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摩擦诱发高铬铸铁相变的透射电镜研究 总被引:2,自引:0,他引:2
利用透射电子显微镜研究了高铬铸铁在摩擦过程中的显微组织变化。结果表明:奥氏体基体在摩擦应力的作用下发生相变。摩擦表面形成α‘M。次表层形成γ与α’M共存区;γ与.ε共存区;γ位错丛聚区。 相似文献
3.
Thin film of Ti-Ni alloy has a potential to perform the microactuation functions required in the microelectromechanical system (MEMS).It is essential, however, to have good uniformity in both chemical composition and thickness to realize its full potential as an active component of MEMS devices.Electron beam evaporation technique was employed in this study to fabricate the thin films of Ti-Ni alloy on different substrates.The targets used for the evaporation were first prepared by electron beam melting.The uniformity of composition and microstructure of the thin films were characterized by electron probe microanalysis (EPMA), Auger electron spectroscopy (AES), X-ray diffraction (XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM) and transmission electron microscopy (TEM).The mechanical property of the thin films was evaluated by the nano-indentation test.The martensitic transformation temperature was measured by differential scanning calorimetry (DSC).It is confirmed that the chemical composition of deposited thin films is identical to that of the target materials.Furthermore, results from depth profiling of the chemical composition variation reveal that the electron beam evaporation process yields better compositional homogeneity than other conventional methods such as sputtering and thermal evaporation.Microstructural observation by TEM shows that nanometer size precipitates are preferentially distributed along the grain boundaries of a few micron size grains.The hardness and elastic modulus of thin films decreases with an increase in Ti contents. 相似文献
4.
Corrosion-Electrochemical behavior of a commercial API5CT grade L80 type 13Cr tubing enriched with microalloying elements
is studied in 6, 7.5, 9, 12 and 15% HCl solutions by electrochemical methods. The objective is to contribute to the comprehension
of corrosion phenomena caused by HCl of similar concentrations, generally used in acidizing job. The corrosion morphology
is examined by scanning electron microscopy (SEM) coupled with EDAX. The soluble corrosion products are analyzed by atomic
absorption spectroscopy and colorimetric methods. General, as well as localized, corrosion is present. The severest general
corrosion with a maximum rate of 26 mm/year is obtained at 15% HCl. The localized corrosion which morphologically differs
as function of HCl concentrations is revealed by SEM investigation. In all the above HCl solutions, the commercial 13% Cr
martensitic stainless steel tubing shows no passive state. Above 6% HCl, the microalloying elements promote forming a discontinuous
film of the corrosion products. The corrosion rate slightly decreases in 15% HCl compared to the published data on a conventional
13% Cr martensitic stainless steel tubing. This is due to both the chemical composition (silicon, manganese and vanadium)
and microstructural properties. Copper seems to additionally accelerate the corrosion of the alloy.
Published in Russian in Zashchita Metallov, 2007, Vol. 43, No. 4, pp. 372–380.
The article was translated by the authors in English. 相似文献
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L.Wang D.Xu B.C.CaiInformation Storage Research Center Shanghai Jiao Tong University Shanghai China Manuscript received September in revised form November 《金属学报(英文版)》2002,15(4):391-395
TiNi thin films were sputter-deposited on circular single-cry stal silicon substrates un-der various sputtering parameters. The crystal structure and residual stress of the as-deposited films were determined by X-ray diffraction and substrate-curvature method. The phenomenon of stress-suppressed martensitic transformation was observed. R is considered that the residual stresses in SMA thin films based on circular substrates act as balanced biaxial tensile stresses. The status of equilibrant delays the align-ment of self-accommodated variants and the volume shrinkage during the martensitic transformation. 相似文献
7.
XIE Changsheng SUN Peizhen ZHAO Jiansheng CHEN Yuqiu Huazhong University of Science Technology Wuhan China XIE Changsheng Associate Professor Department of Mechanical Engineering No. Huazhong University of Science Technology Wuhan China 《金属学报(英文版)》1990,3(1):52-57
The microstructures of Fe-Mn-Ni-Cr steels with medium carbon and the effect of alloy ele-ments on them have been investigated by means of X-ray diffraction quantitative phase ana-lyses,metallography and hardness tests.The volume fraction of martensite in steels quenchedat 1100℃ can be expressed as:f_M~(1100)=162.643-15.482Mn-7.36Ni-4.286(Cr+Mo+V)Based on this expression,the quasi-equilibrium microstructure diagram has been obtained.Itis shown that the effect of Mn on the austenite stability is greater than that of Ni.The equiva-lent [Ni]=2.104Mn+Ni and equivalent [Cr]=Cr+Mo+V.The driving force for martensite transformation at M_s point has been calculated to hedrastically decreased by element Mn. 相似文献
8.
本文利用X射线定量相分析及金相观察和硬度测试,考察了中碳Fe-Mn-Ni-Cr钢的组织及合金元素的作用。建立了经1100℃淬火后的马氏体体积分数与合金成分的定量关系式; f_M~(1100)=162.643-15.482Mn-7.36Ni-4.286(Cr+Mo+V)并在此基础上给出了亚平衡组织图。结果表明,Mn稳定奥氏体的作用大于Ni的作用。Ni和Cr当量分别以[Ni]=2.104Mn+Ni,[Cr]=Cr+Mo+V表示。计算了M_S点处的马氏体相变驱动力,指出Mn具有强烈降低相变驱动力的作用。 相似文献
9.
10.
G. X. Zhao M. Zheng X. H. Lv X. H. Dong H. L. Li 《Metals and Materials International》2005,11(2):135-140
The corrosion behavior of 13Cr martensitic stainless steel in a CO2 environment in a stimulated oilfield was studied with potentiodynamic polarization and the impedance spectra technique. The
results showed that the microstructure of the surface scale clearly changed with temperature. This decreased the sensitivity
of pitting corrosion and increased the tendency toward general (or uniform) corrosion. The capacitance, the charge transfer
resistance, and the polarization resistance of the corrosion product scale decrease with increasing temperature from 90 to
120 °C, and thus the corrosion is a thermal activation controlled process. Charge transfer through the scale is difficult
and the corrosion is controlled by a diffusion process at a temperature of 150 °C. Resistance charge transfer through the
corrosion product layer is higher than that in the passive film. 相似文献