全文获取类型
收费全文 | 6775篇 |
免费 | 631篇 |
国内免费 | 968篇 |
专业分类
电工技术 | 218篇 |
综合类 | 434篇 |
化学工业 | 1186篇 |
金属工艺 | 1421篇 |
机械仪表 | 269篇 |
建筑科学 | 195篇 |
矿业工程 | 402篇 |
能源动力 | 121篇 |
轻工业 | 355篇 |
水利工程 | 53篇 |
石油天然气 | 153篇 |
武器工业 | 99篇 |
无线电 | 721篇 |
一般工业技术 | 1954篇 |
冶金工业 | 561篇 |
原子能技术 | 75篇 |
自动化技术 | 157篇 |
出版年
2024年 | 29篇 |
2023年 | 103篇 |
2022年 | 186篇 |
2021年 | 236篇 |
2020年 | 246篇 |
2019年 | 246篇 |
2018年 | 197篇 |
2017年 | 270篇 |
2016年 | 263篇 |
2015年 | 284篇 |
2014年 | 426篇 |
2013年 | 413篇 |
2012年 | 449篇 |
2011年 | 555篇 |
2010年 | 352篇 |
2009年 | 471篇 |
2008年 | 370篇 |
2007年 | 490篇 |
2006年 | 439篇 |
2005年 | 367篇 |
2004年 | 340篇 |
2003年 | 298篇 |
2002年 | 229篇 |
2001年 | 163篇 |
2000年 | 175篇 |
1999年 | 140篇 |
1998年 | 100篇 |
1997年 | 101篇 |
1996年 | 86篇 |
1995年 | 61篇 |
1994年 | 50篇 |
1993年 | 36篇 |
1992年 | 50篇 |
1991年 | 39篇 |
1990年 | 27篇 |
1989年 | 16篇 |
1988年 | 14篇 |
1987年 | 10篇 |
1986年 | 6篇 |
1985年 | 5篇 |
1984年 | 15篇 |
1983年 | 4篇 |
1982年 | 3篇 |
1981年 | 3篇 |
1980年 | 2篇 |
1979年 | 2篇 |
1976年 | 2篇 |
1975年 | 4篇 |
1974年 | 1篇 |
排序方式: 共有8374条查询结果,搜索用时 15 毫秒
1.
Xuewu Li Lin Zhang Tian Shi Weining Yu Jinhui Shao Xuegang Zhou Yuxing He Binbin Zhang 《工业材料与腐蚀》2021,72(5):951-959
Ti-based amorphous metallic glasses have excellent mechanical, physical, and chemical properties, which is an important development direction and research hotspot of metal composite reinforcement. As a stable, simple, efficient, and large-scale preparation technology of metallic powders, the gas atomization process provides an effective way of preparing amorphous metallic glasses. In this study, the controllable fabrication of a Ti-based amorphous powder, with high efficiency, has been realized by using gas atomization. The scanning electron microscope, energy-dispersive spectrometer, and X-ray diffraction are used to analyze surface morphology, element distribution, and phase structure, respectively. A microhardness tester is used to measure the mechanical property. An electrochemical workstation is used to characterize corrosion behavior. The results show that as-prepared microparticles are more uniform and exhibit good amorphous characteristics. The mechanical test shows that the hardness of amorphous powder is significantly increased as compared with that before preparation, which has the prospect of being an important part of engineering reinforced materials. Further electrochemical measurement shows that the corrosion resistance of the as-prepared sample is also significantly improved. This study has laid a solid foundation for expanding applications of Ti-based metallic glasses, especially in heavy-duty and corrosive domains. 相似文献
2.
For the purpose of developing biodegradable magnesium alloys with suitable properties for biomedical applications, Mg–Zn–Ca–Cu metallic glasses were prepared by copper mold injection methods. In the present work, the effect of Cu doping on mechanical properties, corrosion behavior, and glass-forming ability of Mg66Zn30Ca4 alloy was studied. The experimental findings demonstrated that the incorporation of Cu decreases the corrosion resistance of alloys, but increases the microhardness and degradation rate slightly. However, the addition of a trace amount of Cu can make the samples have antibacterial properties. Therefore, Mg–Zn–Ca–Cu has great advantages in clinical implantation and is the potential implant material. 相似文献
3.
