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排序方式: 共有758条查询结果,搜索用时 250 毫秒
1.
New HPLC Method to Determine Ethyl Carbamate in Alcoholic Beverages Using Fluorescence Detection 总被引:2,自引:0,他引:2
ABSTRACT: A new methodology to the quantification of ethyl carbamate (EC) has been developed. This method allows the analysis by HPLC of ethyl carbamate in samples of wine, fortified wine, and wine brandy, by a pre-column derivatization with 9-xanthydrol, and fluorescence detection. This does not require previous sample extraction or concentration. The method presents an average recovery of 96% among samples studied, a detection limit of 4.2μg/L, and an average intermediate precision of 6.3%. The comparison of the results obtained for EC analysis on the same wine brandy samples by GC/MS and HPLC are statistically indistinguishable with 97.5% probability. The results of the analysis of 42 samples are presented. 相似文献
2.
Sex phermone components of mulberry looper,Hemerophila atrilineata butler (lepidoptera: Geometridae)
Zhong-Xing Tan Regine Gries Gerhard Gries Guo-Qiang Lin Guan-Qin Pu Keith N. Slessor Jianxiong Li 《Journal of chemical ecology》1996,22(12):2263-2271
(6Z-9S, 10R)-Epoxy-octadecene (SR-1) and (3Z, 6Z-9S, 10R)-epoxy-octadecadiene (SR-2) are sex pheromone components of the mulberry looper (MBL),Hemerophila atrilineata Butler. Compounds extracted from female MBL pheromone glands were identified by coupled gas chromatographic-electroantennographic detection (GC-EAD) and GC-mass spectrometry. In field experiments in China,SR-2,RS-2, or both combined were hardly attractive, butSR-2 in combination withSR-1 attracted significant numbers of MBL males. Synergistic behavioral activity ofSR-1 plusSR-2, but not of corresponding antipode mixtures, indicates enantiospecificity of MBL pheromone communication. Because blends of racemic and enantiospecific (SR)1 plus2 were similarly attractive, racemic1 plus2 may have potential for mass trapping or confusion of MBL males in commercial mulberry plantations. 相似文献
3.
桑叶天然染料的萃取和稳定性研究 总被引:2,自引:0,他引:2
采用正交实验法及单因子实验法,有效地萃取桑叶染液并对其稳定性进行了研究和探讨。发现桑叶的水萃取液和盐酸萃取液的光吸收曲线相似。桑叶天然染料萃取的最大影响因子是萃取剂的种类,有效的萃取剂在本试验中是氢氧化钠,其萃取液的色浓度、光密度值大,氢氧化钠最佳浓度为20%。三种萃取液的光稳定性和抗还原性能均较好,其中H2O和HCl萃取液的抗氧化性能较弱,而NaOH萃取液的稳定性则较好,并且均可在一定的条件下保存几天,因此一次萃取一定量的桑叶染液可供给几天染色用,减少了提取桑叶染液的次数,节约了时间、劳力及能耗,有利于桑叶染料实用化的进程。 相似文献
4.
测试结果显示,柞桑双绉与桑丝双绉在设计技术参数上的不同,导致了这两种织物的外观及使用性能的差异。 相似文献
5.
Huali Hu Wenbiao Shen Pengxia Li 《International Journal of Food Science & Technology》2014,49(2):399-409
Here we investigated the effect of hydrogen sulphide (H2S) on postharvest quality of mulberry fruit and possible underlying mechanisms. Endogenous H2S content first increased after harvest and then decreased sharply with the process of ripening and senescence. A fumigation with H2S released from 0.8 mm NaHS solution could significantly enhance the endogenous H2S content by increasing the activities of D‐cysteine desulfhydrase and L‐cysteine desulfhydrase. NaHS could significantly slow down the ripening rate of mulberry fruit and reduce the respiratory intensity and anthocyanin content. Moreover, H2S fumigation was able to obviously delay or slow down the decreases in soluble protein, titratable acidity and ascorbate contents. Further results showed that activities of representative antioxidant enzymes in H2S‐treated sample were higher than those of control samples during storage, resulting in a decrease in superoxide anion production. Together, these results clearly indicate that H2S fumigation has a potential role in the preservation of mulberries. 相似文献
6.
