实验室的质量监督(上)

质量监督是实验室保持人员能力,进行自我完善,日常渐进的重要手段,是持续改进的重要组成部分,也是实验室管理工作的难点,本文给出质量监督的目的、对象、方法、记录等.     

低渗透率地层渗透率的确定方法

结合大庆油田外围低渗透率地层的地质特点,根椐渗流理论和岩心分析资料,分析了地层渗透率与孔隙度、组成地层的各种矿物含量以及泥质含量之间的关系,建立了不同矿物组合地层的渗透率计算方程。用本方法计算的和岩心分析的渗透率进行了对比,二者之间具有较好的一致性。     

Numerical simulation of typical contact situations of brake friction materials

In the paper, a model typical for contact situations of automotive brakes is established based on the method of movable cellular automata. The processes taking place at local contacts in an automotive brake system are analysed. Based on microscopic and micro-analytical observations, the following contact situations were simulated: (i) a couple of ferritic steel against pearlitic steel, both covered by an oxide layer mixed with graphite nanoparticles and (ii) the same situation but without oxide layers. The results of calculated mean coefficients of friction of the oxide-on-oxide contact correspond well to expected values for a real braking system, whereas steel-on-steel contact are twice as high. This allows one to make some conclusions; for example, oxide formation will take place more quickly than friction layer elimination, and finally this is responsible for the stabilisation of the coefficient of friction.     

Preparation of CeO2-ZrO2 mixed oxide with high surface area and high thermal stability

Ceria-zirconia solid particles have been recognized as a key material of the automotive exhaust catalysts since they can release and uptake oxygen owing to the rapid reversible oxidation states of cerium between Ce³⁺ and Ce⁴⁺. Several methods have recently been described to prepare the CeO₂-ZrO₂ solid particles used in the catalysts. In this paper, a new coprecipitation method is used to prepare the CeO₂-ZrO₂ solid particles. The Ce-Zr alcogel is dried and calcined in flowing N₂ not in flowing air under atmospheric pressure. The results show that the ceria-zirconia sample calcined at 650 °C has high surface area over 90 m²g⁻¹, which drops to 40 m²g⁻¹ following treatment at 900°C.     

Numerical simulation of flying phenomena of the running tape on rotating drum

This paper analyzes the running mechanism of flexible and thin tape above rotating protrusion through a numerical simulation. The scope of analysis is confined to the phenomena of elastohydrodynamic lubrication between the rotating drum with a protrusion and the running tape. This model is based on the modified Reynolds equation and the equation of plate considering the effect of geometric nonlinearity and geometry of protrusion. Finite element method of Bubnov-Galerkin type is adopted as a numerical simulation technique to solve the above two coupled nonlinear equations. In numerical simulation, the influences of tape tension and protrusion velocity are evaluated in simple model. In complex models, the reciprocal action of two protrusions is simulated.     

钻速模式动态辨识方法研究

目的：钻进过程是一个复杂的工艺过程，影响钻速的因素错综复杂。为钻井参数优化和实时控制，提出钻速动态模型。方法：对影响钻速的因素进行分析，用系统辨识方法建立钻速模式。结果：利用该方法建立了华北油田岔河集地区的钻速模型，取得满意结果。结论：此动态钻速模式能更准确、科学地描述钻进过程，并在钻井参数最优化、钻井过程的闭环控制等方面具有广阔的应用前景。     

盖层封闭能力的灰聚类评价方法

提出灰聚类评价方法，用于盖层封闭能力定量评价。所有被评价对象构成聚类对象集，所有评价指标构成评价指标集，所划分的盖层封闭能力等级构成聚类的灰类集，按照最大聚类权确定对象所属的灰类，即盖层的封闭能力级别。评价流程是：确定指标灰类模式→数据预处理→利用聚类公式计算→利用最大聚类权准则抉择。这种方法避免了加法评分法要依靠人的主观经验划定总评分值的问题，而且由于把评价对象视为“灰”的，具有处理边缘信息的能力。以琼东南盆地３个主要探区的盖层封闭性评价为例，介绍了灰聚类评价的具体应用方法。灰聚类评价方法同样可用于储集层评价、圈闭评价等地质问题的定量研究。表２参３（王孝陵摘     

利用先进的结构试验系统进行发动机构件的仿真疲劳试验

本文介绍一套先进的构件实验设备的功能及其在发动机构件疲劳试验方面的具体应用实例．通过对几种受力较复杂构件的受力分析设计出实验方法，使构件在实验室中受力情况与构件实际受力情况相似或相同，这样，得出的试验数据就可为构件的可靠性分析工作提供较好的依据．     

A scheme to randomly generate surface dust points for the 3D complex variable boundary element method (CVBEM)

A scheme to randomly generate dust points on the surface of a three-dimensional (3D) object is proposed. This scheme will potentially eliminate the bias of a density of points which are approximately equally spaced on the surface, as well as eliminate possible weighting requirements for areas of higher density. This method has the potential to reduce computational effort, as fewer points might be required to define the surface area. The global trial function vector can be assigned to these dust points and then entered into the complex variable boundary element method (CVBEM) commercial code. This scheme can be applied to each piece of a system that is comprised of a connected multiple geometry. A noticeable benefit of this approach is that the same problem can be studied several times, using a new random distribution of surface points each time. The smallest error can then be determined and that run selected. The Mathematica code used to generate the scheme is attached as an appendix.     

THE USE OF TRANSMISSION AND TRANSFLECTANCE NEAR INFRARED SPECTROSCOPY FOR THE ANALYSIS OF BEER

Both transmission and transflectance near infrared spectroscopy have been evaluated for the rapid analysis of beer components. Results of sufficient accuracy have been obtained for ethanol content and Original Gravity. Application of a first derivative mathematical treatment on the spectral data improved calibration equations. Better accuracy was achieved using the transmission mode compared to that using the transflectance mode.