RFCCU反再系统防结焦措施的应用及技术分析

介绍了济南分公司140万t／a RFCCU两个周期运行后反再系统的结焦情况，详细介绍了防治结焦所采取的措施，并进行了技术分析。两次停工后的设备检查，证明所采取的防治措施是十分有效的。     

石油渣油制备针状焦研究--中间馏分热反应研究

石油渣油的组成复杂,分子量分布宽,直接焦化不能生产针状焦。采用一定的预处理技术将渣油中适宜制备针状焦的组分保留,可获得理想的焦化原料。通过以辽河减压渣油为原料,经溶剂萃取对渣油进行"掐头去尾"处理,获得了分子量分布窄、杂质含量少的中间馏分A及馏分B。对馏分A、B分别进行热反应研究,结果表明:渣油的预处理效果明显,中间馏分热反应产物具有光学各向异性物含量高、取向性好等特点,是制备针状焦的理想原料。     

6m焦炉投产初期的热工管理

简要介绍焦化厂6m焦炉投产一年多以来的生产现状，整改措施和焦炉热工管理。     

贮煤塔开闭器驱动装置的改造

针对炼铁厂炼焦车间贮煤塔和开闲器驱动装置存在故障频繁，堵煤、开闭器易损坏和吹风管堵塞等问题，通过分析并结合实际情况，将煤塔漏嘴由27只减为9只双曲线形状漏嘴，开闭器驱动装置由车载驱动改为固定驱动。改造后，解决了使用中堵煤及开闭器驱动装置损坏等问题，降低了设备故障率，减少了生产成本，增加了装煤量，满足了生产需要。     

Split and collectorless flotation to medium coking coal fines for multi-product zero waste concept

The medium coking coal fines of − 0.5 mm from Jharia coal field were taken for this investigation. The release analysis of the composite coal reveals that yield is very low at 10.0% ash, about 25% at 14% ash and 50% at 17% ash level. The low yield is caused by the presence of high ash finer fraction. The size-wise ash analysis of − 0.5 mm coal indicated that − 0.5 + 0.15 mm fraction contains less ash than − 0.15 mm fraction. Thus, the composite feed was split into − 0.5 + 0.15 mm and − 0.15 mm fractions and subjected to flotation separately. The low ash bearing fraction (− 0.5 + 0.15 mm) was subjected to two stages collectorless flotation to achieve the concentrate with 10% ash. The cleaner concentrate (18.9%) with 10% ash was recovered which has an application in metallurgical industries. The concentrate of 30.2% yield with 12.5% ash could be achieved in one stage collectorless flotation which is suitable for use in coke making as sweetener. As the − 0.15 mm fraction contains relatively high ash, collector aided flotation using sodium silicate was performed to get a concentrate of 23.6% yield with about 17% ash. The blending of this product with cleaner tail obtained from − 0.5 + 0.15 mm produces about 35.0% yield with 17% ash and that can be utilized for coke making. The reject from the two fractions can be used for conventional thermal power plant or cement industries using a 23.5% ash after one stage collector aided flotation and the final tailings produced content ash of 61.6% can be used for fluidization combustion bed (FBC). This eventually leads to complete utilization of coal.     

焦化加热炉爆管故障分析与预防

焦化加热炉炉管内的物料通常为有杂质容易结焦的混合渣油,如果设计不合理、操作控制不当、运行周期过长等,极易造成炉管爆管事故。以2005年9月大庆石化分公司炼油厂焦化加热炉爆管故障为例,阐述了焦化加热炉的爆管原因、故障处理及预防措施,认为注水量小、渣油中含催化剂、负荷偏离设计工况、烧焦周期和烧焦速度不当等引起严重结焦是爆管的主要原因。     

ZSM-5型沸石催化剂的结焦与失活

本文对ZSM-5型沸石催化剂结焦与失活的关系进行了系统的评述.探讨了ZSM-5沸石的酸度和微孔结构对结焦过程的影响.     

一种基于时间戳认证的零水印方案设计

零水印方法是一种新的数字水印方法。本文介绍了零水印的概念及零水印技术的关键问题,提出了一种基于时间戳认证的零水印方案。该方案很好地解决了非零水印的不可见性与鲁棒性之间的矛盾,具有可行性和通用性。     

焦炉烘炉问题探讨

介绍了柳钢焦化厂6、7号焦炉烘炉中存在的问题及其改进措施。     

粗苯放散气体回收系统的开工调试经验

介绍了焦化厂粗苯放散气体回收系统开工调试的经验。