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排序方式: 共有1891条查询结果,搜索用时 15 毫秒
1.
Chuncheng Wei Zhen Liu Yun Wu Yeqing Liu Heng Zhang Peng Wang Qiyan Sun Lijuan Zhou 《Ceramics International》2021,47(13):18693-18698
Laminated Si3N4/SiCw ceramics were successfully prepared by tape casting and hot-pressing. Its mechanical properties were measured and the impact resistance was discussed. The toughness of the laminated Si3N4/SiCw ceramics was 13.5 MPa m1/2, which was almost 1.6 times that of Si3N4/SiCw composite ceramics, namely 8.5 MPa m1/2. Moreover, the indentation strength of laminated Si3N4/SiCw ceramics was not sensitive to increasing indentation loads and exhibited a rising R-curve behaviour, indicating that the laminated Si3N4/SiCw ceramics had excellent impact resistance. The improved toughness and impact resistance of laminated Si3N4/SiCw ceramics was attributed to the residual stress caused by a thermal expansion coefficient mismatch between the different layers, resulting in crack deflection and bridging of SiC whiskers in the interface layer, thus consuming a large amount of fracture work. 相似文献
2.
Chaoxin Li Yi Zhou Yuming Tian Yuanyuan Zhao Kaiyue Wang Guomin Li Yuesheng Chai 《Ceramics International》2019,45(5):5613-5616
Ceramics with mullite whiskers were prepared from coal fly ash and Al2O3 raw materials, with AlF3 used as an additive. The phase structures and microstructures of the ceramics were identified via X-ray diffraction and scanning electron microscopy, respectively. The results show that pickling of coal fly ash is an effective method for enhancing the flexural strength of ceramics. Sintering temperature and AlF3 addition were also key factors influencing the creation of ideal ceramics. The ceramic made from pickled coal fly ash, 6?wt% AlF3, and sintered at 1200?°C, exhibited the highest flexural strength of 59.1?MPa, and had a bulk density of 1.32?g/cm3 and porosity of 26.8%. The results show that ceramic materials made under these conditions are ideal candidates for manufacturing ceramic proppants for the exploitation of unconventional oil and gas resources. 相似文献
3.
Hong Wei Li Li Ya‐Li Ma Ru‐Xue Liu Shuang‐Yan Meng Li‐Tong Niu Zhe Zhang Zhi‐Wang Yang 《火与材料》2019,43(7):868-879
Through the simple precipitation of palygorskite (PGS) by zinc borate (ZB) (to make PGS@ZB) and the decoration of PGS@ZB by dodecylamine (N), a novel organic‐inorganic@inorganic hybrid flame retardant of PGS@ZB‐N was prepared and was incorporated with ethylene vinyl acetate copolymer (EVA) to improve its flame retardance. The structure and morphology of PGS@ZB‐N were characterized by Fourier transform infrared (FTIR) spectroscopy, X‐ray diffraction (XRD), and scanning electron microscopy (SEM), and it was confirmed that the PGS@ZB‐N hybrid had been successfully prepared. The flame retardancy and burning behavior of EVA/PGS@ZB‐N/EG (EG = expandable graphite) composite were studied through thermogravimetric analysis (TGA), limiting oxygen index (LOI), UL‐94 (by the vertical burning test), and cone calorimeter test (CCT) characterizations. The prepared EVA/PGS@ZB‐N/EG composite obtained an LOI value of 41.2% with the addition of 30 wt% PGS@ZB‐N/EG. It was found that EVA/PGS@ZB‐N/EG was protected through a gas phase and condensed phase alternating synergistic effect mechanism. 相似文献
4.
《Ceramics International》2020,46(7):8839-8844
In this work, B4C-covered zirconia-toughened alumina (ZTA) particles are prepared and oxidised at 1050 °C for different times (0, 2, 4, and 8 h) in air. The X-ray diffraction and electron probe micro-analysis results show that the covering layer is mainly composed of oxide B2O3 intermetallics, residual B4C particles, and Al18B4O33 whiskers. The scanning electron microscopy results show that the growth of Al18B4O33 whiskers on the ZTA particles enhances with increasing heat preservation time; the optimum holding time is determined to be 8 h Al2O3 in the ZTA particles diffuse into the covering layer and combine with B2O3 to form Al18B4O33 whiskers; the Al18B4O33 whiskers grow via the liquid-solid mechanism. 相似文献
5.
T-ZnO晶须增强环氧树脂复合材料的力学行为 总被引:10,自引:0,他引:10
研究了以四脚状氧化锌(T-ZnO)晶须为增强剂,环氧树脂复合材料的力学行为。结果表明,由具有三维空间结构的T-ZnO晶须为增强剂所制备的环氧树脂复合材料具有各向同性的力学性能,T-ZnO晶须填加质量分数为6%时,就可使材料的力学性能改善;拉伸强度提高到169%,拉伸功几乎提高了100%,冲击强度提高到300%,抗弯的断裂功提高到158%,而压缩强度略有下降。 相似文献
6.
采用SEM 和 Magiscan-2A 图像分析系统研究了晶须取向对SiCw/6061Al复合材料在300℃压缩变形行为的影响.结果表明:晶须取向影响着晶须折断程度和转动角度; 随着晶须取向角的增加,晶须转动和折断行为所导致的软化效果下降.同时晶须取向也影响复合材料的热压缩应力-应变曲线的形状.在热压缩变形过程中,晶须取向角为0°和30°的复合材料表现出明显应变软化现象, 晶须取向角为45°的复合材料无明显软化现象.晶须取向角为90℃的复合材料表现出应变硬化现象. 相似文献
7.
Depletion and hillock formation were examined in-situ in a scanning electron microscope (SEM) during electromigration of bamboo
Al interconnect segments. Hillocks formed directly at the anode ends of the segments by epitaxial addition of Al at the bottom
Al/TiN interface. Depletion occurred nonuniformly from the cathode end and stopped once the distance between the leading void
and the hillock reached the critical length for electromigration at the given current density. A modified equation for the
drift velocity is proposed, which includes the effect of nonuniform depletion and predicts that interconnects with nonuniform
depletion are more reliable than those with uniform depletion. 相似文献
8.
SiC(w)/TZP+mullite陶瓷复合材料界面和组成设计与力学性能 总被引:2,自引:1,他引:1
本文从理论上分析了SiC(w)TZP+mullite(p)复合材料界面残余热应力及其在基质内的分布规律。提出在SiC(w)表面涂复Al2O3和在PZT中加入mullite(p)联合作用来降低晶须/基质界面残余热应力的界面设计方案,导出SiC(w)和mullite(p)协同补强PZT的匹配条件。制备了SiC(w)/TZP+mullite(p)复合材料并了SiC(w)表面涂层Al2O3厚度和SiC(w 相似文献
9.
低品位硼矿的富集加工技术 总被引:2,自引:0,他引:2
报道了青海大柴旦地区低品位硼矿富集加工的新工艺,该工艺使硼矿品位30%-35%,B2O3收率大于80%,该工艺路线已工业化。 相似文献
10.
本文以硼酸铝晶须为增强剂,以4,5-环氧环己烷-1,2-二甲酸二缩水甘油酯(TDE-85),甲基纳狄克酸酐(MNA)、N,N’-二胺基二苯甲烷型双马来酰亚胺(BMI)/O,O′-二烯丙基双酚A(BA)体系分别作为基体制备晶须增强复合材料。研究了晶须对树脂的尺寸、表面处理方法、含量对树脂体系力学性能和热性能的影响;通过扫描电子显微镜(SEM)分析了浇注体的弯曲、冲击断口,研究晶须的增强机理。 相似文献