An enhanced,acoustic emission-based,single-fiber-composite test

In the single-fiber-composite (SFC) test, a fiber imbedded in a matrix is loaded in tension, resulting in a fragmentation of the fiber. In the conventional version of this test, the final fiber fragmentation length distribution is used with a micro-mechanical model to determine the average fiber/matrix interfacial shear stress. In the enhanced version of this test, one also determines the applied stress at each fiber fracture, and from this, one can evaluate the strength of the fiber at short gage lengths. In our measurement system, we utilize an acoustic emission (AE) technique to detect the fiber fractures and to locate the fiber breaks and so determine both the fiber failure stresses as well as the fiber fragmentation lengths while the test is in progress. Critical to the success of this test is a broadband AE system that utilizes point-like AE sensors, procedures for evaluatingin situ, the wavespeed of the first wave arrival and signal processing techniques for determining the arrival time of this signal as precisely as possible for a broad range of wave shapes. Here we describe the application of such an enhanced SFC test procedure to investigate the failure of a Nicalon fiber in an epoxy matrix.     

三轴应力下盐岩声发射特征研究（研究生论坛稿件）

利用MTS815 Flex Test GT岩石力学试验系统和PCI–2声发射(AE)三维定位实时监测系统,开展不同围压下盐岩的三轴压缩声发射定位试验,探讨盐岩轴向加载过程中声发射特征的围压效应。研究结果表明：盐岩AE定位点多少与振铃计数率大小、能率高低具有良好的一致性。声发射高计数、高能率、定位点集聚段等随围压增加而滞后。低围压下,盐岩发生剪切破坏,高计数、高能率、AE定位点集聚段主要出现在屈服阶段和峰值应力前阶段;高围压下,盐岩呈塑性大变形特征,高计数、高能率、AE定位点集聚段主要在峰值阶段及峰后阶段出现。围压增加,累计计数和定位点的总量呈减少趋势;最大能率和累计能量随围压增加而减小,5MPa约分别为30MPa的43倍和22倍。     

UHMWPE/LDPE复合材料拉伸破坏的声发射特性研究(Ⅱ)

本文续“UHMWPE/LDPE复合材料拉伸破坏的声发射特性研究(Ⅰ)”,进一步研究了UHMWPE/LDPE复合材料拉伸破坏的声发射特性,具体研究了[0°]、[90°]在拉伸破坏过程中声发射参数特征,并对拉伸破坏机理进行了初步的研究。     

头孢匹罗的合成

丙炔胺和环戊酮在无水乙醇中回流反应5 h生成2,3-环戊烯并吡啶,收率55%。7-氨基头孢烷酸和2-甲氧亚氨基-2-(2-氨基-4-噻唑基)-(z)-硫代乙酸苯胼噻唑酯(AE活性酯)发生酰化反应生成头孢噻肟酸,收率90%。在三甲基碘硅烷作用下,头孢噻肟酸与2,3-环戊烯并吡啶反应,生成头孢匹罗,收率65%1。H NMR对产物及中间体进行了鉴定。     

Comprehensive assessment on dynamic roof instability under fractured rock mass conditions in the excavation disturbed zone

The damage process of fractured rock mass showed that the fracture in rocks induced roof collapse in Yangchangwan Coal Mine,China.The rock mass was particularly weak and fractured.There occurred 6 large-scale dynamical roof falls in the excavation disturbed zone (EDZ) with the collapsing volume of 216 m3.First,the field detailed geological environment,regional seismic dy-namics,and dynamic instability of roadways were generally investigated.Second,the field multiple-index monitoring measurements for detecting the deep delamination of the roof,convergence deformation,bolt-cable load,acoustic emission (AE) characteristic pa-rameters,total AE events,AE energy-releasing rate,rock mass fracture,and damage were arranged.Finally,according to the time-space-strength relations,a quantitative assessment of the influence of rock-mass damage on the dynamic roof instability was accomplished.     

