On-line mass spectrometry system for measurements at single-crystal electrodes in hanging meniscus configuration

We present the construction and some first applications of an On-line electrochemical mass spectrometry system for detecting volatile products formed during electrochemical reactions at a single-crystal electrode in hanging meniscus configuration. The system is based on a small inlet tip made of porous Teflon and a Peek holder, which is brought in close proximity (ca. 10–20 μm) to the electrode surface. The tip is connected to the mass spectrometer by glass and metal tubing. Because of the small amount of gas entering the mass spectrometer, no differential pumping is needed during the measurement. The tip construction and preparation introduced here leads to reproducible voltammetry with very good cleanliness characteristics. The presence of the tip has no significant influence on the blank voltammetry of a Pt(111) in sulfuric acid, and on voltammetric responses for CO adlayer oxidation, methanol oxidation, and hydroxylamine electrochemistry on Pt(111). The formation of gaseous products in these reactions can be followed accurately and is in good agreement with earlier results obtained by other mass spectrometric or spectroscopic techniques. The time response and tailing of the setup is on the order of seconds and mainly determined by the distance between the tip and the electrode.     

Lowering the erosion wear of long blades of the last stages by optimum hanging

Problems of optimum hanging of long rotor blades of the last stages of steam turbines are considered. Causes of nonuniform erosion wear of the inlet edges connected with inaccurate location of holes for the external damper coupling on the chord of the profile are determined. Methods for optimizing the hanging of blades for raising the reliability of the last stages are suggested. Main results of hanging performed with the help of a specially developed “LIBRA” soft hardware are presented. __________ Translated from élektricheskie Stantsii, No. 11, November 2006, pp. 36–41.     

高层建筑外墙干挂花岗岩质量监控

结合安业大厦施工实例，介绍了高层建筑大面积干挂花岗岩的施工过程。为了确保工程一次成活达优，对实施工程质量进行全方位监控。首先确定质量监控的目的，明确专项管理组织及专项负责人，严格监理指令制度。同时针对监控的重点、难点和关键点，组织各方实现工程质量的监控。     

高层建筑屋面悬挑曲梁结构施工技术

本文通过工程实例,说明采用型钢和钢管组合支撑体系,解决高层建筑屋面悬挑曲梁结构的支模难题,保证工程质量和施工安全,并探讨施工中型钢的节点连接做法。     

滩海海底管线悬空问题治理对策

根据埕岛油田浅海滩涂地带海底管线的安全评估报告,对目前影响海底管线安全的悬空问题进行分析和讨论,并针对其产生悬空的原因提出治理的对策和方法。重点介绍了水下支撑固定法。     

宣钢棒材加热炉悬臂辊道的改进

对宣钢棒材加热炉出入炉悬臂辊道漏水、烧损等现象进行了分析，提出了改进措施。     

Latchkey children and susceptibility to peer pressure: An ecological analysis.

Data on adolescents' after-school experiences and their susceptibility to peer pressure were derived from surveys administered to a heterogeneous sample of 865 adolescents in Grades 5–9. Consistent with the findings of previous studies, the results show that Ss who reported home after school were not significantly different from those who were supervised by their parents at home during after-school hours. However, when a 2nd sample of latchkey children (n?=?594) was studied to include greater variation in after-school experiences, Ss who were more removed from adult supervision were found to be more susceptible to peer pressure to engage in antisocial activity. Ss who were home alone were less susceptible to peer pressure than are those who were at a friend's house after school, and those who were at a friend's house, in turn, were less susceptible than were those who describe themselves as "hanging out." Moreover, latchkey Ss whose parents knew their whereabouts and those who had been raised authoritatively were less susceptible to peer influence than were their peers, even if their afternoons were spent in contexts in which adult supervision was lax and susceptibility to peer pressure was generally high. (17 ref) (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

关于电子皮带秤挂码标定的探讨

在电子皮带秤称量输送物料的传输系统中,当出现对实物标定困难和安装位置不便于链码标定的计量点时,简单、易行的选择就是进行挂码标定。笔者就怎样减少挂码标定的误差,获得较高的标定精确度等,进行了探讨,可供相关专业参考。     

可控式循环通断程序的算法

本文重点介绍了采用梯形图编写的一个程序算法,使用该算法,可以解决高炉上料时,由于炉料中粉末多而引起的高炉悬料情况的发生.     

Spartan6芯片μC/OS-Ⅱ的可抢占式嵌套中断控制方法

介绍了Spartan6芯片搭载MicroBlaze软核的硬件平台,以及集成了μC/OS-Ⅱ操作系统的软件平台;给出了在此软硬件平台上的可抢占、可嵌套的中断机制的实现方法;灵活地运用面向底层硬件代码与操作系统代码之间的参数传递,协调了中断处理与任务调度之间的关系。阐述了方案的原理,给出了程序流程图;通过试验,验证了可抢占、可嵌套的中断机制的正确性与可行性。