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1.
通过制备不同晶相结构〔单斜相(m-ZrO_2)、四方相(t-ZrO_2)和无定型(a-ZrO_2)〕ZrO_2载体,再通过沉积沉淀法制得Cu/m-ZrO_2、Cu/t-ZrO_2和Cu/a-ZrO_2催化剂,分别用于催化二乙醇胺脱氢合成亚氨基二乙酸反应。采用XRD、氮气物理吸附脱附、XPS、H_2-TPR、CO_2-TPD对催化剂的结构进行了表征。结果表明,Cu/m-ZrO_2催化剂界面更加有利于Cu~+/Cu~0稳定存在,具有更多的碱性位点,且抗氧化性较好。在二乙醇胺脱氢反应中,Cu/m-ZrO_2催化剂性能最好,反应时间为2.5 h,亚氨基二乙酸收率为97.64%。 相似文献
2.
Hao Li Pengcheng Zhang Shengquan Yu Hongyu Yang Bin Tang Fuhai Li Shuren Zhang 《Ceramics International》2019,45(9):11639-11647
Mg2(Ti1-xSnx)O4 (x?=?0–1) ceramics were prepared through conventional solid-state method. This paper focused on the dependence of microwave dielectric properties on crystal structural characteristics via crystal structure refinement, Raman spectra study and complex chemical bond theory. XRD spectrums delineated the phase information of a spinel structure, and structural characteristic of these compositions were achieved with the help of Rietveld refinements. Raman spectrums were used to depict the correlations between vibrational phonon modes and dielectric properties. The variation of permittivity is ascribed to the Mg2(Ti1-xSnx)O4 average bond covalency. The relationship among the B-site octahedral bond energy, tetrahedral bond energy and temperature coefficient are discussed by defining on the change rate of bond energy and the contribution rate of octahedral bond energy. The quality factor is affected by systematic total lattice energy, and the research of XPS patterns illustrated that oxygen vacancies can be effectively restrained in rich oxygen sintering process. Obviously, the microwave dielectric properties of Mg2(Ti1-xSnx)O4 compounds were obtained (= 12.18, ?=?170,130?GHz, ?=??53.1?ppm/°C, x?=?0.2). 相似文献
3.
Hashim A.
Hashim 《国际强度与非线性控制杂志
》2020,30(10):3848-3870
》2020,30(10):3848-3870
This paper introduces two novel nonlinear stochastic attitude estimators developed on the Special Orthogonal Group with the tracking error of the normalized Euclidean distance meeting predefined transient and steady‐state characteristics. The tracking error is confined to initially start within a predetermined large set such that the transient performance is guaranteed to obey dynamically reducing boundaries and decrease smoothly and asymptotically to the origin in probability from almost any initial condition. The proposed estimators produce accurate attitude estimates with remarkable convergence properties using measurements obtained from low‐cost inertial measurement units. The estimators proposed in continuous form are complemented by their discrete versions for the implementation purposes. The simulation results illustrate the effectiveness and robustness of the proposed estimators against uncertain measurements and large initialization error, whether in continuous or discrete form. 相似文献
4.
5.
分析了冶炼烟气制酸工艺的特点,介绍了由PROFIBUS-DP现场总线构建的冶炼厂烟气制酸监控系统,详细介绍了其硬件配置及相应的软件设计。 相似文献
6.
Frequency Insertion Strategy for Channel Assignment Problem 总被引:1,自引:0,他引:1
This paper presents a new heuristic method for quickly finding a good feasible solution to the channel assignment problem
(CAP). Like many other greedy-type heuristics for CAP, the proposed method also assigns a frequency to a call, one at a time.
Hence, the method requires computational time that increases only linear to the number of calls. However, what distinguishes
the method from others is that it starts with a narrow enough frequency band so as to provoke violations of constraints that
we need to comply with in order to avoid radio interference. Each violation is then resolved by inserting frequencies at the
most appropriate positions so that the band of frequencies expands minimally. An extensive computational experiment using
a set of randomly generated problems as well as the Philadelphia benchmark instances shows that the proposed method perform
statistically better than existing methods of its kind and even yields optimum solutions to most of Philadelphia benchmark
instances among which two cases are reported for the first time ever, in this paper.
