两种塑性变形加工1060纯铝的组织和性能研究

采用等通道角挤压变形和累积叠轧焊两种大塑性变形方法对1060纯铝进行了加工，研究分析了纯铝在加工后的微观组织和力学性能变化和规律。结果表明：在相同的累积变形条件下，ARB和ECAP都能实现材料的晶粒细化和力学性能改善的目的。但南于两种塑性加工方式细化晶粒的机理和加工工艺不同．所以晶粒细化程度和力学性能的改善程度有所差别。ARB法将晶粒最小可以细化到500nm左右，ECAP法能细化晶粒到大小约为1μm。     

基于免疫抗体记忆分类算法的变压器故障诊断

针对传统克隆免疫算法应用于变压器故障诊断时学习速度慢、无分类能力及抗体空间小等缺点,提出一种免疫抗体记忆分类算法。利用免疫抗体识别抗原的原理和抗体记忆功能,将克隆选择与进化算法相结合,通过学习训练抗原及附属类型信息,得到由不同类型检测集组成的故障信息库,从而在保证亲和力的同时,加快学习速度,扩大免疫搜索空间,并利用人工识别球与刺激水平的线性关系对故障类型进行快速诊断。实验结果证明,该算法具有较快的运行速度及较高的诊断准确率。     

Synergistic interaction of biocatalyst with bio-anode as a function of electrode materials

Comprehensive study was performed to understand the synergistic interaction between the biocatalyst and anode in terms of electron discharge (ED) pattern and microbial growth by varying electrode (bio-anode) materials viz., graphite, aluminum, brass, copper, nickel and stainless steel. Experiments were performed in bio-electrochemical cell consisting of three electrodes (bio-anode as working electrode, carbon rod as counter electrode and Ag/AgCl(S) as reference electrode) employing anaerobic mixed culture as anodic biocatalyst. Voltammetric and chronoamperometric analysis were used to enumerate the ED and redox reactions. Presence of higher microbial population and dominance of Gram positive bacteria with higher ED supported graphite function as a good bio-anode material. Nickel and stainless steel showed higher ED after graphite associated with dominance of Gram positive bacterial population. Although higher ED was noticed with brass, metal oxidation and decrement in ED with time doesn’t support its function as bio-anode. In spite of higher ED than nickel and stainless steel, aluminum and copper showed significant metal oxidation leading to change in both physical and electrochemical properties along with dominant growth of Gram negative bacteria. This study gives a comprehensive idea on biocatalyst interaction with anode in extracellular electron transfer which is important in improving the anode performance. Juxtaposing the results, it can be deduced that the outcome of the present study can be extended to all bio-electrochemical systems including microbial fuel cell (MFC).     

Hydrogen storage in bulk Mg-Ti and Mg-stainless steel multilayer composites synthesized via accumulative roll-bonding (ARB)

We have tested the hydrogen storage cycling behavior of bulk centimeter-scale magnesium - titanium and magnesium - stainless steel multilayer composites synthesized by accumulative roll-bonding (ARB). Roll-bonding of either titanium or stainless steel with magnesium allows the reversible hydrogen sorption of the resulting composite at 350 °C. Identically roll-bonded pure magnesium can hardly be absorbed at this temperature. In the composites, the kinetics of the first cycle of absorption (also called “activation”) improves with increased number of fold and roll (FR) operations. With increasing FR operations the distribution of the Ti phase is progressively refined, and the shape of the absorption curve no longer remains sigmoidal. Increasing the loading amount of the second phase also accelerates the kinetics. This holds true up to a threshold limit. Microscopy analysis performed on 1-2 wt.% hydrogen absorbed composites demonstrates that MgH₂ formed exclusively on various heterogeneous nucleation sites. During activation, MgH₂ nucleation occurred at the Mg-hard phase interfaces. During the subsequent absorption cycles, heterogeneous nucleation primarily occurred in the vicinity of “internal” free surfaces such as cracks.     