基于自编码和知识蒸馏的表面缺陷检测方法

针对传统的表面缺陷检测方法只能对具有高对比度或低噪声的明显缺陷轮廓进行检测的问题,提出了一种基于自编码和知识蒸馏的表面缺陷检测方法来准确定位和分类从实际工业环境捕获的输入图像中出现的缺陷。首先,设计了一种级联自动编码器（CAE）架构用于分割和定位缺陷,其目的是将输入的原始图像转换为基于CAE的预测蒙版;其次,利用阈值模块对预测结果进行二值化以获得准确的缺陷轮廓;然后,把缺陷区域检测器提取并裁剪出来的缺陷区域视为下一个模块的输入;最后,将CAE分割结果的缺陷区域通过知识蒸馏进行类别分类。实验结果表明,与其他几种表面缺陷检测方法相比,所提出的方法综合性能最好,其缺陷检测平均准确率为97.00%。该方法能够有效地对较小的、边缘不清晰的缺陷进行分割,满足对物品表面缺陷实时分割检测的工程要求。     

Mechanical behavior and failure analysis of brittle sandstone specimens containing combined flaws under uniaxial compression

Based on the axial stress-axial strain curves, the effect of fissure angle on the strength and deformation behavior of sandstone specimens containing combined flaws is analyzed. The mechanical parameters of sandstone specimens containing Combined flaws are all lower than that of intact specimen, but the reduction extent is distinctly related to the fissure angle. The results of sandstone specimens containing combined flaws are obtained by the acoustic emission, which can be used to monitor the crack initiation and propagation. The ultimate failure mode and crack coalescence behavior are evaluated for brittle sandstone specimens containing combined flaws. Nine different crack types are identified on the basis of their geometry and crack coalescence mechanism （tensile crack, hole collapse, far-field crack and surface spalling） for combined flaws. The photographic monitoring was also adopted for uniaxial compression test in order to confirm the sequence of crack coalescence in brittle sandstone specimens containing combined flaws, which recorded the real-time crack coalescence process during entire deformation. According to the monitored results, the effect of crack coalescence process on the strength and deformation behavior is investigated based on a detailed analysis for brittle sandstone specimens containing combined flaws by using digital photogrammetry.     

计算机辅助声发射源检测定位系统

针对普通声发射（ＡＥ）检测仪缺乏源定位功能，开发了计算机辅助ＡＥ源检测定位系统，并详细论述了该系统的组成、接口、源定位算法和程序、剔除噪声等问题     

Mechanical properties and microstructures of hot extruded AE42 alloy with addition of zinc

Mechanical properties and microstructures of AE42 magnesium alloy with addition of Zn and subjected to hot extrusion at 370 ℃ and an extrusion ratio of 8：1 were investigated. The results show that for the AE42 alloy, the addition of Zn can obviously improve its elongation as well as the ultimate tensile and yield strengths below 150 ℃. The addition of Zn can refine the mierostructure of the AE42 alloy, and result in the precipitation of Mg17Al12 and MgZn2 phases. Due to the addition of Zn to the AE42 alloy, the amount of Al11RE3 phase decreases, while the Al11RE3 phase becomes short rod-shaped from acicular and block, and distributes along the grain boundaries, which will have a stronger effect on the tensile properties of the alloy at elevated temperature. In addition, with the presence of MgZn2 precipitates, the sliding of grain boundaries is restrained and the strength of the alloy gets enhanced.     

基于One-Shot聚合自编码器的图表示学习

自编码器（AE）是一种高效的图数据表示学习模型,但大多数图自编码器（GAE）为浅层模型,其效率会随着隐藏层的增加而降低。针对上述问题,提出基于One-Shot聚合（OSA）和指数线性（ELU）函数的GAE模型OSA-GAE和图变分自编码器模型OSA-VGAE。首先,利用多层图卷积网络（GCN）构建编码器,并引入OSA和ELU函数;然后,在解码阶段使用内积解码器恢复图的拓扑结构;此外,为了防止模型训练过程中的参数过拟合,在损失函数中引入正则化项。实验结果表明,OSA和ELU函数可以有效提高深层GAE的性能,改善模型的梯度信息传递。在使用6层GCN时,基准引文数据集PubMed的链接预测任务中,深层OSA-VGAE相较于原始的VGAE在ROC曲线下的面积（AUC）和平均精度（AP）上分别提升了8.67和6.85个百分点,深层OSA-GAE相较于原始的GAE在AP和AUC上分别提升了6.82和4.39个百分点。