Won-Young Shin was born in Busan, Korea in 1978. He received B.S. in industrial engineering from Pohang University of Science and Technology
(POSTECH) in 2001 and M.S in operation research and applied statistics from POSTECH in 2003. Since 2003 he has been a researcher
of Agency for Defense Development (ADD) in Korea. He is interested in optimization of communication system and applied statistics.
Soo Y. Chang is an associate professor in the Department of Industrial Engineering at Pohang University of Science and Technology (POSTECH),
Pohang, Korea. He teaches linear programming, discrete optimization, network flows and operations research courses. His research
interests include mathematical programming and scheduling. He has published in several journals including Discrete Applied
Mathematics, Computers and Mathematics with Application, IIE Transactions, International Journal of Production Research, and
so on. He is a member of Korean IIE, and ORMSS.
Jaewook Lee is an assistant professor in the Department of Industrial Engineering at Pohang University of Science and Technology (POSTECH),
Pohang, Korea. He received the B.S. degree in mathematics with honors from Seoul National University, and the Ph.D. degree
from Cornell University in applied mathematics in 1993 and 1999, respectively. He is currently an assistant professor in the
department of industrial engineering at the Pohang University of Science and Technology (POSTECH). His research interests
include nonlinear systems, neural networks, nonlinear optimization, and their applications to data mining and financial engineering.
Chi-Hyuck Jun was born in Seoul, Korea in 1954. He received B.S. in mineral and petroleum engineering from Seoul National University in
1977, M.S. in industrial engineering from Korea Advanced Institute of Science and Technology in 1979 and Ph.D. in operations
research from University of California, Berkeley, in 1986. Since 1987 he has been with the department of industrial engineering,
Pohang University of Science and Technology (POSTECH) and he is now a professor and the department head. He is interested
in performance analysis of communication and production systems. He has published in several journals including IIE Transactions,
IEEE Transactions, Queueing Systems and Chemometrics and Intelligent Laboratory Systems. He is a member of IEEE, INFORMS and
ASQ. 相似文献
7.
马钢二烧结配料计算机控制系统 总被引:1,自引:0,他引:1
阐明了马钢二烧结配科计算机控制系统的目的、控制形式、控制原理;根据烧结配料控制对象的特点对信号采样和控制算法进行了探讨;提供了系统的主要硬件结构,软件功能和程序框图。 相似文献
8.
9.
Kurjenniemi Janne Hämäläinen Seppo Ristaniemi Tapani 《Wireless Personal Communications》2003,27(4):337-351
In this article we consider the performance of the 3.84 Mcpstime-division duplex (TDD) mode of UTRA (Universal TerrestrialRadio Access) network. We emphasize two of the radio resourcemanagement algorithms, handover and uplink power control, whoserole in the overall system performance is studied extensively.First, a handover algorithm used in WCDMA (Wideband Code DivisionMultiple Access) standard is considered in a TDD-mode operation.This gives rise to a careful setting of different handoverparameters, and the evaluation of the effects to the systemperformance. Secondly, the specified uplink power controlalgorithm is considered. Since it is based on several user-mademeasurements which may involve both random and systematic errors acareful study about the suitability of the power control scheme iscarried out. 相似文献
10.
孙洪松 《石油化工管理干部学院学报》2006,(1):52-55
目前,我国股票市场上的股票评级尚处于探索阶段,评级时多采用专家法或历史法,而对于影响股票评级的各因素的确定以及因素间的相互作用缺乏定量分析。研究将结构模型应用到我国股票市场的股票评级中,建立关于我国股票评级的财务结构模型;分析各个因素对股票评级的影响;建立股票评级经验模式值。 相似文献