in the range from (293 to 363) K at atmospheric pressure. The combined expanded uncertainty of the density, atmospheric pressure, viscosity, and temperature measurements at the 95% confidence level with a coverage factor of k = 2 is estimated to be 0.15%, 1.0%, 3.5%, and 15 mK, respectively. The values of uncertainty for density and viscosity include the effects of purity and calibration (total expanded uncertainty). These experimental data were used to develop wide-range correlations for the density and viscosity based on theoretically confirmed Arrhenius–Andrade and Vogel-Tamman-Fulcher (VTF) models. The value of the glass temperature ( T g= 179.78 K.) for the oleic acid was estimated using the VTF parameters derived from the present viscosity measurements. To additionally validate the reliability of the measured density data, the same oleic acid samples were measured using the pycnometric method. The present study showed that the densities measured using the modified hydrostatic weighing densimeter (HWD) agree with the values obtained using the pycnometric method within 0.09% for Sample 1 and 0.25% for Sample 2. 相似文献
2.
因为电子衡器在安装与调试过程中出现的较为特殊的故障,难以找出正确的起因与处理方法,所以介绍了如何保证电子衡器的正常使用和计量准确性的工作体会。 相似文献
3.
变形观测与高精度测量机器人系统 总被引:2,自引:0,他引:2
介绍了中南大学自行研制开发的高精度测量机器人系统的组成,工作原理,以及该系统实现高精度观测所采取的主要措施;仪器室内检定,野外边频同测,高精度气象改正,周日观测等,同时以某电站大坝的变形观测为例,简单介绍该系统可达到的精度及工程应用领域。 相似文献
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R. Masui 《International Journal of Thermophysics》2002,23(4):921-935
The development of a magnetic suspension densimeter that has been built for measurement of the density of compressed liquid at pressures up to 30 MPa in the temperature range 20 to 150°C is described. The densimeter was first built by the author and his coworkers at NIST. We describe here further improvements made on a second system built at NMIJ based on the same principle. The densimeter uses a small coil suspended from an electronic balance. Within the coil is placed a sample cell in which the pressurized sample and a buoy, which is a permanent magnet, are enclosed. For measurement of density, balance readings are recorded (1) with the buoy at rest and (2) with the buoy in magnetic suspension. The measurement procedure is basically a hydrostatic weighing, which is simpler than those of conventional magnetic densimetry. As an example, measurements of toluene density performed as part of an inter-laboratory comparison are presented. The data agreed with reliable literature values to within a few hundredths of a per cent. 相似文献
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An analysis is presented on development, production, and use of high-capacity weighing machines in Russia in the last ten years. Aspects arising in type approval testing are considered for high-capacity weighing machines working over wide temperature ranges. 相似文献
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介绍了铁合金冶炼时需要准备的原料,对不合格原料需要进行加工处理,达到合格粒度。并提出了影响铁合金冶炼过程有原料的粒度,配料称量,混合等重要因素。 相似文献
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