《Ceramics International》2021,47(22):31470-31475
In this study, the impact of cobalt oxide (CoO) on the structure, stability, linear and nonlinear optical parameters of B2O3–Na2O–ZnO glasses was scrutinized. A series of glass system (ZnCoNaB-glasses) was successfully prepared through the melt quenching approach. Optical absorbance, reflectance, transmittance and FTIR spectroscopy were performed for all ZnCoNaB-glasses. The FTIR results showed that the BO4 units are enhanced while nonbridging oxygens are decreased with further CoO addition. Furthermore, ZnO exists as four-coordinated [ZnO4] units and these units decreased with further doping of CoO. These structural variations produce a decreasing impact in Urbach energy and nonlinear refractive index, meanwhile enhance the glass stability. Further, the metallization criterion (M) values indicate that our glass samples can be used for a new generation of nonlinear optical glasses. The preceding results can predict that the investigated ZnCoNaB-glasses will be utilized in versatile applications; especially optical switching and computing. 相似文献
4.
Lu Xu Baijun Liu Mingyao Zhang Yang Bai Jinming Zhang Jiayin Song 《Polymer Engineering and Science》2020,60(6):1194-1201
A series of methacrylate-acrylonitrile-butadiene-styrene (MABS) resins was prepared using bulk polymerization. The polarity of the continuous phase and the compatibility of two phases were changed by adjusting the methyl methacrylate (MMA) content, choosing values that were close to styrene-butadiene rubber solubility value. The possibility of controlling the microstructure of the MABS resin by changing the polarity of the components and the compatibility of two phases was assessed. The dynamic mechanical analysis shows that the compatibility of two phases varies with the MMA content. The morphological analysis shows that increasing MMA contents results in a gradual decrease in the sub-inclusion structure with a network skeleton of rubber particles, and that all the particles become solid rubber when the MMA content reaches 75%. The sub-inclusion structure reappears but does not have a network skeleton when the MMA content is 90%. The impact strength and morphological analysis indicate that the solid rubber particles and the sub-inclusion structure with a network skeleton provide excellent toughness, while the sub-inclusion structure without a network skeleton does not. In contrast, the transmittance of the ABS resin first increased and then decreased with increasing MMA content. 相似文献
5.
《Ceramics International》2015,41(8):9373-9382
The aim of this work was to study the bioactivity of systems based on a clinically tested bioactive glass (BG) particulates (mol%: 4.33 Na2O−30.30 CaO−12.99 MgO−45.45 SiO2−2.60 P2O5−4.33 CaF2) and organic carriers. The cohesiveness of injectable bone graft products is of high relevance when filling complex volumetric bone defects. With this motivation behind, BG particulates with mean sizes within 11−14 μm were mixed in different proportions with glycerol (G) and polyethylene glycol (PEG) as organic carriers and the mixtures were fully injectable exhibiting Newtonian flow behaviors. The apatite forming ability was investigated using X-ray diffraction and field emission scanning electron microscopy under secondary electron mode after immersion of samples in simulated body fluid (SBF) for time durations varying between 12 h and 7 days. The results obtained revealed that in spite of the good adhesion of glycerol and PEG carriers to glass particles during preparation stage, they did not hinder the exposure of bioactive glass particulates to the direct contact with SBF solution. The results confirmed the excellent bioactivity in vitro for all compositions expressed by high biomineralization rates with the formation of crystalline hydroxyapatite being identified by XRD after 12 h of immersion in SBF solution. 相似文献
6.
