Transmission electron microscopic analysis of kidney glomeruli obtained by fine-needle aspiration

Aspiration biopsy of tumors and transplanted organs is a popular atraumatic method for diagnosis and also for the management of patients. Apart from the cytological analyses, it is clear that large aggregates of cells are obtained and these may be examined by electron microscopy. A study was carried out with dogs to assess the yield of intact glomeruli and tubules, resulting from a standard fine-needle aspiration procedure. Employing a 20-gauge needle, yields of approximately ten intact glomeruli were obtained with a tissue processing protocol that utilized filtration through a nylon mesh and backwashing, to resuspend the trapped aggregates. Processing for electron microscopy was carried out in microcentrifuge tubes. The ultrastructural preservation was excellent and the extension of these studies to investigations of not only renal transplantation, but also for diagnosis in human renal diseases of a broad spectrum, is suggested.     

GCr15轴承钢的热变形模拟试验研究

利用先进的Gleeble-2000热模拟试验机，对GCr15轴承钢某一轧制过程进行模拟试验，测定出GCr15轴承钢动态CCT曲线，并结合微观组织分析，制定合理的GCr15轴承钢轧后控制冷却工艺，以期达到提高GCr15轴承钢质量的最终目的。     

Preparation of ultra fine nickel-copper bimetallic powder for BME-MLCC

The preparation of ultra fine nickel-copper bimetallic powder with two-stage chemical reduction method was investigated. Reductive sugar and hydrazine hydrate were employed as reducing agent in different reductive stage, respectively. Reaction of CuSO₄·5H₂O with reductive sugar at 70 °C gives cuprous oxide and copper particles, then as-prepared mixture and nickelous hydroxide were reduced by hydrazine hydrate, and nickel-copper powder having excellent dispersibility was prepared. Influences of nickel added on composition and dispersibility of powder were studied. TG/DTG/DTA of nickel-copper powder, which is stable in room temperature, were discussed with thermal analyzer. Relation of nickel content to oxidation temperature was investigated. Ni-Cu bimetallic powder particles have a fully coated structure when nickel content is up to 30%. As-prepared nickel-copper powder was applied in base metal electrode-multilayer ceramic capacitor (BME-MLCC). The end termination has high adhesion force, fairly good densification, low resistivity, excellent solderibility behavior and resistance behavior to soldering.     

Handling of fine-particles by time-averaged particle driving method in plasmas

We developed a noble technique for the fine-particle handling in plasmas. In this method a pair of point electrodes are introduced in the plasma, to which positive pulses are applied alternatively. When the pulse repetition period is shorter than the particle response time, the particles feel only time-averaged force because of their large mass. Spatial profile of the equivalent potential of the time-averaged force varies from a circle to an ellipse with an increase in the local discharge at the electrodes. The particles are eventually transported toward a middle point between two point-electrodes, being almost independent of their initial positions. This method is quite effective for converging fine particles in the plasma.     

精细陶瓷注射成型工艺现状及发展动态

精细陶瓷注射成技术远比人们起初想象复杂的多，它已不再被人们认为是由塑料工业直接转变而来的技术。本文论述了陶瓷注射成型工艺的关键技术及其发展动态，提出了今后注射民面临的主要问题及需要加强的研究领域。     

微量Mn对纯银的性能影响

在99.995%Ag中添加0.01wt%Mn，制成99.99%银材，进行机械性能测试。当ε=97%时，在25℃下，σb＝340MPa，Hv＝103保持365d稳定不变，即在高纯Ag中存在微量Mn，能细化Ag的晶粒。晶粒小，晶界增多，变形抗力增大，起到强化和稳定机械性能的作用。     

铜塔铸造工艺

介绍了五台山铜塔铸造工艺,由于其结构特殊,故采用了3种工艺分别铸造而成:细砂湿模造型、树脂砂毁模贴皮造型和熔模铸造.介绍了铜塔表面化学着色技术.铜塔铸造工艺对其他相似艺术铸品具有一定的借鉴价值.     

超高分子相对质量部分水解聚丙烯酰胺合成研究

选择AM均聚后水解工艺路线,采用新型复配引发体系,合成作为油田驱油剂的超高相对分子质量聚丙烯酰胺(简称PAM).在所选高效的引发体系下,考察了主要聚合反应因素对产品平均分子相对质量的影响,确定了聚合工艺条件溶液的pH值为11～11.5,W(单体)为45%,W(引发剂)为70×10-6,W(链转移剂)为1.3×10-6.在优化的聚合条件下,合成了相对分子质量高达25×106,水解度在20%～30%可调,过滤比小于1.3的聚丙烯酰胺.     

水泥基复合材料纳米化改性的研究

水泥基材料中70％为纳米尺度的C—S—H凝胶,因此对水泥基材料进行纳米改性具有很好的基础,我国有一些关于纳米基材料在混凝土中应用的研究,但目前还不可能在实体工程中采用这种混凝土。纳米在水泥科技中的应用应首先是纳米技术与一些技术含量高的水泥基复合材料的结合。研制具有超高性能(力学)以及特定功能的纳米水泥基复合材料是目前水泥基材料纳米化改性的研究方向。