Microencapsulation of bioactive compounds from mulberry (Morus alba L.) leaf extracts by protein–polysaccharide interactions
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Methavee Peanparkdee Satoshi Iwamoto Chaleeda Borompichaichartkul Kiattisak Duangmal Ryo Yamauchi 《International Journal of Food Science & Technology》2016,51(3):649-655
Mulberry leaf extracts were generated using four concentrations of ethanol (50%, 60%, 70%, and 95% v/v). A 60% ethanolic mulberry leaf extract (60E) yielded a high total phenolic content (TPC) and antioxidant activity using 1, 1‐diphenyl‐2‐picrylhydrazyl (DPPH) radical scavenging and a ferric reducing antioxidant power (FRAP) assay. Coating materials were derived using a combination of soy protein isolates (SPI) and low methoxyl (LM) pectin in a 1:1 ratio. The effect of various parameters on microencapsulation, such as pH (3.5, 4.0, and 4.5) and the concentration of coating materials (2.5, 5.0 and 7.5% w/v), was studied. Microcapsules produced using 60E as a core material at pH 4.0 with 7.5% of coating material showed a high encapsulation yield, encapsulation efficiency, TPC and antioxidant activity. 相似文献
7.
近年来,蛋白质与多酚类物质的相互作用是食品领域的研究热点之一,两者的结合受到多种因素的影响,其中pH值是重要的影响因子。该文研究了不同pH值条件下桑椹多酚(Mulberry Polyphenols,MP)对乳清蛋白(Whey Protein,WP)理化性质和功能特性的影响。结果表明,桑椹多酚改变了复合蛋白粉的色泽、粒径大小和Zeta电位。同时,还提高了乳清蛋白的溶解性、乳化性能,在pH值3.0时乳清蛋白的乳化能力和乳化稳定性分别达到7.23 m2/g prot和89.56%,较对照组分别提高了2.66%和1.21%。通过高效液相色谱法对桑椹多酚-乳清蛋白粉中的单体酚类进行定量分析,在pH值5.0和7.0条件下结合的单体酚含量比pH值1.0和3.0高。此外,较空白对照组而言,添加桑椹多酚提高了乳清蛋白的DPPH自由基清除率、ABTS+自由基清除能力和FRAP还原能力,最高分别达到89.28%、81.70%和530.95μmol/g prot。综上所述,利用动物蛋白结合植物多酚是创新功能食品组分的手段,反应体系的pH值对结合效率有重要影响,为今后... 相似文献
8.
该研究通过研究桑椹酒渣中的酚类化合物,为开发酒渣的价值提供一定的理论基础和数据支撑。建立云桑二号桑椹酒渣中的酚类化合物的高效液相色谱-四极杆飞行时间串联质谱法(HPLC-Q-Time-of-Flight Mass Spectrometry,HPLC-Q-TOF-MS)定性分析方法。液相色谱使用ZORBAX SB-Aq(2.1 mm×100 mm,1.8-Micron)色谱柱,流动相为乙腈和0.1%(V/V)甲酸水溶液,梯度洗脱,采用ESI离子源在负离子模式进行质谱检测。最终鉴定出云桑二号桑椹酒渣中酚类物质共14种。然后利用标准品对照高效液相色谱法(High Performance Liquid Chromatography,HPLC)对高效液相色谱-四极杆飞行时间串联质谱法鉴定出的多酚类化合物进行了定量测定,发现桑椹酒渣中的酚类物质组成与桑椹大致相同。但各单体酚含量总体降低。其中,花青素类酚类物质含量最高的是天竺葵素-3-葡萄糖苷(718.30μg/g),非花青素类多酚物质含量最高的是儿茶素(1 805.87μg/g)。这些结果表明桑椹酒渣酚类含量丰富,是开发健康食品的良好原料。 相似文献
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