The aim of this study was to investigate the structure and corrosion resistance of amorphous, amorphous‐crystalline, and crystalline Mg67Zn29Ca4 alloy for biodegradable applications. This paper presents a preparation method and results of the structural characterization and corrosion resistance analysis of the material. Samples were prepared in the form of 3 mm diameter rods. The structure of the alloy was examined with the use of X‐ray diffractometry and scanning electron microscopy. The thermal properties of the samples were examined with differential scanning calorimetry (DSC). Results of DSC analysis were used to determine heat treatment temperatures, allowing to obtain different fractures of crystalline phase in the material. Corrosion resistance of heat‐treated samples was investigated by immersion tests and electrochemical measurements performed in the simulated body fluid. The X‐ray diffraction results confirmed that the prepared Mg67Zn29Ca4 alloy's structure is fully amorphous. After heat treatment, samples with different fractions of amorphous phase in the structure were obtained. Immersion tests of the samples showed that the structure significantly influenced corrosion resistance in examined materials. It should be pointed out, that certain amounts of crystalline phase in amorphous matrix can greatly improve the corrosion resistance of Mg67Zn29Ca4 alloy. 相似文献
7.
3D laser ultramicroscopy (3D LUM) is intended specially for determining the concentration and size distribution of submicron inclusions in the bulk samples of high-purity materials for visible and IR fiber optics. In this work the 3D LUM technique is shown to be able to identify the nature of individual inclusions detected. The measurement of the light scattered by an inclusion at a varied probe beam wavelength and polarization and at a varied scattered light collection angle makes it possible to determine the inclusion refractive index. The 3D LUM possibilities are illustrated by the example of studying the inclusion nature in the As2S3 glass samples prepared by the direct synthesis from elements in a quartz container at elevated temperatures. 相似文献
8.
《Intermetallics》2015
The tribological properties of zirconium-based bulk metallic glass (BMG) sliding against polymers, steels, and ceramics at different loads and speeds were investigated. Acoustic emission (AE) technology was used to analyze wear states. The frictional coefficients of the BMG slid against the steel and ceramic balls were high but decreased with increased applied normal load and sliding speed. As the steel balls were more ductile than the ceramic ones, the steel–BMG sliding pairs generated weaker AE signals and exhibited larger wear rates. The BMG tested against the polymer balls had much lower and more stable frictional coefficients than the ones against the steel or ceramic balls because of transferred polymer layers on the BMG surfaces. The BMG against the polymer balls also exhibited the highest AE signals among the three types of counter materials used, indicating that abrasive wear dominated in the polymer-BMG sliding pairs. These results demonstrated the potential application of the BMG as a new tribomaterial that could be an alternative to the traditional crystalline metals for various counter materials. 相似文献
9.
J. Gutirrez J. M. Barandiarn Z. Kaczkowski 《Materials Science and Engineering: A》2004,370(1-2):392-395
The change of magnetoelastic properties after thermal treatments has been investigated for two groups of metallic glasses. (Fe79Co21)75+xSi15−1.4xB10+0.4x (x (at.%)=0, 2, 4, 6, 8, 10) has been studied both in the as-prepared state and after thermal annealing in an applied magnetic field, to achieve a particular domain structure, at temperatures well below the crystallization temperatures. Changes in the ΔE effect, magnetomechanical coupling (k) and internal friction coefficient (Q−1) are reported, reaching values of about 60% of the saturation value ES. Fe64Ni10Nb3Cu1Si13B9 alloys annealed in vacuum for 1 h in the temperature range 350–550 °C showed maximum values of the ΔE effect and k of 61% and 0.85, respectively, accompanied by a minimum value of Q of around 2 for the sample annealed at 460 °C. These variations are related to the progress of nanocrystalization. The properties achieved are among the best reported for magnetomechanical applications. 相似文献
10.
在分析了双极型晶体管和场效应晶体管各自的特点和不足后,介绍了一种既具有双极型晶体管较大电流容量和功率输出,又具有场效应晶体管高输入阻抗的电子器件——双极MOS场效应晶体管(BJMOSFET),同时指出体硅BJMOSFET的阳极扩散区与衬底之间存在较大的漏电流,可产生较大的寄生效应。提出了一种新型固体电子器件——基于SOI的BJMOSFET,分析了其工作原理j与体硅BJMOSFET比较,由于SOI技术完整的介质隔离避免了体硅器件中存在的大部分寄生效应,使基于SOI的BJMOSFET在体效应、热载流子效应、寄生电容、短沟道效应和闩锁效应等方面具有更优良的特性。 相似文献