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2.
稀有金属伟晶岩的结晶过程是认识其成矿作用的重要方面。前人利用冷却模型所推测出的侵入变质围岩的伟晶岩冷却时间为几天至几千年,但对侵位于花岗岩中伟晶岩的结晶过程缺乏相关研究。基于此,对新疆大喀拉苏及镜儿泉地区稀有金属伟晶岩的野外地质观察及年代学研究显示,两处伟晶岩的侵位模式不同,侵位时花岗岩围岩的温度有别。大喀拉苏1号伟晶岩(年龄为(248.4±2.1)~(228.4±0.3)Ma)主要侵位于较冷花岗岩围岩(年龄为(261.4±2.1)Ma)的席理面,边缘可能出现过度冷却。最新铌钽铁矿U-Pb年代学显示,镜儿泉1号锂辉石伟晶岩形成时代为(250.8±1.0)Ma,熔体侵位于温度较高的花岗岩(年龄为(252.9±1.9)Ma)内部断层,其冷却结晶受花岗岩温度及区域地热梯度制约,冷却时间可能超过3 Ma。综上所述,过度冷却模型的适用性、铌钽铁矿U-Pb同位素体系的封闭温度都需要进一步研究,以解释同位素年龄与冷却模型所得结晶时间的显著差异。 相似文献
3.
采用盐类熔剂对大体积Al-4.5wt%Cu合金进行净化处理,研究了熔剂净化对Al-4.5wt%Cu合金过冷及组织的影响。通过大量的实验研究证明:粘性熔剂更能有效地去除合金中的异质核心,使合金获得较大的过冷度;随着过冷度的增大,合金的宏观组织由细小的等轴晶逐渐过渡到粗大的柱状晶,其临界转变过冷度为40℃;二次枝晶间距随过冷度的增大而增大,其转变过冷度为50℃。 相似文献
4.
定向凝固法制备YBC超导体的若干材料学问题 总被引:5,自引:0,他引:5
讨论了定向凝固法制备YBCO超导体涉及的包晶转变与包晶反应,成分过冷,扩散控制生长模型,界面效应及定向凝固YBCO生长晶体学等问题。 相似文献
5.
1 INTRODUCTIONMetallicglassisregardedasastatethatisofdis orderunlikecrystalalloyswith periodicatomstruc ture.Soitshowsexcellentcapabilitiesofsoftmag netism ,mechanics ,corrosionresistance ,etc .How ever ,mostofamorphousalloyswereproducedbyus ingrapidsolidificationmethodssuchassplatquench ing ,meltspinning ,andsoon ,withcharacteristiccoolingratesof 10 4 10 6 K/s .Becauseamorphousal loysarepreparedwithsilk ,powderandribbon ,itisgreatlylimitedinengineeringapplication .Recently ,severalbulk… 相似文献
6.
Y.P. Lu G. C. Yang C.L. Yang H.P. Wang Y.H. Zhou 《金属学报(英文版)》2006,19(1):43-50
A large undercooling level up to 550K (0.386Te) was achieved in eutectic Ni78.6Si21.4melt by the combination of molten-glass and cyclic superheating. A microcrystaUine structure is obtained at large undercooling. Surprisingly, the morphology of ct(Ni) phase transits from the non-faceted phaseto faceted phase at large undercooling of 390K. Based on the classical nucleation theory and transient nucleation theory, the process of microstructure evolution and competitive nucleation was analyzed, and the refinement of crystal structure is determined by the high nucleation rate under large undercooling. 相似文献
7.
Titanium in the rapidly cooled hypereutectic gray iron 总被引:4,自引:0,他引:4
Y. Lerner 《Journal of Materials Engineering and Performance》2003,12(2):141-146
The effect of titanium on the structure and properties of a rapidly cooled hypereutectic cast gray iron has been studied on
the example of permanent mold (PM) casting. A microstructure study showed that titanium is a relatively strong element in
controlling solidification structure by increasing undercooling and thus promoting type D graphite. The effectiveness of titanium
additions depends on the base iron carbon equivalent (CE) with more pronounced changes in iron with a lower CE. The undercooling
ability of the titanium decreases after exceeding a certain level. Increasing titanium from 0.09–0.12% slightly increases
undercooling in iron with lower CE, but this effect was reduced in a more strongly hypereutectic iron. Alloying with titanium
generally improves tensile strength, but the effectiveness of titanium additions also depends on the base iron CE range. Scanning
electron microscope (SEM) studies revealed that most of the titanium-containing compounds were located in the metallic matrix:
titanium carbides have been found in pearlite, while titanium nitrides and carbonitrides were located in ferrite. The presence
of large amounts of extremely hard titanium-containing compounds, which often appear with steadite in a relatively high phosphorous
content PM gray iron, amplifies the negative effect of titanium on machinability. This study suggests that for optimal combination
of tensile strength/microstructure with good machinability, the titanium content in PM gray iron should not exceed 0.075%. 相似文献
8.
Microstructures and evolution mechanism of highly undercooled Ni-Pb hypermonotectic alloy 总被引:1,自引:0,他引:1
The microstructures and evolution mechanism of the undercooled Ni-20%Pb(molar fraction) alloy were investigated systematically by high undercooling solidification technique. The experiment results indicate that the morphology of α-Ni phase and the distribution of Pb element in undercooled Ni-20% Pb alloys change with the in-crease of undercooling. The main evolution mechanisms of α-Ni are dendrite remelting and recrystallization. Pb phase in the microstructure of Ni-20% Pb hypermonotectic alloy originates from L2 phase separated from the parent melt during the cooling process through immiscible gap and L2 phase formed at the temperature of monotectic trans-formation. The solubility of Ph element in α-Ni phase under high undercooling condition is up to 5.83% which is ob-viously higher than that under equilibrium solidification condition. The real reason that causes the solubility difference is distinct solute trapping. 相似文献
9.
研究了Si Zr B模壳涂层对准晶Al72Ni12Co16合金过冷度与凝固组织的影响规律。通过使用Si Zr B涂层模壳,在Al72Ni12Co16合金中获得了不同大小的过冷度,其最大值达到195K。根据经典形核理论,计算了熔体与涂层内壁间的润湿角。研究结果表明:Si Zr B涂层对过冷准晶Al72Ni12Co16合金熔体具有较强的抑制形核作用,因而可使大体积合金熔体获得深过冷。 相似文献
10.
液态金属快速结晶的热力学驱动力 总被引:1,自引:0,他引:1
采用超高真空无容器悬浮熔炼技术使液态Fe和Ni的过冷度分别达200和235K,借助量热法测定出其比热各为48.6和40.5J·mol~(-1)·K~(-1).据此精确计算出深过冷Fe和Ni快速结晶的热力学驱动力△G_(LS),并与Turnbull模型和Dubey-Ramachandrarao模型的近似计算结果相比较,发现这两种近似模型在过冷度超过100K时均产生大于1%的偏差.进一步分析发现,△G_(LS)的计算偏差对深过冷液态金属中晶体形核率的影响极大,因此快速凝固研究中应尽可能精确计算△G_(LS). 相似文献