测定钠中杂质的手动阻塞计的研究

文章介绍了测定钠中杂质浓度的手动阻塞计的原理、装置和实验结果。为了减少测量误差,我们研究了影响准确测定阻塞温度的因素,并且找到了减少测量误差的办法。在同样的杂质饱和温度下,该阻塞计测得的高、低阻塞温度所对应的杂质浓度差是很接近的。对氧其差值为1.03ppm;对氢为0.0763ppm。     

High temperature controlled atmosphere experiments for catalysts in a transmission electron microscope

A new transmission electron microscopy (TEM) specimen preparation procedure for high temperature experiments using a controlled atmosphere specimen holder (HTCASH) has been developed. It is designed for studying the microstructure of catalyst specimens before and after treatments in various gases. The procedure involved (1) finding a new formula for the embedding material, (2) devising a new method of making specimen supports, and (3) developing a method for removing the embedding material after the specimen has been microtomed. These techniques were then brought together to produce the ideal specimens for the HTCASH experiments. As an extra benefit, this procedure is also suitable for preparing specimens for ultrahigh resolution imaging experiments. The application of the new procedure in HTCASH experiments is illustrated through a high temperature reduction of a Co/SiO₂-923 catalyst.     

高压变频器在煤气加压机中的应用

2005年11月份邯郸钢铁厂8万煤气柜外送煤气加压机采用高压变频技术改造。其原因是该加压机外送量波动较大，采用普通阀门调节打回流，将会浪费大量电能，采用变频技术改造后，节能效果非常明显。     

Preparation of CeO2-ZrO2 mixed oxide with high surface area and high thermal stability

Ceria-zirconia solid particles have been recognized as a key material of the automotive exhaust catalysts since they can release and uptake oxygen owing to the rapid reversible oxidation states of cerium between Ce³⁺ and Ce⁴⁺. Several methods have recently been described to prepare the CeO₂-ZrO₂ solid particles used in the catalysts. In this paper, a new coprecipitation method is used to prepare the CeO₂-ZrO₂ solid particles. The Ce-Zr alcogel is dried and calcined in flowing N₂ not in flowing air under atmospheric pressure. The results show that the ceria-zirconia sample calcined at 650 °C has high surface area over 90 m²g⁻¹, which drops to 40 m²g⁻¹ following treatment at 900°C.     

Schwingfestigkeit von Schraube‐Mutter‐Verbindungen

High cycle fatigue of bolted connections Extensive tests regarding the influences on the fatigue of bolt‐nut‐connections of preloading with torsion, of preloading with yielding, of loading with superimposed bending and of the tested lot are processed. These influences are not yet known according to VDI 2230. New testing devices were designed for these tests, which allow a far less expensive operation and may easily be used for bolts of diameters up to M100 and testing frequencies up to 1000 Hz. The validity of fatigue resistance according to VDI 2230 is specified with respect to the test results. The determined influence of the tested lots is unexpectedly high. The manufacturing process of bolts should be improved to minimize this influence.     

宝鸡市医用诊断X线照射频度调查

本文报道从1984年6月1日至1985年5月31日对宝鸡市五县(区)医用诊断 X 线照射频度的调查结果。结果表明,胸透和群检胸透医照率最高,占医疗照射总人次数的68.7%,门诊医照率为70.8人次/千人·年,人群受照率为344。5人次/千人·年。按年龄比较,青壮年组医照率最高,占医照总人次数的57.2%。按性别比较,男性多于女性。     

导磁不锈钢毛的结构化研究

研制了一种新型的结构化钢毛——胶结钢毛。和传统的普通钢毛相比,胶结钢毛具有很强的结构刚度和很低的钢毛流失量;同时,对高岭土有较高的除铁效率。     

粘土作为高放废物处置回填材料的可行性研究

本文以西北粘土为对象,对其压实行为、热传导、膨胀特性,以及吸附和渗透性能进行了初步研究,借以探讨西北粘土在高放废物处置中用作回填材料的可行性。试验表明,以西北粘土为基材,经过适当的热改性和吸附改性,在初始含水量约为9%,于70MPa 下成型,用作高放废物处置中的回填材料是可行的。     

Two-level optimal output feedback stabilizer design

The paper addresses the design of two-level power system stabilizers using an optimal reduced order model whose state variables are torque angles and speeds. The reduced order model retains their physical meaning and is used to design a two-level linear feedback controller that takes into account the realities and constraints of electrical power systems. The two-level control strategy is used, and a global control signal is generated from the output variables to minimize the effect of interactions. The effectiveness of this controller is evaluated and a multimachine system is given as an example to illustrate the advantages of the proposed method. Responses of the system with a two-level scheme and an optimal reduced order scheme are included for comparative analysis.     

简易高性能纳秒脉冲发生器

为了实现电子散射飞行时间谱仪电子束的脉冲化及产生时一幅变换器的启动或停止信号。我们利用开关晶体管的雪崩特性研制了一个性能好，成本低的纳秒脉冲发生器。该发生器输出上升时间好于Ｉｎｓ，幅度达１０Ｖ的负尖脉冲，用作时一幅变换器的启动或停止信号；也输出上升时间约３ｎｓ，幅度５－３０Ｖ连续可调和宽度５－２３０ｎｓ可调的正脉冲，用作电子束脉冲化的调制信号，脉冲重复率为１５０×１０＾３ｓ＾－１。它可广泛用于类似