轧制温度和累积应变对累积叠轧焊AZ31镁合金板材组织和性能的影响

通过光学显微镜（OM）、扫描电镜（SEM）和力学性能检测,研究了AZ31镁合金在不同温度和累积应变条件下累积叠轧后的微观组织和力学性能。结果表明：晶粒尺寸随累积叠轧温度降低和累积应变增加而减小;经过3道次的ARB变形后,晶粒细化不再显著,但是组织均匀性得到改善。300℃以上的ARB变形对AZ31板材的强度和延性均有一定...     

TA1/Q235循环累积变形复合界面的特性

借助金相显微镜、能谱议等手段,分析Gleeble-1500热模拟试验机循环累积变形复合后的T1/Q235复合试样的界面组织、相结构和成分变化.结果表明,T1/Q235在800℃以上900℃以下用循环累积变形复合的方法进行压制时,界面附近出现明显的过渡区域,但界面又不会有较明显的脆性相.影响结合强度.在850℃进行较低速率,多道次轧制,大的累积压下量的工艺方法,不会使结合界面处的脆性物质增加而明显降低结合强度.     

浅析层状复合板轧制新工艺

本文在对国内外层状金属复合板生产研究文献查阅分析的基础上,着重介绍了钎焊热轧法、燃烧合成轧制法、包套轧制法、PPR方法、ARB方法、PIT方法等复合新工艺基本工作原理,以及目前国内外应用各种新工艺所生产研究的新材料复合板,同时分析了复合板生产存在的问题,展望了复合板生产工艺的发展方向。     

热处理对累积叠轧Ti/Ni叠层复合材料组织与性能的影响

研究了热处理对累积叠轧多层Ti/Ni复合材料显微组织与力学性能的影响。结果表明,钛层与镍层的再结晶温度均在500 ℃左右,并且首先在界面附近的组织发生静态再结晶形核与晶粒长大现象;经200 ℃×8 h退火处理后,复合板的强度与硬度均达到最高值,此时抗拉强度为691.5 MPa,钛、镍层平均硬度分别为198.8 HV0.1和226.5 HV0.1;经500 ℃×2 h退火后,复合板断后伸长率达到最高值59.7 %。     

血管紧张素转换酶抑制剂联合血管紧张素II受体拮抗剂对糖尿病肾病肾功能临床疗效的Meta分析

目的: 评价血管紧张素转换酶抑制剂 (ACEI) 联合血管紧张素II受体拮抗剂 (ARB) 对糖尿病肾病肾功能的临床治疗效应。方法: 检索1990年1 月至2012年3月期间,国内公开发表的有关ACEI 或ARB联合及单独用药对治疗糖尿病肾病的随机对照临床试验研究文献,分析符合纳入标准的文献中有关肾功能疗效指标,并对其药物治疗前后的差值进行Meta 分析。结果: 共12项文献,包括900例糖尿病肾病患者纳入研究。Meta 分析显示,与ACEI 或ARB单独治疗组的肾功能指标相比,联合治疗组患者的 24 h 尿微量白蛋白排泄率、24 h 尿微量白蛋白和24尿蛋白定量的标准化均数合并效应量均有明显的改善 (P<0.05),而单药组和联合用药组之间的血肌酐、尿素氮和电解质则无明显改变。结论: ACEI 联合ARB治疗较单独用药治疗能明显改善糖尿病肾病患者尿蛋白的滤过作用,期待更多高质量的随机双盲对照试验提供高质量的证据。     

低压循环相变对累积叠轧TA1/Q235钢复合板结合特性影响的研究

根据工业纯钛TA1和Q235钢两种材料相变温度接近的特点,提出了利用低压循环相变预复合-累积叠轧焊制备TA1/Q235钢复合板的新方法。研究结果表明:经过热循环后的试样,在变形过程中,C、Ti原子的扩散并不限于沿垂直于界面的方向,而是可以沿任意方向随机进行的,在Q235钢界面附近没有出现柱状晶,界面附近的铁素体晶粒,从界面附近沿心部成梯度分布;采用累积叠轧焊所制备出的TA1/Q235钢复合板的结合强度得到明显改善,在复合温度为850℃、低压循环相变3次所得到的TA1/Q235钢累积叠轧焊复合板结合强度达到257.3MPa。但是,当热循环相变次数过多时,会增加金属间化合物的厚度,对结合强度产生不利影响。