电火花铣削钛合金电极损耗在线补偿研究

根据电火花铣削等损耗理论，对用电火花铣削钛合金的加工中电极损耗补偿作了分析阐述。并根据正交试验的数据对理论分析结果进行对比，同时给出了一定的结论和建议。     

The effect of supercooling on crystallization of cocoa butter-vegetable oil blends

The solid fat content (SFC), Avrami index (n), crystallization rate (z), fractal dimension (D), and the pre-exponential term [log(γ)] were determined in blends of cocoa butter (CB) with canola oil or soybean oil crystallized at temperatures (T _Cr) between 9.5 and 13.5°C. The relationship of these parameters with the elasticity (G′) and yield stress (σ^*) values of the crystallized blends was investigated, considering the equilibrium melting temperature (T _M ^o) and the supercooling (i.e., T _Cr ^o−T _M ^o) present in the blends. In general, supercooling was higher in the CB/soybean oil blend [T _M ^o=65.8°C (±3.0°C)] than in the CB/canola oil blend [T _M ^o=33.7°C (±4.9°C)]. Therefore, under similar T _Cr values, higher SFC and z values (P<0.05) were obtained with the CB/soybean oil blend. However, independent of T _Cr TAG followed a spherulitic crystal growth mechanism in both blends. Supercooling calculated with melting temperatures from DSC thermograms explained the SFC and z behavior just within each blend. However, supercooling calculated with T _M ^o explained both the SFC and z behavior within each blend and between the blends. Thus, independent of the blend used, SFC described the behavior of G′_eq and σ^* and pointed out the presence of two supercooling regions. In the lower supercooling region, G′_eq and σ^* decreased as SFC increased between 20 and 23%. In this region, the crystal network structures were formed by a mixture of small β′ crystals and large β crystals. In contrast, in the higher supercooling region (24 to 27% SFC), G′_eq and σ^* had a direct relationship with SFC, and the crystal network structure was formed mainly by small β′ crystals. However, we could not find a particular relationship that described the overall behavior of G′_eq and σ^* as a function of D and independent of the system investigated.     

A new strategy for defect inspection by the virtual inspection in semiconductor wafer fabrication

The defect of process equipments is a major factor that impairs the yields in the mass production of semiconductor wafer fabrication and it is a main supervision means to use high-resolution defect inspection tools to detect and monitor the defect damage. Due to the high investment costs of these inspection tools and the resulting decrease in the throughput, how to improve the sampling rate is an important issue for the associated inspection strategy. This paper proposes a new concept and implementation of virtual inspection (VI) to enhance the detection and monitoring of defect in semiconductor production process. The underlying theory of the VI concept is that the state variables identifications (SVIDs) of process equipments can reflect the process quality effectively and loyally. The approach of VI is to combine the application of the fault detection and classification (FDC), and the defect library and the re-engineering of inspection procedure to reach the full-scope of strategic objective. VI enables the defect monitoring to enter a new era by promoting the monitoring level of defect inspection from the previous lot-sampling basis to the wafer-sampling level, and hence upgrades the sampling strategy from random-sampling to full and right-sampling. In this study, various typical defect cases are utilized to illustrate how to create VI models and verify the reliability of the proposed approach. Furthermore, a feasible architecture of the VI implementation for mass production in semiconductor factory is presented in the paper.     

扩展Oracle Spatial实现跨服务器的空间数据管理*

海量空间数据的管理需要多服务器的支持,空间数据的跨服务器操作是必须解决的关键问题。针对Oracle数据库系统的Client／Server体系在管理跨服务器空间数据中存在的问题,利用远程内嵌过程和触发器等相关技术,设计并扩展了Oracle Spatial的功能,实现了基于Oracle的空间数据跨服务器分布式管理。     

Influence of the connecting tube at the cold end in a U-shaped pulse tube cryocooler

In some special applications, the pulse tube cryocooler must be designed as U-shape; however, the connecting tube at the cold end will influence the cooling performance. Although lots of U-shape pulse tubes have been developed, the mechanism of the influence of the connecting tube on the performance has not been well demonstrated. Based on thermoacoustic theory, this paper discusses the influence of the length and diameter of the connecting tube, transition structure, flow straightener, impedance of the inertance tube, etc. on the cooling performance. Primary experiments were carried out in two in-line shape pulse tube cryocoolers to verify the analysis. The two cryocoolers shared the same regenerator, heat exchangers, inertance tube and straightener, and the pulse tube, so the influence of these components could be eliminated. With the same electric power, the pulse tube cryocooler without connecting parts obtained 31 W cooling power at 77 K; meanwhile, the other pulse tube cryocooler with the connecting parts only obtained 27 W, so the connecting tube induced more than a 12.9% decrease on the cooling performance, which agrees with the calculation quite well.     

