Phase constitution,microstructure and mechanical properties of a Ni-based superalloy specially designed for additive manufacturing

In this study, a kind of Ni-based superalloy specially designed for additive manufacturing (AM) was investigated. Thermo-Calc simulation and differential scanning calorimetry (DSC) analysis were used to determine phases and their transformation temperature. Experimental specimens were prepared by laser metal deposition (LMD) and traditional casting method. Microstructure, phase constitution and mechanical properties of the alloy were characterized by scanning electron microscopy (SEM), transmission scanning electron microscopy (TEM), X-ray diffraction (XRD) and tensile tests. The results show that this alloy contains two basic phases, γ/γ', in addition to these phases, at least two secondary phases may be present, such as MC carbides and Laves phases. Furthermore, the as-deposited alloy has finer dendrite, its mean primary dendrite arm space (PDAS) is about 30-45 μm, and the average size of γ' particles is 100-150 nm. However, the dendrite size of the as-cast alloy is much larger and its PDAS is 300-500 μm with secondary and even third dendrite arms. Correspondingly, the alloy displays different tensile behavior with different processing methods, and the as-deposited specimen shows better ultimate tensile stress (1,085.7±51.7 MPa), yield stress (697±19.5 MPa) and elongation (25.8%±2.2%) than that of the as-cast specimen. The differences in mechanical properties of the alloy are due to the different morphology and size of dendrites, γ', and Laves phase, and the segregation of elements, etc. Such important information would be helpful for alloy application as well as new alloy development.     

单晶凝固组织的样品尺寸效应

通过对不同直径的单晶样品的凝固实验，研究了样品尺寸对单晶凝固组织的影响规律，研究发现，随样品尺寸减小，单晶凝固组织被细化，尤其一次枝晶间距λ1和枝晶间γ′相尺寸对样品尺寸的依赖性更为明显；样品尺寸影响的要质在于此表面积的变化，进而对凝固过程温度梯度产生影响，最终作用于凝固组织和力学性能，一次枝晶间距λ1和枝晶间γ′尺寸与样品的比表面积近拟呈线性关系，样品尺寸变化，明显改变了单晶生长过程的温度梯度和合金的高温持久寿命。     

GJB712A-2001航天用GH4169高温合金锻制圆饼规范介绍

介绍了GH 4 16 9高温合金锻制圆饼规范的修订内容 ,对其主要技术指标作了简要说明 ,并与国外同类标准进行了比较。     

Ca,Mg对镍基高温合金力学性能和热塑性的影响

本文研究了单加或同时添加微量Ca和Mg对变形及铸态镍基高温合金力学性能和热塑性的影响。试验表明,适量的Mg或Ca、Mg对提高合金的持久断裂寿命、高温拉伸塑性以及改善热塑性都取得良好效果。     

Thermal—Mechanical Fatigue Behavior and Life Analysis of Cast Ni—base Superalloy K417

In-phase(IP) and out-of-phase(OP)thermal-mechanical fatigue(TMF) behavior of cast Ni-base superalloy K417 was studied.All experiments were carried out under total strain control with temperature cycling between 400-850℃.Both in-phase and out-of-phase TMF specimens exhibited cyclic hardening followed by cyclic softening at the minimum temperature.Besides,they cyclically hardened in the early stage of life followed by cyclic softening at the minimum temperature.Besides,they cyclically hardened in the early stage of life followed by cyclic softening at the maximum temperature.OP TMF life was longer than of IP TMF.Various damage mechanisms operating in different controlled strain ranges and phasing were discussed.A few life prediction methods for isothermal fatigue were used to handle TMF fatigue and their applicability to superalloy K417 was evaluated.The SEM analysis of the fracture surface showed that transgranular fracture was the principal cracking mode for both IP and OP TMF.Oxidation was the main damage mechanism in causing shorter fatigue life for IP TMF compared with OP TMF.     

铸造镍基K3合金的激光熔覆开裂及工艺研究

研究了铸造镍基Ｋ３合金的激光熔覆过程，分析了原始组织及激光熔覆工艺参数对熔覆裂纹形成的及作用；探讨了使用激光熔覆技术对损伤的Ｋ３合金叶片进行修复的可能性。研究结果表明，Ｋ３合金中沿界分布的低熔点共晶及碳化物是引起激光熔覆开裂的主要因素，采用较高的功率密度和较快的扫描速度进行激光熔覆，可减少热影响区范围，明显地抑制熔覆裂纹的产生。     

高温合金材料在铝电解工业中的应用探讨

对高温合金在铝电解工业用作惰性金属阳极材料的选择进行阐述，并就实际应用过程中的抗氧化耐腐蚀性进行探讨；阐述适用于铝电解工业的惰性阳极合金所应具备的必要条件和必须解决的问题，并介绍目前有关的研究动态和研究方向。     

定向结晶时高温合金组织控制的工艺前景EI

报道了俄国航空材料研究院(ВИАМ)在定向单晶高温合金组织控制方面的最新研究成果,例如,利用高速定向结晶工艺创造具有单晶组织的宽弦叶片,以及制造前后缘为规定位相的单晶,而在叶身中部为细柱状定向结晶组织的复合组织叶片。这些新工艺提高了材料的工作能力和发动机寿命。     

冶炼工艺对GH871合金涡轮盘韧性的影响

研究了AIM ESR和VIM ESR两种冶炼工艺对GH871合金涡轮盘三种韧性指标的影响,结果表明:冶炼工艺对该合金在室温、650℃拉伸和缺口冲击韧性影响较小,采用VIM ESR冶炼工艺可以显著提高GH871合金在700℃拉伸韧性和I型裂纹平面应变的断裂韧性。     

熔体处理对一种Inconel 718C改型高温合金组织与性能的影响

在试验合金中,1600℃熔体处理对凝固后组织和性能产生显著影响。经1600℃熔体处理后,合金样品二次枝晶间距显著降低,元素偏析情况得到有效改善,凝固过程析出的TCP相数量明显减少,热处理后γ″析出相也更加细小均匀。熔体处理对合金室温和700℃拉伸强度影响不大,但却显著提高合金的拉伸塑性和700℃/620MPa持久性能。在1600℃熔体处理10min时,合金的综合力学性能最佳;延长熔体处理时间至15min时,合金力学性能呈下降趋势。