Review of pulsed thermal NDT: Physical principles,theory and data processing

This paper summarizes the basics of pulsed thermal nondestructive testing (TNDT) including theoretical solutions, data processing algorithms and practical implementation. Typical defects are discussed along with 1D analytical and multi-dimensional numerical solutions. Special emphasis is focused on defect characterization by the use of inverse solutions. A list of TNDT terms is provided. Applications of active TNDT, mainly in the aerospace industry, are discussed briefly, and some trends in the further development of this technique are described.     

High areal capacitance of FeOOH-carbon nanotube negative electrodes for asymmetric supercapacitors

The relatively low capacitance of negative electrodes, as compared to the capacitance of advanced positive electrodes, poses a serious problem, since this limits the development of asymmetric supercapacitor (SC) devices with a large voltage window and enhanced power-energy characteristics. We fabricate negative SC electrodes with a high capacitance that match the capacitance of advanced positive electrodes at similar active mass loadings, as high as 37?mg?cm^?2. Cyclic voltammetry, impedance spectroscopy, galvanostatic charge-discharge data and the power-energy characteristics of the asymmetric SC device exhibit good electrochemical performance for a voltage window of 1.6?V. Our approach involves the development and application of particle extraction through liquid-liquid interface (PELLI) methods, new extraction mechanisms and efficient extractors to synthesize α-FeOOH and β-FeOOH electrode materials. The use of PELLI allows agglomerate-free processing of powders, which facilitates their efficient mixing with multiwalled carbon nanotubes (MWCNT) and allows improved electrolyte access to the particle surface. Experiments to determine the properties of FeOOH-MWCNT composites provided insight into the influence of the electrode material and the structure of extractor molecules on the composite properties. The highest capacitance of 5.86?F?cm^?2 for negative electrodes and low impedance were achieved using α-FeOOH-MWCNT composites and a 16-phosphonohexadecanoic acid (PHDA) extractor. This extractor allows adsorption on particles, not only at the liquid-liquid interface, but also in the bulk aqueous phase and can potentially be used as a capping agent for particle synthesis and as an extractor in the PELLI method.     

高性能调度技术中应用程序调度模型设计--地理空间信息网格调度技术的研究

地理空间信息网格调度技术，要比传统的高性能计算中的调度技术复杂，原因是如果将全部网格资源作为一个应用程序的调度和执行目标，必将导致通信延迟、成本昂贵、执行低效等。为此，综合考虑应用程序特性、机器特性等，研究设计了地理空间信息网格高性能调度技术中的应用程序调度模型，包括地理空间信息网格应用程序分析；资源特性分析；应用程序分解；性能预测；资源调度；机器选择；任务映射；任务调度；任务调度器和调度器管理模块。以实现为不同的应用程序匹配不同的计算资源，提高计算资源的利用率和应用程序的执行效率。     

锰铜基高阻尼合金中锌量的测定──硫氰酸盐萃取分离络合滴定法

基于甲基异丁基甲酮于稀盐酸介质中定量地萃取Ｚｎ￣（２＋）与ＣＮＳ￣－形成的络阴离子。从而达到与共存的锰、镍、铝、铬的完全分离。在有氟化物、硫脲存在时Ｆｅ￣（３＋）、Ｃｎ￣（２＋）和Ａｇ￣＋也不被萃取。有机相中的锌于ＰＨ５．５“六胺”缓冲介质中返萃取回水相，用ＥＤＴＡ滴定。在文中给定的条件下锌的一次被萃取率可达９９％以上，成功地解决了锰铜基高阻尼合金中共存离子对锌量测定的干扰问题。     

船闸直立墙基坑开挖与锚固施工程序

三峡船闸深槽开挖与锚固工程量大，工期紧，施工强度高，施工难度大。因此，合理的施工程序有利于边坡稳定和施工，是快速和高质量施工的关键。分析了永久船闸直立墙基坑开挖与锚固施工程序的复杂性和进行研究的必要性。介绍了设计阶段研究船闸开挖与锚固的施工程序。对施工过程中研究施工程序时考虑的因素，研究的主要内容以及实际采用的施工程序作了简要的分析，归纳和总结。     

Influence of accelerated ageing on methacrylate‐based denture resins heterogeneity as viewed by ESR‐spin‐probe method

The electron‐spin‐resonance (ESR) spin‐probe method, was used to study the heterogeneity of denture resins based on poly(methyl methacrylate). Results for three resins processed by microwave energy, conventional curing and cold curing (depending on the curing procedure and exposed to ageing in various environmental conditions) were compared. All three cured resins were stored over the same time (1200 h) in distilled water at ambient temperature and in artificial saliva at 348 K. The temperature‐dependent ESR spectra of a spin probe dispersed in the denture resins are analyzed in terms of line‐shapes and line‐widths. The appearance of two spectral components was taken as an indication of resin heterogeneity. The results reveal that the cold‐cured resin has a lower local density in comparison with microwave and conventionally cured resin. The amount of residual monomer also contributes to the local motion of polymer segments. The change of denture resins exposed to ageing is influenced both by the structure of the original resin and the ageing conditions. Restricted motion of a spin probe incorporated into the acrylic resins exposed to accelerated ageing suggests additional crosslinking of polymer chains. The differences are observed for all the investigated resins, but the highest change is observed with the cold‐cured resin. The ESR results are accompanied by T_g and T_m measurements. Copyright © 2005 Society of Chemical Industry     

美国国家公园申报准则及审议程序

本文所讲述的是美国国家公园服务中心在评估申请提案、制定审查方案过程中所应用的各种标准和准则 ,同时也列出了一些认识、保护未列入国家公园体系中其他重要资源的途径和方法。     

Solution of a multidimensional inverse radiation problem by means of mode reduction

The Karhunen–Loève Galerkin procedure is employed to solve an inverse radiation problem of determining the time‐varying strength of a heat source, which mimics flames in a furnace, from temperature measurements in three‐dimensional participating media where radiation and conduction occur simultaneously. The inverse radiation problem is solved through the minimization of a performance function, which is expressed by the sum of square residuals between calculated and observed temperature, using a conjugate gradient method. Through the Karhunen–Loève Galerkin procedure, one can represent the system dynamics with a minimum degree of freedom, and consequently the amount of computation required in the solution of the inverse problem is reduced drastically when the present technique is adopted. Copyright © 2004 John Wiley & Sons, Ltd.