Simulation and experimental study of phase segregation in helical pipes: A new method for flow conditioning

The aim of the present study is to contribute some knowledge of phase separation phenomena of gas–liquid turbulent flow in curved pipe and provide a basis for the development of an in-line gas–liquid separator and flow pattern conditioning device. A systematic study of gas–liquid three-phase flow in 3D helical pipes was numerically performed. Gas phase distribution in the flow through the helical pipe was analyzed for various flow parameters conditions and different pipe geometries. Experimental qualitative results show that a helical pipe can, successfully, be used to condition a bubble flow into a stratified (stratified wavy flow). The main idea is to put it just upstream of sensors that are flow regime dependent; ensuring that the sensor, once calibrated to work in this flow pattern, suffers no reduction in its performance and, consequently, avoid additional sources of error.     

Characterization of extensional rheological filament stretching with a dual‐mode Giesekus model

A new, simple, formulation that describes capillary thinning as predicted by a two‐mode Giesekus model is derived, and its application in analyzing data from extensional rheometry (capillary thinning) experiments is discussed. An algorithm is presented that can be used to fit the expressions obtained from the Giesekus model to extensional rheometry data. Examples of data fitting are given for an idealized data set, for measurements obtained for aqueous solutions of 6 wt % 900,000 molecular weight polyethylene oxide, and for biological fluids obtained from pitchers of Nepenthes Rafflesiana. Good fits to the data were obtained, with coefficients of determination in excess of 0.98. For each data set, it was possible to calculate values of extensional viscosity and relaxation time for each of the two modes, allowing quantitative comparison of different fluids or of the same fluid as it ages. © 2016 American Institute of Chemical Engineers AIChE J, 62: 2188–2199, 2016     

Additive Manufacturing of Dense Ceramic Parts via Direct Ink Writing of Aqueous Alumina Suspensions

Additive manufacturing of near‐net‐shaped dense ceramic components has been established via room‐temperature direct writing of highly loaded aqueous alumina suspensions in a layer‐by‐layer fashion. The effect of alumina solid loading on rheology, specimen uniformity, density, microstructure, and mechanical properties was studied. All suspensions contained a polymer binder (~5 vol.%), dispersant, and 51–58 vol.% alumina powder. Rheological measurements indicated all suspensions to be yield‐pseuodoplastic, and both yield stress and viscosity were found to increase with increasing alumina solid loading. Shear rates ranging from 19.5 to 24.2/s, corresponding to viscosities of 9.8 to 17.2 Pa·s, for the 53–56 vol.% alumina suspensions were found to produce the best results for the 1.25‐mm tip employed during writing. All parts were sintered to >98% of true density, with grain sizes ranging from 3.2 to 3.7 μm. The average flexure strength, which ranged from 134 to 157 MPa, was not influenced by the alumina solid loading.     

Rheology evolution of a geopolymer precursor aqueous suspension during aging

Geopolymer-based glass-ceramic matrix composites can be processed at room temperature and a heat treatment below 100°C leads to matrix hardening thanks to the geopolymerization mechanisms. The stabilization of the matrix into glass-ceramics is achieved via a post-curing at high temperature. This paves the way of the utilization of cost-effective liquid composite molding processes, for which all the necessary equipment is already available for processing temperature ranges related to polymer matrix composites, provided that the rheological behavior of the precursor is suitable to conveniently permeate the fibrous preform. The paper describes the thixotropic rheological behavior of a reference suspension at processing temperature (10°C-20°C) and its evolution along aging at −18°C. The changes are interpreted in terms of geopolymerization mechanisms (dissolution and polycondensation) and suspension rheology (predominance of hydrodynamic effects at high shear rate). On this basis, a phenomenological modeling framework, combining two Krieger-Dougherty equations, is proposed to build a relationship between the effective viscosity of the suspension and the phenomena involved during aging (dissolution of aluminosilicate particles) and shearing (microstructure scalar variable).     

Transparent polycrystalline MgAl2O4 ceramic fabricated by spark plasma sintering: Microwave dielectric and optical properties

The optical properties and microwave dielectric properties of transparent polycrystalline MgAl₂O₄ ceramics sintered by spark plasma sintering (SPS) through homemade nanosized MgAl₂O₄ powders at temperatures between 1250 °C and 1375 °C are discussed. The results indicate that, with increasing sintering temperatures, grain growth and densification occurred up to 1275 °C, and above 1350 °C, rapid grain and pore growth occurred. The in-line light transmission increases with the densification and decreases with the grain/pore growth, which can be as high as 70% at the wavelength of 550 nm and 82% at the wavelength of 2000 nm, respectively. As the sintering temperature increases, Q×f and dielectric constant ε_r values increase to maximum and then decrease respectively, while τ_f value is almost independent of the sintering temperatures and remains between −77 and −71 ppm/°C. The optimal microwave dielectric properties (ε_r=8.38, Q×f=54,000 GHz and τ_f=−74 ppm/°C) are achieved for transparent MgAl₂O₄ ceramics produced by spark plasma sintering at 1325 °C for 20 min.