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《Calphad》2021
The present work illustrates the effect of quasi-hydrostatic pressure on the positions and widths of the homogeneity ranges of the intermetallic phases TiFe and TiFe2 at high temperatures. The experiments were performed with Ti–Fe diffusion couples that were heat treated in a multi-anvil press at 2.5 GPa. The solubility limits of the phases were derived from the concentration profiles that were measured using electron probe microanalysis. It was found that the homogeneity ranges of TiFe and TiFe2 extend to higher titanium concentrations, if the pressure is applied. The positions of the phase boundaries of the intermetallics on the iron-rich side are not affected by the pressure. The accuracy of the experimental data including the homogeneity ranges and temperatures was verified by comparing the homogeneity ranges of β-Ti(Fe), α/δ-Fe(Ti) and γ-Fe measured in this study with the homogeneity ranges taken from literature. The pressure was calibrated using the pressure-induced phase transitions of bismuth. 相似文献
3.
Jialong Tian M. Babar Shahzad Wei Wang Lichang Yin Zhouhua Jiang Ke Yang 《材料科学技术学报》2018,34(9):1671-1675
The effect of Co addition on the formation of Ni-Ti clusters in maraging stainless steel was studied by three dimensional atom probe (3DAP) and first-principles calculation. The cluster analysis based on the maximum separation approach showed an increase in size but a decrease in density of Ni-Ti clusters with increasing the Co content. The first-principles calculation indicated weaker Co-Ni (Co-Ti) interactions than Co-Ti (Fe-Ti) interactions, which should be the essential reason for the change of distribution characteristics of Ni-Ti clusters in bcc Fe caused by Co addition. 相似文献
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超声波强化原油破乳电脱盐技术的工业实践 总被引:9,自引:1,他引:8
报道了采用超声波强化原油破乳电脱盐技术的开发与工业应用.经过实验室开发确定的超声波强化原油破乳电脱盐专利技术--超声波-电场联合破乳脱盐组合技术采用顺逆流方式.该技术于2003年9月在齐鲁分公司完成工业应用试验后,超声波强化原油破乳设备直接投入生产运行,在不加入化学破乳剂的情况下,可使胜利混输原油(平均盐浓度为50 mg/L,平均水质量分数为0.5%~1.0%)脱后盐浓度低于3 mg/L,水质量分数小于0.3%. 相似文献
6.
MPTA型原油脱金属剂的工业应用 总被引:2,自引:2,他引:0
在对高金属含量原油进行初步评价的基础上,利用SH—Ⅰ型电脱盐试验仪对自主开发的MPTA型原油脱金属剂进行了原油脱金属的实验室研究。结果表明,当MPTA型脱金属剂加入量为250μg/g时,钙的脱除率可达97.4%,并且对其它金属元素,如镍、铁、钠、锰、铝和钒也有明显的脱除效果。该剂在山东恒源石油化工股份有限公司重交沥青车间500kt/a的电脱盐装置上进行原油脱金属工业试验的结果表明,经过二级电脱盐处理后,钙的脱除率达到99.1%,钠的脱除率为94.6%,铁的脱除率为82.9%,并可在一定程度上降低原油中镍和铜的含量。使用MPTA型原油脱金属剂显著降低了一、二级电脱盐装置的电场电流,有利于炼油厂的节能降耗。 相似文献
7.
P. G. Muzykov Y. I. Khlebnikov S. V. Regula Y. Gao T. S. Sudarshan 《Journal of Electronic Materials》2003,32(6):505-510
To establish fast, nondestructive, and inexpensive methods for resistivity measurements of SiC wafers, different resistivity-measurement
techniques were tested for characterization of semi-insulating SiC wafers, namely, the four-point probe method with removable
graphite contacts, the van der Pauw method with annealed metal and diffused contacts, the current-voltage (I-V) technique,
and the contactless resistivity-measurement method. Comparison of different techniques is presented. The resistivity values
of the semi-insulating SiC wafer measured using different techniques agree fairly well. As a result, application of removable
graphite contacts is proposed for fast and nondestructive resistivity measurement of SiC wafers using the four-point probe
method. High-temperature van der Pauw and room-temperature Hall characterization for the tested semi-insulating SiC wafer
was also obtained and reported in this work. 相似文献
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9.
The motional transition and heterogeneity of semi‐interpenetrating networks (SIPNs) based on polyurethane (PU) with carboxylic groups and methacrylic copolymer (PM) with tertiary amine groups were studied by the electron spin resonance (ESR) spin probe method. The concentration of functional groups in both prepolymers varied from 0 to 0.45 mmol g?1. Spin‐probed SIPNs show that the temperature‐dependent spectra are sensitive to polymer interactions imposed by functional groups. These interactions determine the free volume distribution in the matrix and temperature at which motional transition takes place. The fraction of free volume increases with functional group concentration and reaches its maximum at 0.25 mmol g?1. Further increases in the functional group concentration reduce the free volume. The results of the networks with strong interactions are discussed in terms of the interference of the plasticizing effect of the PU component and the formation of possible cluster cross‐links, which restricts segmental motions. Copyright © 2003 Society of Chemical Industry 相似文献
10.
介绍了用单根光纤传输测量信号和功率信号的光功率推动液体压力测量仪及其工作原理。该仪器以电容式压力传感器的δ元件作为压力检测元件,采用低功耗前置器电路和简单直杆结构,实现了便携式测量。测量范围为O~100kPa,精度为O.01kPa。 相似文献