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排序方式: 共有281条查询结果,搜索用时 15 毫秒
1.
Influence of ion bombardment on the properties and microstructure of unbalanced magnetron deposited niobium coatings 总被引:3,自引:0,他引:3
The effect of the ion bombardment to unbalanced magnetron deposited, approximately 1.5 and 4.5 μm thick, Nb coatings have been investigated as the bias voltage was varied from UB=−75 to −150 V. Increasing bias voltage increased the hardness of the coating from 4.5 to 8.0 GPa. This was associated with residual stress and Ar incorporation into the Nb lattice. Strong {110} texture developed in the samples deposited at low bias voltages, while beyond UB=−100 V a {111} texture became dominant. However, strong {111} texture was observed only with the thicker 3Nb coatings. Secondary electron microscopy investigation of the coating topography showed fewer defects in the thicker coatings. All coatings exhibited good corrosion resistance, with the thicker coatings clearly outperforming the thinner ones. Excessive bias voltages (UB=−150 V) was found to lead to poor adhesion and loss of corrosion resistance. 相似文献
2.
本文通过有关理论依据和试验数据,着重阐述了在显像(示)管测试中,阴极像中心黑洞状缺陷产生的原因以及消除这种缺陷的处理方法。通过这种处理方法处理过的显像(示)管,其整体质量水平(尤其是真空度)将会得到明显的提高。 相似文献
3.
The XPS of bulk tungsten carbide, partially oxidized WC surfaces at 373 and 573 K as well as tungsten trioxide have been reported. Bulk WC has been prepared from WO3 as a starting material in a mixture of CH4 (20%) and H2 (80%) at 1150 K for 4 h, while partially oxidized WC surfaces were prepared by oxygen chemisorption on a clean WC surface at 200 K, then the temperatures were raised to 373 and 573 K respectively. The XPS of a freshly prepared WC reveals the presence of a small amount of WO3 on the surface and a slightly higher concentration in the bulk. The oxygen-exposed fresh WC surfaces and surfaces treated at temperatures higher than 373 K show the presence of WO3 in a considerable quantity depending on the length and the treatment temperature. Ar+ bombardment of this partially oxidized surface reduces WO3 to WO2 and W(0), while WC is partially reduced to W(0). Isomerization reactions of alkanes on oxygen-exposed WC surface occurs in reality on a composite surface structure containing WC, WO3, WO2 and elemental W(0). 相似文献
4.
秀卢瑟福背散射-沟道技术(RBS-C)和X射线衍射技术(XRD)研究了Pt和注入YSZ(Y2O3稳定的ZrO2)后产生的损伤和退火过程中损伤的恢复及注入Pt的晶化,RBS-C分析表明YSZ室温下的存在较强自退火效应,XRD分析结果示出硫以铂的晶化产生很大影响。 相似文献
5.
综述了堆内辐照对锆合金电化学性能影响的概况,浅析了堆内辐照损伤的机理,并重点探讨了主要的堆内辐照源——中子辐照对锆合金微观结构与氧化性能的影响。进一步阐述了堆外离子轰击模拟堆内中子辐照研究方法的进展概况,并就离子轰击实验参量的选择进行了较为深入的分析。 相似文献
6.
7.
离子轰击膏剂渗硼试验 总被引:1,自引:0,他引:1
通过增加辅助阴极,提高无附加热源的离子渗氮炉的升温速度和使用温度,以满足离子渗硼的需要,对以硼铁为供硼剂的渗硼膏剂进行试验,选出在本试验条件下的最佳渗硼膏剂。利用此膏剂,对45钢在850℃×3h条件下进行离子渗硼,得到180μm厚的渗硼层。 相似文献
8.
CrAlN is a good candidate as an alternative to conventional CrN coatings especially for high temperature oxidation-resistance applications. Different CrAlN coatings were deposited on hardened steel substrates by cathodic arc evaporation (CAE) from chromium-aluminum targets in a reactive nitrogen atmosphere at negative substrate bias between − 50 and − 400 V. The negative substrate bias has important effects on the deposition growth rate and crystalline structure. All our coatings presented hardness higher than conventional CrN coatings. The friction coefficient against alumina and tungsten carbide balls was around 0.6. The sliding wear coefficient of the CrAlN coatings was very low while an important wear was observed in the balls before a measurable wear were produced in the coatings. This effect was more pronounced as the negative substrate bias was increased. 相似文献
9.
Ichiro Takano Yoshiharu Arai Michiko Sasaki Yoshio Sawada Kaori Yamada Takayoshi Yagasaki Yuji Kimura 《Vacuum》2006,80(7):788-792
Biodegradable plastics can be used as conventional plastics, while on disposal they decompose to water and carbon dioxide by microorganisms existing in natural environment. Products using biodegradable plastics have recently been developed in many companies pursuing ecology. In this study, surface modification of biodegradable plastics was carried out by inert ion beams for improvement of photo deterioration under an ultraviolet ray. The hardness of biodegradable plastics tended generally to decrease with irradiation of an ultraviolet ray. In this method, the hardness of ion-bombarded biodegradable plastics was kept at an initial value under an ultraviolet ray, because the modified layer by ion bombardment intercepted an ultraviolet ray. The hardness of He+ ion-bombarded biodegradable plastics showed larger value than that of Ar+ ion bombardment. He+ ion bombardment at ion energy of 10 keV produced the suitable property with both of high transmittance of a visible ray and high interception of an ultraviolet ray in a surface layer of biodegradable plastics. 相似文献
10.
Sliding, abrasive, and impact wear tests were performed on chromium nitride (CrN)-based coatings deposited on mirror-polished M2 high speed steel substrates by the novel high power impulse magnetron sputtering (HIPIMS) utilising high peak cathode powers densities of 3000 W cm−2. The coatings were compared to single layer CrN and multilayer superlattice CrN/NbN coatings deposited by the arc bond sputtering (ABS) technique designed to improve the coating substrate adhesion by a combined steered cathodic arc/unbalanced magnetron (UBM) sputtering process. The substrates were metal ion etched using non-reactive HIPIMS or steered cathodic arc at a substrate bias voltage of −1200 V. Subsequently a 2- to 3-μm thick CrN or CrN/NbN coating was deposited by reactive HIPIMS or UBM. No bias was used during the HIPIMS deposition, while the bias during UBM growth was in the range 75-100 V. The ion saturation current measured by a flat electrostatic probe reached values of 50 mA cm−2 peak for HIPIMS and 1 mA cm−2 continuous during UBM deposition. The microstructure of the HIPIMS coatings observed by transmission electron microscopy was fully dense in contrast to the voided columnar structure observed in conventional UBM sputtered CrN and CrN/NbN. The sliding wear coefficients of the HIPIMS CrN films of 2.3×10−16 m3 N−1 m−1 were lower by a factor of 4 and the roughness of the wear track was significantly reduced compared to the UBM-deposited CrN. The abrasive wear coefficient of the HIPIMS coating was 2.2×10−13 m3 N−1 m−1 representing an improvement by a factor of 3 over UBM deposited CrN and a wear resistance comparable to that of the superlattice CrN/NbN. The adhesion of the HIPIMS deposited CrN was comparable to state-of-the-art ABS technology. 相似文献