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排序方式: 共有126条查询结果,搜索用时 15 毫秒
1.
2.
Jogender Singh Douglas E. Wolfe 《Journal of Materials Engineering and Performance》2005,14(4):448-459
Fabrication of cost-effective, nano-grained net-shaped components has brought considerable interest to Department of Defense,
National Aeronautics and Space Administration, and Department of Energy. The objective of this paper is to demonstrate the
versatility of electron beam-physical vapor deposition (EB-PVD) technology in engineering new nanostructured materials with
controlled microstructure and microchemistry in the form of coatings and net-shaped components for many applications including
the space, turbine, optical, biomedical, and auto industries. Coatings are often applied on components to extent their performance
and life under severe environmental conditions including thermal, corrosion, wear, and oxidation. Performance and properties
of the coatings depend upon their composition, microstructure, and deposition condition. Simultaneous co-evaporation of multiple
ingots of different compositions in the high energy EB-PVD chamber has brought considerable interest in the architecture of
functional graded coatings, nano-laminated coatings, and design of new structural materials that could not be produced economically
by conventional methods. In addition, high evaporation and condensate rates allowed fabricating precision net-shaped components
with nanograined microstructure for various applications. Using EB-PVD, nano-grained rhenium (Re) coatings and net-shaped
components with tailored microstructure and properties were fabricated in the form of tubes, plates, and Re-coated spherical
graphite cores. This paper will also present the results of various metallic and ceramic coatings including chromium, titanium
carbide (TiC), titanium diboride (TiB2), hafnium nitride (HfN), titanium-boron-carbonitride (TiBCN), and partially yttria stabilized zirconia (YSZ) TBC coatings
deposited by EB-PVD for various applications.
This paper was presented at the International Symposium on Manufacturing, Properties, and Applications of Nanocrystalline
Materials sponsored by the ASM International Nanotechnology Task Force and TMS Powder Materials Committee, October 18–20,
2004, Columbus, OH. 相似文献
3.
Alper Sarıoğlan Ömer Tunç Savaşçı Ayşe Erdem-Şenatalar Vu Thu Ha Gilbert Sapaly Younès Ben Taârit 《Catalysis Letters》2007,118(1-2):123-128
MFI type inorganic carrier was used in two different cationic forms, hydrogen and calcium respectively. MFI-supported molybdenum
and rhenium catalysts were prepared. The activities of the catalysts were compared for the aromatization reaction of methane.
Higher activity values were attained with the catalysts supported on HZSM-5. Aromatics were also observed with the catalysts
supported on CaZSM-5, despite their deficiency in acid sites. Highly dispersed rhenium is expected to be formed with the use
of the inorganic carrier in calcium form. On the other hand, lower reaction rates were observed with rhenium supported on
CaZSM-5, in spite of the improved dispersion of the active rhenium species on this catalyst. This was interpreted in terms
of the critical role of the acid sites in the conversion of methane to aromatics, compared to the improved dispersion of the
active metal. 相似文献
4.
锝萃取型发生器技术是采用溶剂萃取的方法生产^99Tc^m。对锝萃取工艺条件进行了初步研究。由于锝与铼有相似的化学性质,实验中研究了在碱性体系中甲乙酮对铼的萃取行为,考察了萃取剂用量、碱液浓度、铼的浓度及水相中铝浓度对萃取铼的影响,在此基础上进行了^99Tc^m的示踪实验,实验结果表明:甲乙酮对^99Tc^m萃取率达99%。 相似文献
5.
Effect of rhenium addition on isothermal oxidation behavior of single-crystal Ni-based superalloy 总被引:1,自引:0,他引:1
The isothermal oxidation behavior of a nickel-based superalloy, which we designate as DD32, containing 4 wt.% rhenium and another alloy (DD32M) without rhenium were investigated at 900, 1000 and 1100 °C. Oxidized alloys were characterized by SEM, EDX, EPMA and XRD. The two alloys revealed similar oxidation rates at 900 °C, while the DD32 alloy showed a slightly higher mass gain than that of the DD32M alloy during 1000 and 1100 °C exposure. Surface and cross-sectional examination indicated that DD32 alloy showed nonuniform oxidation between dendritic and interdendritic areas at all temperatures. Similar different oxidation behavior between dendritic and interdendritic regions was also observed in the DD32M alloy at 900 °C. However, DD32M showed relatively uniform oxidation at 1000 and 1100 °C exposure. Therefore, Re addition clearly induced the nonuniform oxidation of the alloy. 相似文献
6.
7.
《Journal of Industrial and Engineering Chemistry》2014,20(1):145-152
The metathesis of ethylene and 2-pentene for propylene production was investigated over Re2O7/SiO2-Al2O3 catalysts. The SiO2-Al2O3 (50 wt% Al2O3) were obtained by co-precipitation, physical mixing, and sol–gel coating. The presence of isolated layers/grains γ-Al2O3 either in bulk (physical mixing) or on the surface (sol–gel coating) resulted in isomerization-free metathesis. On the contrary, the Re2O7 catalysts supported on co-precipitated SiO2-Al2O3 or the direct synthesis showed both metathesis and double-bond shift isomerization activities and as a consequence, higher propylene yield was obtained via the secondary metathesis reaction. The catalytic properties were also correlated with the Al-atom rearrangements and the acidic characters/strengths. 相似文献
8.
《Journal of the European Ceramic Society》2014,34(16):4443-4449
Rhenium diboride (ReB2) powder was prepared by mechanochemical processing of Re–B powder mixtures with subsequent annealing at temperatures of 600 °C to 1200 °C. Reactive evolution during the synthesis was investigated; furthermore, the effects of the amount of excess B on the reactions that occurred during the synthesis were assessed. The substantial reaction of Re with B occurred at 700 °C to form Re7B3 with a small amount of ReB2. At 800 °C, Re7B3 converted into ReB2; this conversion was enhanced with increasing temperature and increasing amount of excess B. At 1000 °C or above, single-phase ReB2 powder without trace quantities of Re7B3 was obtained for compositions with 15 wt% or greater excess B. The synthesized ReB2 powder particles were submicrometer with the vast majority being ∼500 nm. In addition, the resulting ReB2 powders were consolidated by hot pressing or spark plasma sintering to examine the sinterability of the powders. 相似文献
9.
10.