氢化物原子荧光光谱法测定酱油中微量铅的方法研究

建立了一种快速、高效的QuEChERS-高效液相色谱-质谱联用法（QuEChERS-HPLC-MS/MS）测定谷类杂粮制品中脱氧雪腐镰刀菌烯醇（DON）、3-乙酰脱氧雪腐镰刀菌烯醇（3-ADON）、15-乙酰脱氧雪腐镰刀菌烯醇（15-ADON）和玉米赤霉烯酮（ZON）共4种真菌毒素。样品前处理采用乙腈-水溶剂提取，经Florisil+C18+无水硫酸镁净化后检测。以0.10%甲酸-乙腈作为流动相，在质谱检测器的多反应监测模式下进行分析。结果表明，4种真菌毒素在各自的线性范围内线性关系良好，相关系数R2均大于0.999，回收率在85.1%～102.0%，相对标准偏差（RSD）为2.11%～6.22%。该方法具有前处理简单、净化效果好、灵敏度高和检测速度快的优点，适用于谷类杂粮制品中DON、3-ADON、15-ADON 和ZON的分析和定量检测。     

An experience of tunnelling in mudstone area in southwestern Taiwan

Many tunnels will be constructed in southwestern Taiwan in the upcoming decade to meet the huge demands of transportation, energy and water infrastructure projects. Mudstone strata cover more than a 1000 km² area, consisting mainly of massive mudstone or alternation of mudstone and sandy layer, exhibiting unfavorable geological and hydrological characteristics, making it extremely difficult for tunnelling. This paper presents the lessons learned from three tunnelling projects in the 1990s in a mudstone area. In addition to discussing the rock behavior in the vicinity of tunnel and its failure patterns, the monitoring data during tunnelling are presented as well. Finally, the effective method of design and construction are recommended for tunnelling in mudstone area.     

侯马冶炼厂奥斯麦特熔炼炉炉渣恶化的处理

介绍侯马冶炼厂奥斯麦特熔炼炉3次炉渣恶化的原因，采取的措施和结果。粉煤灰积存，生料堆积和风料比失当造成炉渣SiO2含量升高，Fe含量降低是炉渣恶化的主要原因，添加高铁造渣成分调整渣组成或不加料浸沿喷枪正常熔炼状态操作，将生料中的铁氧化造渣，提高炉温，改善炉渣性质，使炉况恢复正常。     

KCl与NaCl在低盐固态法酱油发酵中的应用比较

对KCl与NaCl在低盐固态酱油发酵中的应用进行了比较研究。结果表明：用KCl代替NaCl，KCl的浓度要高于NaCl才能抑制发酵期间杂茵的污染，且使用KCl的发酵效果比NaCl要好。     

Some results on generalized residual entropy

Shannon’s entropy plays an important role in the context of information theory. Since this entropy is not applicable to a system which has survived for some units of time, the concept of residual entropy has been developed in the literature. Here we generalize the residual entropy by choosing a convex function ? with ?(1) = 0. In this paper, some orderings and aging properties have been defined in terms of the generalized residual entropy function and their properties have been studied. Quite a few results available in the literature have been generalized and some distributions (viz. uniform, exponential, Pareto, power series, finite range) have been characterized through the generalized residual entropy.     

可焊性高强度钢筋的开发与生产

为进一步开发国际钢材市场，研制开发了符合加拿大可焊性高强度钢筋标准要求的高强度钢筋．制定了化学成分及力学性能内控标准，分析了生产工艺各环节对成分和性能的影响，依据试验结果，在全面统计分析的基础上，调整了冶炼成分，生产的531批钢筋全部合格．通过直方图及回归分析，说明了制定的产品生产工艺可行，也为今后的生产提供了理论依据。     

考虑抗力退化的公路钢筋混凝土梁抗弯强度可靠性分析

本文采用了一个时变荷载模型和一个考虑了钢筋锈蚀，钢筋屈服拉力，混凝土抗压强度和粘结力等多个影响因素的多参数抗力劣化模型，对公路钢筋混凝土梁抗弯强度可靠性在服役期内的变化趋势进行了研究，并针对一实例对各影响参数对可靠性分析的敏感性进行了分析。     

芝麻辣酱的制作

本文探讨了在黄酱的基础上，加入芝麻、辣椒等各种辅料，配制出芝麻香味浓郁、辣味适中的芝麻辣酱。本文对原材料的配方、主要生产设备、生产工艺流程、原材料处理、生产过程中的操作要点及质量标准等多方面进行了详细论述。     

Physiological deterioration of cassava roots

Rapid post-harvest physiological deterioration of cassava roots (Manihot esculenta Crantz) appears to be due essentially to wound responses, comparable to those observed in other plant storage organs. The wound responses observed include: increased activity of phenylalanine ammonia lyase, an enzyme associated with phenol biosynthesis; increased activity of peroxidase and polyphenol oxidase; formation of phenols/polyphenols including leucoanthocyanidins, catechins, sco-poletin and condensed tannins, and often the formation of a wound periderm. In cassava, the responses did not remain localised at wound surfaces in roots when held at low storage humidity but spread through the roots causing a discolouration of the vascular tissue and storage parenchyma. Roots stored at high humidity showed a more typical wound response with localised production of phenols and periderm formation.     

对我国酱油酿造几项新技术应用之浅见

本文概述了三十年来我国酿造酱油工业开展研究的六项新技术在现阶段的投产可行性，及进一步研究方向的看法。