席夫碱与硝酸铈复配物对1060纯铝的缓蚀作用

采用极化曲线、电化学阻抗谱、扫描电镜和能谱分析,研究合成的3-吡啶-4-氨基-1,2,4-三唑-5-硫酮席夫碱及其复配物硝酸铈在质量分数为3.5%NaCl溶液中对1060纯铝的缓蚀作用。结果表明：在293 K时席夫碱可有效抑制纯铝在3.5%NaCl溶液中的腐蚀,当席夫碱浓度为0.4 g.L_-1时缓蚀率最高,可达76.0%。席夫碱为混合型缓蚀剂,其在1060纯铝表面的吸附符合Langmuir吸附模型,且同时存在物理吸附和化学吸附。0.2 g.L_-1席夫碱与0.03 g.L_-1硝酸铈复配缓蚀率可达88.2%,二者具有协同缓蚀作用。     

Acoustic emissions during fracture toughness tests of steels exhibiting varying ductility

This investigation is primarily aimed at examining steels with varying ductility using characteristics of acoustic emission (AE). Four steels (AISI 1060, AISI 1080, SA333 grade 6 and AISI 304LN) were selected and their structure property relations were characterized using standard metallographic examinations, hardness and tensile properties. Fracture toughness of these steels was determined as per the guidelines of ASTM standard E1820 with simultaneous recording of AE signals. The results of these investigations have been used to demonstrate that: (a) nature of the variation of AE cumulative counts with time is different for linear and non-linear load–displacement plots, (b) synergistic analysis of the rate of change of cumulative energy, cumulative counts and intensity of AE signals provide the point of crack initiation in a material, and (c) fracture toughness of a material estimated using AE parameters is lower compared to that obtained by ASTM standard procedure.     

高防腐铝合金电缆桥架生产工艺

介绍了高防腐铝合金电缆线桥架的生产工艺,通过控制用料的质量、冲压、焊接和阳极氧化等因素,用６０６３合金型材和１０６０铝合金板材可以生产出性能优良的铝合金电缆桥架。     

太阳能热水器铝合金托架的电泳涂漆工艺

介绍了太阳能热水器铝合金托架的电泳涂漆工艺。分析了影响铝合金托架电泳涂漆质量的主要因素，给出了相应的解决措施和最佳工艺参数。     

Fabrication of ultrafine-grained AA1060 sheets via accumulative roll bonding with subsequent cryorolling

Ultrafine-grained (UFG) AA1060 sheets were fabricated via five-cycle accumulative roll bonding (ARB) and subsequent three-pass cold rolling (298 K), or cryorolling (83 K and 173 K). Microstructures of the aluminum samples were examined via transmission electron microscopy, and their mechanical properties were measured via tensile and microhardness testing. Results indicate that ultrafine grains in ARB-processed sheets were further refined by subsequent rolling, and the grain size became finer with reducing rolling temperature. The mean grain size of 666 nm in the sheets subjected to ARB was refined to 346 or 266 nm, respectively, via subsequent cold rolling or cryorolling (83 K). Subsequent cryorolling resulted in ultrafine-grained sheets of higher strength and ductility than those of the sheets subjected to cold rolling.     

5454热挤压管与1060冷拉管性能对比试验

简述了５４５４热挤压管在碳铵生产企业碳化水箱上的应用,分析了ＲＥ（稀土）在５４５４合金中的作用,通过对比试验评价了５４５４热挤压管与１０６０冷拉管的耐冲刷磨损性、耐腐蚀性及冷弯曲加工性。     

纳米BN对1060铝微孤氧化膜层性能的影响

目的探究微弧氧化电解液中纳米氮化硼(BN)浓度对铝微弧氧化陶瓷层组织和性能的影响。方法在硅酸盐体系电解液中加入1~5 g/L不同浓度的纳米BN,制备纳米BN复合微弧氧化层。利用扫描电镜、能谱仪和X射线衍射仪,分别表征纳米BN复合微弧氧化层的微观组织、元素分布及物相组成。采用涂层测厚仪、粗糙度仪、显微硬度计、摩擦磨损试验机等手段,研究纳米BN对1060纯铝微弧氧化膜层的厚度、粗糙度、显微硬度、摩擦学性能的影响。结果在微弧氧化BN复合膜的表层有弥散分布的BN颗粒,当电解液中添加3 g/L的纳米BN时,制备的微弧氧化层的性能最好,其表面的孔洞数量最少且孔径最小,膜层表面更加致密,其厚度可达到(93.8±1.9)μm,硬度达到(942±51)HV,粗糙度Ra降低为(3.66±0.14)μm,摩擦系数降低为0.55,磨损体积比未添加BN的膜层减少了1.18×10-2 mm3,并且磨痕平整光滑,裂纹较少。结论硅酸盐电解液中加入纳米BN能够改善1060纯铝微弧氧化膜层的综合性能。     

ARB法制备超细晶材料的组织与性能研究

采用累积叠轧焊方法（ARB）对MB2镁合金和1060工业纯铝进行试验,分析了它们变形前后内部微观组织结构的演变和力学性能的变化。结果表明,MB2镁合金平均晶粒细化到1.2μm,抗拉强度由轧制前的235 MPa提高到300 MPa;1060工业纯铝晶粒细化到约400 nm,抗拉强度由轧制前的87MPa提高到220 MPa,硬度由轧制前的37 HV提高到83 HV;2种材料的延伸率在ARB 1道次后下降,并随着轧制道次的增加,材料组织均匀程度提高,抗拉强度变化平缓;MB2镁合金的延伸率回升幅度较大。     

限制模压变形1060纯铝的组织演化与晶粒细化

设计平行模压变形、180°交叉模压变形、90°交叉模压变形对1060纯铝进行系列限制模压变形(CGP)试验,采用透射电镜研究该材料在不同变形工艺下的组织演化规律和晶粒细化速率.结果表明:变形工艺不影响组织的演化规律,但显著影响晶粒细化速率、晶粒细化效果以及大角度晶界的形成;90°交叉模压变形最优.在相同的变形温度、变形速率和应变累积条件下,所能达到的晶粒细化速率和大角度晶界的数量取决于剪切变形模式.     

1060铝材两步化学浸锌工艺

铝材化学性质活泼,欲获得不同性能的镀层,前处理非常重要。选用两步碱性化学浸锌体系对1060铝材进行了前处理,随后镀镍。通过自腐蚀电位-时间曲线,浸锌层扫描电镜(SEM)形貌分析,弯折试验、热震试验等考察了浸锌层与铝基体的附着力,并确定了获得结合力优良的浸锌层的最佳工艺条件:300 g/L NaOH,65 g/LZnO,50 g/L KOCO(CHOH)2COONa,1 g/L FeCl3,2 g/L NaNO3;温度20~30℃,一次浸锌时间60 s,二次浸锌时间30 s,所获浸锌层可满足后续电镀工艺的需要。