废蜜生产焦糖的工艺研究

介绍一种利用废蜜生产焦糖的新工艺。对影响焦糖色率的添加剂，熬制温度、时间等因素进行了研究。     

焦糖色配方的工艺优化

为烹饪中的焦糖色标准化和科学化生产提供科学依据,对焦糖色的最优配方和制作工艺进行了研究。以感官评分为标准,通过单因素试验和响应面试验研究了白砂糖添加量、加热时间、沸水添加量的影响。确定焦糖色最佳制作配方和工艺条件为:白砂糖添加量为153.51 g,加热时间为8.91 min,沸水添加量为99.88 g。经此配方工艺制作的焦糖色感官评分高达98.7,具有焦香味浓郁,色泽呈深黑红棕色且富有光泽等特点。最后,以卤肉为载体,比较焦糖色与常用食品增色剂老抽酱油以及焦糖色和老抽酱油混合物(老抽:焦糖=1:1混合,m/m)对食品色泽参数包括亮度L*值、红度a*值、黄度b*值、彩度c*值的影响。结果表明,三种食品增色剂对卤肉的亮度L*值和黄度b*值和彩度c*值没有显著性差异(p>0.05),对卤肉的红度a*值差异显著(p<0.05),说明焦糖色能够提高卤肉的光泽度和红度,与感官评定结果一致。     

淀粉挤压法焦糖色素生产工艺研究

在以蔗糖为原料采用挤压法生产焦糖色素的基础上,采用正交实验的方法,对以淀粉为原料挤压法生产焦糖色素的工艺进行研究,重点考察了焦糖色素色率、水溶性等指标,确定挤压法焦糖色素的生产条件。     

Detection and Quantification of 4(5)‐Methylimidazole in Cooked Meat

4(5)‐Methylimidazole (4‐MeI) is a nitrogen‐containing heterocyclic compound found in class III and IV ammoniated caramel colors, a group of additives widely used in the food industry. A suspected carcinogen and neurotoxin and efforts are underway to limit its presence in foods. Several methods have been developed to detect and quantitate 4‐MeI in different food matrices, including roasted coffee, beer, soft drinks, and soy sauce; however, no methods are available to measure 4‐MeI in cooked meat and meat products containing lipids and high levels of interfering nitrogen compounds, such as amino acids and peptides. A rapid method using 0.1 M sodium acetate buffer (pH 5) as an extraction solvent followed by derivatization with isobutylchloroformate and gas chromatograph mass‐spectrometry was developed to quantify 4‐MeI in cooked meat products with added caramel colors containing 4‐MeI. Selected ion monitoring mode was used to monitor 4‐MeI ions fragments. In the 8 commercial meat products tested, 4‐MeI levels ranged from 0.041 to 1.015 mg/kg, with recovery of 94.76% to 103.94%. In addition, a matrix‐matched calibration performed by analyzing a spiked cooked meat sample indicated no significant difference (P > 0.05), which means the meat matrix had no effect on the developed method. This method proved useful in analyzing 4‐MeI in meat products with added caramel color containing 4‐MeI.     

焦糖色素的耐盐性及检测方法

阐述了焦糖色素耐盐性的概念,探讨了焦糖色素耐盐性的内在机理,提供了检测的方法。     

Sucrose Degradation Under Model Processing Conditions

ABSTRACT: During raw and refined sugars processing, chemical changes occur that affect yield and end product color. Model sucrose solutions of 65 and 15 brix were treated with invert sugar levels of 0 to 4%, adjusted to pH 6 to 9, then processed 85 7deg;C for 0 to 6 h. Sucrose loss was correlated with changes in invert sugar concentration under acid conditions. Invert sugars concentrations were correlated with color development under alkaline conditions. At both 65 and 15 brix sucrose, and pH below 7.5, samples showed a 25% increase in invert sugars from acid hydrolysis. Sucrose loss was 1.6% with 3% invert sugar present. At pH 8.5 and higher, color increased in direct correlation with invert sugar concentrations.     

EXAMINATION OF SOME BREWING MATERIALS AND CARAMELS FOR THE POSSIBLE OCCURRENCE OF 4-METHYLIMIDAZOLE

An investigation was carried out to determine how much, if any, 4-methylimidazole is present in caramels and some other materials used in brewing. Existing analytical methods were modified to improve sensitivity. 4-Methylimidazole was not detectable in roasted barley, chocolate malt, crystal malt, Farbebier, wort and beer, when the limit of detection was 1 mg/kg. However, caramels manufactured by different processes contained amounts ranging from undetectable to 280 mg/kg.     

Effect of Various Food Additives on the Levels of 4(5)‐Methylimidazole in a Soy Sauce Model System

In this study, the effect of food additives such as iron sulfate, magnesium sulfate, zinc sulfate, citric acid, gallic acid, and ascorbic acid on the reduction of 4(5)‐methylimidazole (4(5)‐MI) was investigated using a soy sauce model system. The concentration of 4(5)‐MI in the soy sauce model system with 5% (v/v) caramel colorant III was 1404.13 μg/L. The reduction rate of 4(5)‐MI level with the addition of 0.1M additives followed in order: iron sulfate (81%) > zinc sulfate (61%) > citric acid (40%) > gallic acid (38%) > ascorbic acid (24%) > magnesium sulfate (13%). Correlations between 4(5)‐MI levels and the physicochemical properties of soy sauce, including the amount of caramel colorant, pH value, and color differences, were determined. The highest correlations were found between 4(5)‐MI levels and the amount of caramel colorant and pH values (r² = 0.9712, r² = 0.9378). The concentration of caramel colorants in 8 commercial soy sauces were estimated, and ranged from 0.01 to 1.34% (v/v).     

给水处理中活性炭吸附性能筛选的新指标——焦糖脱色率研究

对给水处理中活性炭吸附水中有机物的性能筛选指标进行研究,由于测定活性炭焦糖脱色率时所用焦糖的分子质量分布与天然水中有机物的分子质量分布相似,故提出用焦糖脱色率评价给水处理用活性炭的吸附性能.经试验证实,以焦糖脱色率评价活性炭吸附性能的试验结果与DL/T 582-2004(以腐殖酸、富里酸、木质素、丹宁进行评价)的结果相同.建议用于给水处理的活性炭焦糖脱色率＞50％.     

耐酸型焦糖色素制备工艺的研究

对以葡萄糖为原料,复合氨基化合物为催化剂制备耐酸型焦糖色素的工艺进行了研究,在单因素实验基础上,通过正交实验得出较好的工艺条件为糖液浓度60%、保温温度145℃、保温时间3h、催化剂用量5%,得到色率达163626,带负电荷的耐酸焦糖色素产品。