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1.
Ferrite particles coated with biocompatible phases can be used for hyperthermia treatment of cancer. We have synthesized substituted
calcium hexaferrite, which is not stable on its own but is stabilized with small substitution of La. Hexaferrite of chemical
composition (CaO)0.75(La203)0.20(Fe2O3)6 was prepared using citrate gel method. Hydroxyapatite was prepared by precipitating it from aqueous solution of Ca(NO3)2 and (NH4)2HPO4 maintaining pH above 11. Four different methods were used for coating of hydroxyapatite on ferrite particles. SEM with EDX
and X-ray diffraction analysis shows clear evidence of coating of hydroxyapatite on ferrite particles. These coated ferrite
particles exhibited coercive field up to 2 kOe, which could be made useful for hysteresis heating in hyperthermia. Studies
by culturing BHK-21 cells and WBC over the samples show evidence of biocompatibility. SEM micrographs and cell counts give
clear indication of cell growth on the surface of the sample. Finally coated ferrite particle was implanted in Kasaulli mouse
to test its biocompatibility. The magnetic properties and biocompatibility studies show that these hydroxyapatite coated ferrites
could be useful for hyperthermia. 相似文献
2.
1 Influence of PAMAon Boundary Fil mFormation and Friction1.1 Experi mental methodsUltra-thin optical interferometry has been used tostudy thinlubricating fil ms for more than a decade and theexperi mental details of this technique have been reportedpreviously[1].The principle of the test setup is shown inFigure1.A polished steel ball is loaded and rolled againstthe flat surface of a glass disc that is coated with a thinsemi-reflecting chromiumlayer and a silica spacer of about500nmthickne… 相似文献
3.
H. L. Du S. R. Rose Z. D. Xiang P. K. Datta X. Y. Li 《Materialwissenschaft und Werkstofftechnik》2003,34(4):421-426
The oxidation/sulphidation behaviour of a Ti‐46.7Al‐1.9W‐0.5Si alloy with a TiAl3 diffusion coating was studied in an environment of H2/H2S/H2O at 850oC. The kinetic results demonstrate that the TiAl3 coating significantly increased the high temperature corrosion resistance of Ti‐46.7Al‐1.9W‐0.5Si. The SEM, EDX, XRD and TEM analysis reveals that the formation of an Al2O3 scale on the surface of the TiAl3‐coated sample was responsible for the enhancement of the corroison resistance. The Ti‐46.7Al‐1.9W‐0.5Si alloy was also modified by Nb ion implantation. The Nb ion implanted and as received sampels were subjected to cyclic oxidation in an open air at 800oC. The Nb ion implantation not only increased the oxidation resistance but also substantially improved the adhesion of scale to the substrate. 相似文献
4.
5.
工业管道测厚的几点问题探讨 总被引:2,自引:0,他引:2
超声波测厚在腐蚀监测上应用越来越广泛,为让这项检测技术更准确、更可靠,充分发挥功效,文章就工业管道测厚中测厚数据处理、测厚点选择、高温问题以及其它影响因素等几个方面进行了探讨。 相似文献
6.
7.
ImprovingWearResistanceoftheNibaseThermalSprayWeldingCoatingUsingRareEarthsZhaiGuangjie(翟光杰)(InstituteofPhysics,AcademicaSi... 相似文献
8.
埋地管道涂层检测技术现状 总被引:3,自引:0,他引:3
李继华 《石油化工腐蚀与防护》1998,15(4):4-6,52
文章对各种埋地管道涂层检测技术进行了综述,并指出了各种技术的优缺点及应用前景. 相似文献
9.
利用2、4和14mm的X60钢紧凑拉伸试样进行同样应力水平、固定应力比(R=0.1)的疲劳裂纹扩展试验,揭示出高韧性管道钢的疲劳裂纹扩展存在显著的厚度效应。由于应力水平低,相应的离面应力也低,不足以导致分层开裂,因此,裂纹端部的三维应力约束随厚度增加而增大。4mm试样的疲劳裂纹速率远高于2mm试样,但厚度再增大,裂纹扩展速率不再有显著变化。进一步对表面裂纹试样进行疲劳裂纹扩展试验,并用勾线法纪录裂纹扩展情况,利用穿透裂纹的da/dN-ΔK曲线预测表面裂纹扩展,用2mm厚试样的数据控制裂纹表面长度的扩展,用14mm厚试样的数据控制裂纹底部沿厚度方面的扩展,得到了与表面裂纹扩展实验吻合很好的预测结果。 相似文献
10.
Novel polyurethane insulating coatings were prepared from the reaction of glycerin‐terminated polyurethane prepolymers (GPUPs) and a blocked isocyanate curing agent (BIC). The GPUPs were prepared from the reaction of one equivalent of polycaprolactone polyol (CAPA 210) with an excess amount of 4,4′‐methylene bis(phenyl isocyanate) (MDI) and subsequent reaction of the NCO‐terminated polyurethane with glycerin. The BIC was prepared from the reaction of trimethylol propane (TMP), toluene diisocyanate (TDI) and N‐methylaniline (NMA). The polyols and curing agent were characterized by conventional methods while the curing condition was optimized via gel content measurements. The curing kinetics of the polyurethane coating were investigated and the kinetic parameters derived. The crosslink densities of the samples were determined via the equilibrium swelling method, using the Flory–Rehner equation. The relationships between the crosslink density and the electrical, physical, mechanical and dynamic mechanical properties of the coatings were also studied. Copyright © 2005 Society of Chemical Industry 相似文献